Organic electroluminescent device and preparation method thereof
An electroluminescent device and luminescent technology, which is applied in the direction of electric solid device, semiconductor/solid device manufacturing, electrical components, etc., to achieve the effect of high compactness, high thermal stability, and prolong service life
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Embodiment 1
[0054] A method for preparing an organic electroluminescent device, comprising the following steps:
[0055] (1) Preparation of luminescent functional layer and cathode on the anode substrate
[0056] a. Pretreatment of conductive glass substrate
[0057] Take the ITO glass substrate, wash it with acetone, ethanol, pure water and ethanol in sequence, and use an ultrasonic cleaner to clean it for 5 minutes each time. After drying, clean the surface of the cleaned ITO glass substrate. Activation treatment; ITO thickness 100nm;
[0058] b. Preparation of luminescent functional layer and cathode
[0059] A hole injection layer, a hole transport layer, a light-emitting layer, an electron transport layer, an electron injection layer and a cathode are sequentially prepared on an ITO glass substrate by vacuum evaporation;
[0060] Preparation of the hole injection layer: the MoO 3 Doped into N,N'-diphenyl-N,N'-di(1-naphthyl)-1,1'-biphenyl-4,4'-diamine (NPB) as hole injection layer...
Embodiment 2
[0074] A method for preparing an organic electroluminescent device, comprising the following steps:
[0075] (1) Preparation of luminescent functional layer and cathode on the anode substrate
[0076] Same as embodiment 1.
[0077] (2) The encapsulation layer unit is repeatedly prepared on the cathode for 5 times to form an encapsulation layer with a composite structure to obtain an organic electroluminescent device;
[0078]The encapsulation layer unit includes a mixed barrier layer and an inorganic barrier layer stacked in sequence;
[0079] a. A mixed barrier layer with a thickness of 300nm is prepared on the surface of the cathode by vacuum evaporation, and the material of the mixed barrier layer is NPB doped with V 2 o 5 A mixed material formed with Al, in the mixed material, V 2 o 5 The mass fraction is 40%, the mass fraction of Al is 30%, and the vacuum degree of the evaporation process is 5×10 -5 Pa, the evaporation rate is
[0080] b. Prepare an inorganic bar...
Embodiment 3
[0084] A method for preparing an organic electroluminescent device, comprising the following steps:
[0085] (1) Preparation of luminescent functional layer and cathode on the anode substrate
[0086] Same as embodiment 1.
[0087] (2) The encapsulation layer unit is repeatedly prepared on the cathode for 5 times to form an encapsulation layer with a composite structure to obtain an organic electroluminescent device;
[0088] The encapsulation layer unit includes a mixed barrier layer and an inorganic barrier layer stacked in sequence;
[0089] a. A mixed barrier layer with a thickness of 200nm is prepared on the surface of the cathode by vacuum evaporation, and the material of the mixed barrier layer is Alq3 doped WO 3 The mixed material formed with Ni, in the mixed material, WO 3 The mass fraction of Ni is 30%, the mass fraction of Ni is 10%, and the vacuum degree of the evaporation process is 5×10 -5 Pa, the evaporation rate is
[0090] b. Prepare an inorganic barrie...
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