A kind of platinum-nickel alloy superfine wire and its preparation method and application

A platinum-nickel alloy and ultra-fine wire technology, which is applied in other medical devices, guide wires, and pharmaceutical devices, can solve the problems of domestic production capacity that cannot meet demand, high comprehensive performance requirements, and poor biocompatibility, and achieve Good plasticity, excellent comprehensive performance, strong plasticity and ability to maintain plasticity

Active Publication Date: 2021-06-08
GRIKIN ADVANCED MATERIALS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In order to facilitate the doctor to accurately grasp the length and position of the guide wire entering the blood vessel during the operation, a development design is usually made on the front end of the guide wire, such as using a pure gold or platinum coil, but there are problems of low strength, poor plasticity, and high price; Some guide wires use spring coils made of titanium-nickel alloy and platinum-tungsten alloy wire. Although they have a certain developing effect and high strength, they have problems such as poor elasticity or poor biocompatibility.
[0004] The guide wire of the PTCA surgical delivery system requires extremely thin wire diameter at the developing end and high comprehensive performance requirements. The domestic ultra-fine wire industry is mainly dominated by foreign manufacturers, and the core technology of production is also mainly mastered by foreign manufacturers. The domestic production capacity is far away. Unable to meet the demand, especially in the field of ultra-fine wire used in the medical industry, the products are mainly imported from manufacturers such as Germany, the United States, and Japan

Method used

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Examples

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Effect test

preparation example Construction

[0043] A method for preparing a platinum nickel alloy ultrafine material, including the following steps:

[0044] 1) Take platinum, nickel as the raw material, using a vacuum induction melt furnace to melt, the vacuum induction of the molten, the vacuum degree of 10 -1 ~ 10 -2 PA; after the full-melting heat regenerative time is 5 ~ 10 min; copper mold, 5 to 30 minutes after pouring quenching cooling, obtain a platinum nickel alloy ingot, platinum nickel alloy ingot size is

[0045] 2) Rolling the platinum nickel alloy ingot by a hole type rolling mill, the amount of the quarter deformation is 10% to 20% during rolling, forming a platinum nickel alloy bar;

[0046] 3) Pulling processing and heat treatment: pull the platinum nickel alloy bar to pull into a filament material through a brigadier, and the amount of deformation of the drawing processing is 5% ~ 15%, when the amount of deformation reaches 70% to 90%, It performs intermediate heat treatment, the intermediate heat treatm...

Embodiment 1

[0053] 1) Platinum, nickel is a raw material ingredient, and the nickel content is 7 wt.%, The margin is platinum. Zirconia or aluminum oxide 坩 坩, Copper mold, using a vacuum induced melting furnace to smelt, the vacuum is maintained in × 10 -1 ~ × 10 -2 PA, full-melting insulation refining time 5 ~ 10 min; 5 min after pouring, quenching cooling, obtain platinum nickel alloy ingot;

[0054] 2) Hold the platinum nickel alloy ingot with a hole rolling mill, the amount of the quarter deformation is 10% to 20%, forming a bar;

[0055] 3) Pulling processing: Pull the bar into thin wire through the drawing machine, the quarter-deformed amount is 5% to 15%, the deformation amount reaches 70% to 90% to perform intermediate heat treatment, heat treatment temperature 750 ° C, according to the diameter according to the wire The small annealing insulation time is 30, 20, 10 min, respectively. Get the diameter of the filament material

[0056] 4) Filament secondary draw processing: put the d...

Embodiment 2

[0061] Platinum nickel alloy ingredient ratio is in Example 1, processing steps 2) to 4), 6) as in Example 1. Step 5) The continuous annealing temperature is 800 ° C, annealing time 30s. The obtained finished film is smooth, soft, and detects the detection mechanical properties of the wire material, and the results are shown in Table 1.

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PUM

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Abstract

The invention discloses a platinum-nickel alloy superfine wire material, a preparation method and an application thereof, which belong to the technical field of nonferrous metal alloy processing. The Ni content of the ultra-fine wire is 5wt.%-15wt.%, the balance is Pt, the diameter is 1200-1500MPa in tensile strength, and the elongation is 3%-20%. The preparation method is as follows: use platinum and nickel as raw materials, use a vacuum induction melting furnace to melt, refine, and vacuum cast to obtain a platinum-nickel alloy ingot; use a groove rolling mill to roll the ingot to form a platinum-nickel alloy bar Drawing the rods into thin wires through a wire drawing machine, and performing intermediate heat treatment; performing secondary drawing processing on the thin wires to obtain secondary drawn wires; and then performing continuous annealing to obtain ultra-fine wires. The platinum-nickel alloy ultra-fine wire has excellent comprehensive performance, not only has a good developing effect, but also has high mechanical properties, has a strong ability to maintain plasticity, has a smooth surface, and has good flexibility, which can meet the use of the PTCA guide wire developing spring Require.

Description

Technical field [0001] The present invention belongs to the field of colored metal alloy processing, and more particularly to a platinum nickel alloy ultrafine material and a preparation method thereof. Background technique [0002] PTCA (Percutaneous Transluminal Coronary Angioplasty) is a referred to as the peripheral angioplasty, refers to a coronary artery or an implanted stent using a balloon expanded stenosis, and has a blood flow. The emergency PTCA bracket implantation technology is widely used in the treatment of patients with acute myocardial infarction of coronary heart disease. The treatment effect is more reliable than drug treatment, and it is simple and traumatic, which has become a major patient with acute myocardial infarction of coronary heart disease. One of therapeutic measures. [0003] As the guidance of the PTCA surgical delivery system, it is a "track" to provide "track" by a coronary stenosis or occlusion loss to the distal end of the blood vessel, and pr...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22C5/04C22C1/02C22F1/14C22F1/02B21C37/04A61M25/09
CPCA61M25/09A61M2025/09133A61M2205/32A61M2207/00B21C37/047C22C1/02C22C5/04C22F1/02C22F1/14
Inventor 张巧霞罗俊锋罗瑶郭珊珊刘丹徐国进关静李勇军
Owner GRIKIN ADVANCED MATERIALS
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