A kind of platinum-nickel alloy superfine wire and its preparation method and application
A platinum-nickel alloy and ultra-fine wire technology, which is applied in other medical devices, guide wires, and pharmaceutical devices, can solve the problems of domestic production capacity that cannot meet demand, high comprehensive performance requirements, and poor biocompatibility, and achieve Good plasticity, excellent comprehensive performance, strong plasticity and ability to maintain plasticity
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preparation example Construction
[0043] A method for preparing a platinum nickel alloy ultrafine material, including the following steps:
[0044] 1) Take platinum, nickel as the raw material, using a vacuum induction melt furnace to melt, the vacuum induction of the molten, the vacuum degree of 10 -1 ~ 10 -2 PA; after the full-melting heat regenerative time is 5 ~ 10 min; copper mold, 5 to 30 minutes after pouring quenching cooling, obtain a platinum nickel alloy ingot, platinum nickel alloy ingot size is
[0045] 2) Rolling the platinum nickel alloy ingot by a hole type rolling mill, the amount of the quarter deformation is 10% to 20% during rolling, forming a platinum nickel alloy bar;
[0046] 3) Pulling processing and heat treatment: pull the platinum nickel alloy bar to pull into a filament material through a brigadier, and the amount of deformation of the drawing processing is 5% ~ 15%, when the amount of deformation reaches 70% to 90%, It performs intermediate heat treatment, the intermediate heat treatm...
Embodiment 1
[0053] 1) Platinum, nickel is a raw material ingredient, and the nickel content is 7 wt.%, The margin is platinum. Zirconia or aluminum oxide 坩 坩, Copper mold, using a vacuum induced melting furnace to smelt, the vacuum is maintained in × 10 -1 ~ × 10 -2 PA, full-melting insulation refining time 5 ~ 10 min; 5 min after pouring, quenching cooling, obtain platinum nickel alloy ingot;
[0054] 2) Hold the platinum nickel alloy ingot with a hole rolling mill, the amount of the quarter deformation is 10% to 20%, forming a bar;
[0055] 3) Pulling processing: Pull the bar into thin wire through the drawing machine, the quarter-deformed amount is 5% to 15%, the deformation amount reaches 70% to 90% to perform intermediate heat treatment, heat treatment temperature 750 ° C, according to the diameter according to the wire The small annealing insulation time is 30, 20, 10 min, respectively. Get the diameter of the filament material
[0056] 4) Filament secondary draw processing: put the d...
Embodiment 2
[0061] Platinum nickel alloy ingredient ratio is in Example 1, processing steps 2) to 4), 6) as in Example 1. Step 5) The continuous annealing temperature is 800 ° C, annealing time 30s. The obtained finished film is smooth, soft, and detects the detection mechanical properties of the wire material, and the results are shown in Table 1.
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