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Preparation method of overbased bactericide

A bactericide and alkaline technology, which is applied in the preparation of super-alkaline bactericide and electrolyzed water to prepare super-alkaline ionized water, which can solve the problems of poor bactericidal effect of bactericide, high energy consumption, and small amount of treated water.

Active Publication Date: 2021-03-19
广州市婷采化妆品有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] However, the above-mentioned bactericides have low catalytic efficiency due to the cathode electrode used in the electrolysis process, so that the energy consumption in the electrolysis process is high, the amount of treated water is small, and the bactericidal effect of the obtained bactericides is poor.

Method used

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  • Preparation method of overbased bactericide
  • Preparation method of overbased bactericide
  • Preparation method of overbased bactericide

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0079] The preparation method of negative electrode comprises following preparation method:

[0080] (1) Use nickel salt, aluminum salt, lanthanum salt, alkylimidazole halide, ethanedithiol as electrolyte molten salt, copper mesh or nickel mesh as cathode, high-purity aluminum plate as anode, electrodeposition condition 5A / dm 2 , temperature 40 o C, time 30minh, inert gas atmosphere.

[0081] (2) Place the electrode deposited in step (2) in an alkaline solution for corrosion treatment: the alkaline solution is 30wt.% NaOH, a mixture of deionized water and ethanol with a volume ratio of 4:1, accompanied by ultrasound Stirring 30kHz, temperature 30 o c.

[0082] (3) Place the cathode heat-treated in step (2) under the condition of inert gas for heat treatment. The heat treatment takes 12 hours and the temperature is 450 o c.

[0083] (4) Washing and drying: washing with deionized water and air drying in cold air.

[0084] Nickel salt is nickel sulfate or nickel nitrate, 15...

Embodiment 2

[0090] The preparation method of negative electrode comprises following preparation method:

[0091] (1) Use nickel salt, aluminum salt, lanthanum salt, alkylimidazole halide, ethanedithiol as electrolyte molten salt, copper mesh or nickel mesh as cathode, high-purity aluminum plate as anode, electrodeposition condition 10A / dm 2 , temperature 45 o C, time 2h, inert gas atmosphere.

[0092] (2) Place the electrode deposited in step (2) in an alkaline solution for corrosion treatment: the alkaline solution is 32.5wt.% NaOH, a mixture of deionized water and ethanol with a volume ratio of 4:1.25, accompanied by Ultrasonic stirring 35kHz, temperature 33 o c.

[0093] (3) Place the cathode that has been heat-treated in step (2) under inert gas conditions for heat treatment. The heat treatment takes 18 hours and the temperature is 600 o c.

[0094] (4) Washing and drying: washing with deionized water and air drying in cold air.

[0095] Nickel salt is nickel sulfate or nickel n...

Embodiment 3

[0101] The preparation method of negative electrode comprises following preparation method:

[0102] (1) Use nickel salt, aluminum salt, lanthanum salt, alkylimidazole halide, ethanedithiol as electrolyte molten salt, copper mesh or nickel mesh as cathode, high-purity aluminum plate as anode, electrodeposition condition 15A / dm 2 , temperature 50 o C, time 4h, inert gas atmosphere.

[0103] (2) Place the electrode deposited in step (2) in an alkaline solution for corrosion treatment: the alkaline solution is 35wt.% NaOH, a mixture of deionized water and ethanol with a volume ratio of 4:1.5, accompanied by ultrasound Stirring 40kHz, temperature 35 o c.

[0104] (3) Place the cathode heat-treated in step (2) under the condition of inert gas for heat treatment, the heat treatment time is 24 hours, and the temperature is 650 o c.

[0105] (4) Washing and drying: washing with deionized water and air drying in cold air.

[0106] Nickel salt is nickel sulfate or nickel nitrate, ...

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Abstract

According to the invention, a sulfur-doped porous Ni-La / foam metal material is used as a cathode, an inert metal material is used as an anode, an electrolytic cell is divided into an anode chamber, amiddle chamber and a cathode chamber through an ion exchange membrane, a mixed solution of potassium carbonate, potassium bicarbonate and purified water is introduced into the middle chamber, water ispurified into the cathode chamber and the anode chamber, and the power supply is powered on to electrolyze to obtain the bactericide, wherein the pH value of the bactericide is equal to 12.5 + / -0.3,no surfactant, preservative or other additive is added, the main components are purified water and trace mineral elements, and the cleaning effect of the bactericide is greater than 99.9%.

Description

technical field [0001] The invention relates to a preparation method of a superalkaline bactericide, which belongs to the field of electrolyzing water to prepare superalkaline ionized water, which is used in the field of bactericides, disinfectants and cleaning agents. Background technique [0002] At present, the disposable antibacterial hand sanitizers on the market are based on various chemically synthesized surfactants. In order to make them have antibacterial functions, various bactericides are added. In order to avoid the damage of various agents to the skin, there are also Different skin care agents will be added, but although these products have a certain decontamination ability, they are relatively sticky after use, and the experience is not strong, and the hazards of the surfactants contained in the products have been widely concerned in recent years. The focus is mainly on the irritation to the mucous membrane, sensitization to the skin, toxicity, heredity, carcin...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A01N59/00A01P1/00A01P3/00C25D3/66C25D5/34C25D5/40C25D5/48C25D5/50
CPCA01N59/00C25D3/665C25D5/34C25D5/40C25D5/48C25D5/50
Inventor 杜先明
Owner 广州市婷采化妆品有限公司
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