Production process of feed-grade ferrous glutamate
A technology of ferrous glutamate and production process, applied in the general layout of feeding device, crystallization device, chemical/physical/physical-chemical process, etc., can solve the problem of low bioavailability, increase of secretory cells, and nutrient absorption capacity Reduce and other problems, to achieve the effect of simple post-processing, low process energy consumption, and low equipment cost
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Embodiment 1
[0026] see Figure 1-3 :
[0027] (1) Add deionized water and feed grade glutamic acid in reactor 1;
[0028] (2) Slowly input ferric sulfate into reactor 1 through slow injector 2, the molar ratio of total iron content to glutamic acid is 1:1, stir in reactor 1 and heat up to 55°C;
[0029] (3) continue to heat up, control reaction temperature 75 ℃, keep warm for 30min, make raw material generate ferrous glutamate chelate through sufficient reaction;
[0030] (4) stop heating, open reactor 1 outlet valve, the liquid phase part falls into the bottom of crystallization tank 3 after the material in reactor 1 is filtered through strainer 5, makes the temperature in crystallization tank 4 drop to 25 ℃, obtains glutamic acid Ferrous product, when the material in the reactor 1 falls, it hits the vibrating plate 601, and the vibrating plate 601 is hit and reacted by the spring 605, and the vibration drives the material on the filter screen 5 to vibrate, assisting the further separa...
Embodiment 2
[0033] see Figure 1-3 :
[0034] (1) Add deionized water and feed grade glutamic acid in reactor 1;
[0035] (2) Slowly input ferric sulfate into reactor 1 through slow injector 2, the molar ratio of total iron content to glutamic acid is 1:1, stir in reactor 1 and heat up to 60°C;
[0036] (3) continue to heat up, control reaction temperature 80 ℃, keep warm for 30min, make raw material generate ferrous glutamate chelate through sufficient reaction;
[0037] (4) Stop heating, open the reactor 1 outlet valve, the liquid phase part falls into the bottom of the crystallization tank 3 after the material in the reactor 1 is filtered through the filter screen 5, the temperature in the crystallization tank 4 is reduced to 28 ℃, and glutamic acid is obtained Ferrous product, when the material in the reactor 1 falls, it hits the vibrating plate 601, and the vibrating plate 601 is hit and reacted by the spring 605, and the vibration drives the material on the filter screen 5 to vibr...
Embodiment 3
[0040] see Figure 1-3 :
[0041] (1) Add deionized water and feed grade glutamic acid in reactor 1;
[0042] (2) Slowly input ferric sulfate into reactor 1 through slow injector 2, the molar ratio of total iron content to glutamic acid is 1:1, stir in reactor 1 and heat up to 65°C;
[0043] (3) continue to heat up, control reaction temperature 85 ℃, keep warm for 30min, make raw material generate ferrous glutamate chelate through sufficient reaction;
[0044] (4) stop heating, open reactor 1 outlet valve, the liquid phase part falls into the bottom of crystallization tank 3 after the material in reactor 1 is filtered through strainer 5, makes the temperature in crystallization tank 4 drop to 30 ℃, obtains glutamic acid Ferrous product, when the material in the reactor 1 falls, it hits the vibrating plate 601, and the vibrating plate 601 is hit and reacted by the spring 605, and the vibration drives the material on the filter screen 5 to vibrate, assisting the further separa...
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