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Anti-radiation ceramics and preparation method thereof

A radiation protection, ceramic technology, applied in shielding, nuclear engineering, reactors, etc., can solve the problem of mixing uniformity of ferrite and substrate, difficulty in forming and processing of absorbing agent, affecting electromagnetic performance of ferrite, etc. problem, to achieve the effect of suitable for industrial application, good effect, accurate control of chemical composition

Inactive Publication Date: 2011-11-16
HEBEI UNIV OF TECH +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

The common defect of these methods is: the mixing problem of ferrite and substrate, or the problem of mixing uniformity of ferrite and substrate cannot be solved, thus affecting the electromagnetic properties of ferrite
Chinese patent CN 1644546A reports a "composite wave-absorbing material and its preparation process". It adopts the citrate sol-gel method to prepare a barium ferrite layer on the surface of porous glass phase particles, so that it can generate electromagnetic waves. Certain absorption, but there is a certain difficulty in forming and processing wave absorbing agent; Chinese patent CN1807537A discloses a "preparation method of dielectric / magnetic composite wave absorbing powder", which adopts in-situ deposition method to prepare composite The production process of microwave-absorbing materials is complex, time-consuming and labor-intensive, which greatly limits the mass production of materials; Chinese patent CN 1905079A introduces an "electromagnetic compatible anechoic composite wave-absorbing material and its manufacturing method", which refers to the Adding a transition matching section between the ammonia vinegar absorbing material and the ferrite material can have good absorbing performance at high frequencies, but the thickness of the transition matching section is 50mm±2mm, and the matching performance becomes a problem

Method used

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preparation example Construction

[0030] The present invention has designed the preparation method (abbreviation preparation method) of described pottery simultaneously, and the technological design of this preparation method is:

[0031] 1 batching: composition selection and batching according to the percentage by weight of ceramic firing raw materials of the present invention;

[0032]2 Mixing: first ball mill the following raw material components in the raw material composition to the following average particle size: ferrite 2-3μm, zinc oxide 2-3μm, metal powder 2-3μm, kaolin 3-5μm, oxide Silicon 2-5 μm, alumina 8-9 μm, calcium oxide 3-5 μm, tourmaline 8-9 μm; then mix with the cellulose and rare earth in the weight percentage, and mix for 18-36 hours;

[0033] 3 Granulation: adding 3-8% water of the total weight of the constituent raw materials, spraying and granulating in a spray granulation tower;

[0034] 4 Molding: dry pressing molding with product design mold, molding pressure 250-350MPa;

[0035] 5...

Embodiment 1

[0042] A mobile phone anti-radiation ceramic sheet (hereinafter referred to as ceramic sheet) is manufactured.

[0043] The weight percentage composition (raw material component 1) of this ceramic sheet firing raw material is: strontium iron oxide 44%, zinc oxide 23%, copper powder 8%, silicon oxide 5%, aluminum oxide 5%, kaolin 5%, calcium oxide 5%, neodymium nitrate 2%, ferrite tourmaline 1% and cellulose 2%;

[0044] The preparation method of the ceramic sheet is as follows:

[0045] 1 Ingredients: select raw materials and prepare ceramic sheet raw materials according to the weight percentages described in raw material component 1;

[0046] 2. Ball milling: first ball mill the following raw materials in the raw material components to the following average particle size: strontium iron oxide 2.5 μm, zinc oxide 2.5 μm, copper powder 2.5 μm, kaolin 4 μm, silicon oxide 3 μm, aluminum oxide 8 μm, calcium oxide 4 μm, tourmaline 8 μm; then mix evenly with 2% (weight, the same be...

Embodiment 2

[0053] Creates a ceramic sheet. The weight percentage composition of the sintering raw material (raw material component 2) is: 34% of barium iron oxide, 23% of zinc oxide, 8% of nickel powder, 10% of silicon oxide, 5% of aluminum oxide, 8% of kaolin, 5% of calcium oxide, Europium nitrate 4%, Magnesite 2% and Cellulose 1%.

[0054] The following raw materials in the raw material component 2 were respectively ball milled to the following average particle size: barium ferrite 2 μm, zinc oxide 2 μm, nickel powder 2 μm, kaolin 3 μm, silicon oxide 2 μm, aluminum oxide 8 μm, calcium oxide 3 μm, tourmaline 8 μm; then mix evenly with 1% cellulose and 4% europium nitrate, and mix for 18 hours; add 3% water spray granulation of the total weight of the raw material formula; molding pressure 300MPa; control the moisture content of the billet before firing 1.5%; Other operations and technology are the same as embodiment 1.

[0055] The electromagnetic wave radiation tester QX-5 was used t...

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Abstract

The present invention relates to an anti-radiation ceramics and a preparation method thereof. The ceramics is characterized in that the ceramics is composed of the following firing raw materials by weight percentage: 20-45 percent ferrite, 20-30 percent zinc oxide, 5-10 percent metal powder, 5-10 percent silicon oxide, 5-10 percent aluminium oxide, 5-10 percent kaolin, 5-10 percent calcium oxide, 1-5 percent rare earth, 1-5 percent tourmaline and 1-2 percent cellulose, the sum of the various components is 100 percent; the ferrite is strontium iron oxide, barium iron oxide or cobalt iron oxide; the metal powder is copper powder, iron powder or nickel powder; the kaolin is calcined kaolin; the rare earth is at least one of lanthanum nitrate, neodymium nitrate, praseodymium nitrate, europium nitrate and erbium nitrate; and the tourmaline is at least one of iron tourmaline, lithium tourmaline and magnesium tourmaline. The preparation method of the ceramics comprises: 1) material preparation: selecting and preparing materials according to the raw materials of the invention; 2) ball milling and material mixing; 3) granulation; 4) shaping; 5) drying; and 6) firing.

Description

technical field [0001] The invention relates to functional ceramic technology, in particular to a ceramic with radiation protection function and a preparation method thereof. Background technique [0002] With the advancement of science and technology and the rapid development of the information industry, equipment or systems such as computers, mobile phones, fax machines, telephones, and networks have been widely used in the processing of information generation, transmission, reception, and storage. This type of equipment is inseparable from the action of electromagnetic waves when working. The wide application of electromagnetic waves has brought increasingly serious electromagnetic interference and pollution. One of the effective ways to reduce electromagnetic interference is to use microwave absorbing (receiving) materials. When the electromagnetic wave passes through the wave-absorbing material, electromagnetic wave loss will occur, so that the energy of the electroma...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G21F1/08C04B35/40C04B35/453C04B35/622
Inventor 梁金生王丽娟孟军平胡波刘振田张谋
Owner HEBEI UNIV OF TECH
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