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34results about How to "Good microwave absorption characteristics" patented technology

Ni-based alloy magnetic microwave absorbing material and preparation method thereof

The invention discloses a Ni-based alloy magnetic microwave absorbing material and a preparation method thereof. The stoichiometric proportions of a molecular formula of the magnetic microwave absorbing material are as follows: 16.67% of Pr, 83.33%-75% of Ni and 0-8.33% of Fe. The Ni-based alloy magnetic microwave absorbing material is prepared by the following main steps: smelting Pr, Fe and Ni metals, of which the purities are greater than or equal to 99.50% as raw materials under argon or vacuum protection; carrying out heat treatment on a cast ingot at 600-1100 DEG C under vacuum or argon protection; quenching with ice water; and grinding into powder and carrying out ball milling to form powder after mechanically crushing. The Ni-based alloy disclosed by the invention has the advantages of relatively good microwave absorbing effect, wide absorbing frequency band, simple preparation process, high antioxidant resistance and the like in a 2-18GHz of microwave band; and the Ni-based alloy magnetic microwave absorbing material disclosed by the invention is suitable for preparation of microwave absorbing products of requiring wide absorbing frequency band, good wave absorbing property and high corrosion resistance in the magnetic wave absorbing material.
Owner:GUILIN UNIV OF ELECTRONIC TECH

LaCeNi magnetic wave absorbing material and preparation method thereof

The invention discloses a LaCeNi magnetic microwave absorbing material and a preparation method thereof. The stoichiometric proportions of a molecular formula of the magnetic wave absorbing material are as follows: 10.0%-16.7% of La, 0-6.0% Ce and 83.3% Ni. The LaCeNi magnetic microwave absorbing material is prepared by the following main steps: smelting La, Ce and Ni metals, of which the purities are greater than or equal to 99.90% as raw materials under argon protection; carrying out heat treatment on a cast ingot in vacuum at 800-1050 DEG C; quenching with ice water; and carrying out ball-milling to form powder after mechanically crushing. The LaCeNi magnetic microwave absorbing material has relatively excellent microwave absorbing property in a 2-18GHz of microwave band; when the thickness of a compound is 1.5mm, the minimal absorption peak can reach about 40.1dB; the LaCeNi alloy disclosed by the invention has the advantages of good wave absorbing property, wide absorbing frequency band, simple preparation process, good corrosion resistance and the like in the 2-18GHz of microwave band; and the LaCeNi magnetic microwave absorbing material disclosed by the invention is suitable for preparation of microwave absorbing products of requiring wide absorbing frequency band, good wave absorbing property and good corrosion resistance in the magnetic wave absorbing material.
Owner:GUILIN UNIV OF ELECTRONIC TECH +1

HoFeB/Fe3O4 wave-absorbing composite material and preparation method thereof

The invention provides a HoFeB/Fe3O4 wave-absorbing composite material and a preparation method thereof. The HoFeB/Fe3O4 wave-absorbing composite material is suitable for the field of microwave absorbing materials. The preparation method includes the following steps that Ho, Fe and B with the purity equal to or more than 99.95% serve as raw materials respectively and are repeatedly molten into ingots with uniform compositions in an argon atmosphere, vacuumizing is conducted, and the ingots are sealed in quartz glass for homogeneous annealing at 800 DEG C, then quenched with an ice-water mixture, mechanically crushed into powder and ball-milled into powder by using high energy; the powder obtained after high-energy ball milling and ferroferric oxide are placed in an agate mortar for grinding and mixing according to the relative molecular mass ratio, and the HoFeB/Fe3O4 composite material is obtained. The wave-absorbing composite material has a very good microwave absorbing effect in themicrowave frequency band of 2-18 GHz and a wide wave-absorbing bandwidth, has the advantages of a simple preparation process, high oxidation resistance and the like, and can be suitable for preparation of microwave absorption products which require wide wave-absorbing bandwidth, good wave-absorbing performance and high oxidation resistance.
Owner:GUILIN UNIV OF ELECTRONIC TECH

Rare earth Fe-based electromagnetic shielding material and preparation method thereof

The invention discloses a rare earth Fe-based electromagnetic shielding material and a preparation method thereof. The alloy comprises 10.5% of Nd, 81.6-89.5% of Fe and 0.0-7.9% of C in terms of atomic percent, and is prepared according to the following process: taking Nd, Fe and C with the purities of larger than or equal to 99.90% as raw materials, smelting in the protection of argon, performing uniform heat treatment to the alloy in vacuum at 800-1050 DEG C, quenching by using ice water / liquid nitrogen, performing ball milling after mechanically crushing, and performing tempering heat treatment at 50-300 DEG C to prepare a sample. The NdFeC electromagnetic shielding material has relatively excellent microwave absorbing property within a microwave band of 2-18GHz; when an alloy micropowder / paraffin compound has the thickness 1.8mm, the minimum absorption peak thereof can reach about -16.8dB; the electromagnetic shielding material has high microwave absorbing efficiency within the microwave band of 2-18GHz, a wide microwave absorbing band, high temperature stability and low economic cost, and has certain oxidation resistance and corrosion resistance; the electromagnetic shielding material is simple in preparation process, low in economic cost, and suitable for industrial production.
Owner:GUILIN UNIV OF ELECTRONIC TECH

Neodymium-iron-boron permanent magnet wave-absorbing material and preparing method thereof

The invention discloses a neodymium-iron-boron permanent magnet wave-absorbing material and a preparing method thereof. The preparing method includes the steps that ingredients are put into a medium-frequency induction furnace to be melted; rapid-hardening pouring is carried out on a melted solution to obtain rapidly-hardened melt-spun sheets; the rapidly-hardened melt-spun sheets are taken out after being cooled; the rapidly-hardened melt-spun sheets are thermally treated within the temperature ranging from room temperature to 1000 DEG C and crushed, crushed powder is screened, magnetic property parameters such as saturation magnetization intensity, residual magnetism and coercive force are detected, and electromagnetic parameters and the reflectivity R of the powder are tested; a wave absorbing material is obtained, and the wave absorbing material has good microwave absorption characteristic within the microwave band of 2-18 GHz and has multiple absorption peaks. Permanent magnet performance and wave absorbing performance of the neodymium-iron-boron material are considered, and a new direction is developed for neodymium-iron-boron development. The method is simple in preparation process, facilitates industrialization and is convenient to put into production, and the industrial production technology is mature.
Owner:GUILIN UNIV OF ELECTRONIC TECH

Magnetic hollow micro-nano material, preparation method and application thereof

The invention discloses a magnetic hollow micro-nano material, a preparation method and application thereof, and belongs to the technical field of nano materials. According to the magnetic hollow micro-nano material and the preparation method and application thereof, the magnetic hollow micro nano material prepared by a one-step liquid-phase reduction-oxidation method has novel structure and formation mechanism, the contents of Cu and Ni and the composition, feature, and structure of the magnetic hollow micro-nano material can be regulated by changing the reaction temperature, time, stirring speed, gas flow size, and reactant concentration, wherein the diameter of a micro-nano tube is 0.1 to 2 [mu]m, the length is 2 to 12 [mu]m, and the wall thickness is 10 to 140 nm; the diameter of a micro-nano sphere is 0.2 to 5 [mu]m, and the wall thickness is 10 to 180 nm. Because the magnetic hollow micro-nano material is good in dispersibility, good in homogeneity and has good microwave absorption characteristics, the magnetic hollow micro-nano material is widely used in the fields such as microwave absorbing and shield, electrocatalysis, lithium ion batteries and surface enhanced Raman spectroscopy. In addition, the disclosed preparation method is easy to operate, the environment-friendly effect is realized, industrial application potential is good, and the magnetic hollow micro-nano material and the preparation method are suitable for market promotion and application.
Owner:ZHEJIANG NORMAL UNIVERSITY

Biomass charcoal-based catalyst coupled microwave effect catalytic reforming hydrogen production method

The invention belongs to the field of biomass energy utilization, and particularly relates to a biomass charcoal-based catalyst coupled microwave effect catalytic reforming hydrogen production method which mainly comprises the steps of (1) conducting pretreatment, specifically, drying and crushing biomass to obtain a biomass raw material for later use; (2) conducting pyrolysis, specifically, putting a certain mass of biomass raw materials into a pyrolysis reactor, and completely reacting at the temperature of 450-550 DEG C in an inert atmosphere to obtain biomass pyrolytic carbon; (3) carrying out metal loading, specifically, carrying out acid pickling treatment, magnetic stirring, washing, filtering and drying on the biomass pyrolytic carbon, and then carrying out metal loading to obtain a carbon-based catalyst; and (4) carrying out catalytic reforming, specifically, carrying out catalytic reforming on the bio-oil model compound by utilizing a microwave reactor coupled carbon-based catalyst to obtain a hydrogen product. According to the invention, the bio-oil is subjected to catalytic reforming in a microwave coupling carbon-based catalyst manner, so that the reaction process is accelerated, the deactivation rate of the catalyst is reduced, and the hydrogen yield is remarkably improved.
Owner:ZHENGZHOU UNIV +1

A method for smelting manganese-ferroalloy by heating manganese ore with microwave

The present invention relates to a method for smelting a manganese-iron alloy by using microwave heating of manganese ore. According to the method, a microwave generator produces microwaves with a frequency of 2.45 GHZ, the microwaves are introduced into a reactor by using a metal waveguide, the microwave and raw materials for manganese-iron alloy smelting interact in the reactor, the raw materials for manganese-iron alloy smelting absorb microwave energy in the microwave field and the temperature is rapidly increased, an oxidation reduction reaction of manganese oxide and carbon is generated between the raw materials at a temperature of 700-1500 DEG C and is the heat absorption reaction, the microwave is continuously used to heat the reaction raw materials so as to provide heat for the reaction, the microwave field provides the promoting effect for the manganese oxide reduction reaction, and under the microwave effect, the manganese oxide is rapidly reduced so as to generate the manganese-iron alloy. Compared with the method in the prior art, the method of the present invention has the following advantages that the microwave heating is used to smelt the manganese-iron alloy, and advantages of rapid heating, short raw material heating time, energy consumption reducing and the like are provided.
Owner:UNIV OF SCI & TECH BEIJING

Ferrite wave-absorbing material with perovskite structure and preparation method of ferrite wave-absorbing material

InactiveCN113173783AFascinating VersatilityExcellent perovskite structurePerovskite (structure)Materials science
The invention provides a ferrite wave-absorbing material with a perovskite structure and a preparation method of the ferrite wave-absorbing material. The molecular formula of the ferrite wave-absorbing material with the perovskite structure is NdFe<1-x>Ni<x>O<3> (wherein x is equal to 0, 0.1, 0.2 or 0.3). The preparation method comprises the following steps: with neodymium nitrate hexahydrate, iron nitrate nonahydrate and nickel nitrate hexahydrate as raw materials, dissolving the raw materials in deionized water according to a stoichiometric ratio, adding a proper amount of citric acid monohydrate, dropwise adding ammonia water to adjust a pH value to achieve an alkaline environment, and then conducting heating and stirring in a water bath kettle to obtain uniform wet gel; and drying the prepared wet gel in an air dry oven, conducting pre-sintering to obtain a precursor, adding PVA into obtained precursor powder, conducting granulating, performing uniformly grinding, and and carrying out mould pressing to prepare a cylindrical block. The ferrite wave-absorbing material with the perovskite structure has a very good microwave absorbing effect in a microwave band of 2-18 GHz, is wide in absorbing frequency band, and has the advantages that the preparation process is simple, the preparation process is easy to regulate and control and the like.
Owner:GUILIN UNIV OF ELECTRONIC TECH

Chiral planar spiral PPy/Fe3O4 composite broadband microwave absorbent as well as preparation method and application thereof

The invention belongs to the field of microwave absorption, and discloses a chiral planar spiral PPy/Fe3O4 composite broadband microwave absorbent as well as a preparation method and application thereof. The planar spiral polypyrrole with unique morphology is prepared by taking a surfactant as a soft template and adopting a chemical oxidative polymerization reaction method, and the diameter of the planar spiral polypyrrole is 20-40 microns. By taking the material as a precursor, the compound of chiral polypyrrole and Fe3O4 is prepared from the precursor, ferric salt and other raw materials through a dissolution heat method; not only is the morphology novel and unique, but also the content and size of Fe3O4 growing on the surface of polypyrrole can be regulated and controlled by changing the concentration of iron ions in the system and the volume of the added deionized water; and the material has excellent microwave absorption characteristics. The controllable preparation process disclosed by the invention is simple, the product morphology is novel, the characteristics that the reaction conditions are harsh, the morphology of the reaction product is difficult to regulate and control, the experimental repeatability is poor and the like in the previous preparation process are overcome, and the industrial application potential is good.
Owner:ZHEJIANG NORMAL UNIVERSITY +1

A magnetic hollow micro-nano material and its preparation method and application

The invention discloses a magnetic hollow micro-nano material, a preparation method and application thereof, and belongs to the technical field of nano-materials. The invention discloses that the magnetic hollow micro-nano material prepared by a one-step liquid-phase reduction-oxidation method not only has a novel structure and formation mechanism, but also can regulate the concentration of Cu and Ni by changing the reaction temperature, time, stirring speed, gas flow, and reactant concentration. Content and composition, morphology and structure of magnetic hollow micro-nano materials, in which the diameter of micro-nanotubes is 0.1-2 μm, the length is 2-12 μm, and the wall thickness is 10-140 nm; the diameter of micro-nanospheres is 0.2-5 μm, and the wall thickness is 10~180nm. Because of the good dispersion and uniformity of the magnetic hollow micro-nano material and good microwave absorption characteristics, it is widely used in the fields of microwave absorption and shielding, electrocatalysis, lithium-ion batteries, and surface-enhanced Raman spectroscopy. In addition, the preparation method disclosed in the present invention is simple to operate, environmentally friendly, has good potential for industrial application, and is suitable for market promotion and application.
Owner:ZHEJIANG NORMAL UNIVERSITY

Preparation method and application of microwave absorbing diatom mud coating

The invention relates to a preparation method for a microwave absorption diatom ooze coating material and an application. The method comprises the following steps: mixing diatom ooze dry powder, a microwave absorbent and a dispersant according to a mass ratio of 1:1.5:(18-25), performing soaking for 10-20min, and performing electric stirring for 30-60min to obtain the microwave absorption diatom ooze coating material; and the microwave absorbent is a carbon magnetic heterostructural micro nano fiber. According to the microwave absorption diatom ooze coating material prepared from the method, when the microwave absorption diatom ooze coating material is applied, a concrete construction method comprises the following steps: scraping bottom-layer putty on cleaned wall surfaces, grinding wall surfaces until the wall surfaces are smooth, dispersing the microwave absorption diatom ooze coating material to building wall surfaces uniformly by 2-3 times, making diatom ooze patterns or performing coloring or making a press polishing layer at the treated building wall surfaces, and performing maintenance for 1-2 days to obtain the finished product. The microwave absorption diatom ooze coating material is an ideal green and environmentally-friendly building and decorative material, has excellent microwave absorbing characteristics, beautifies and decorates environments, and can avoid electromagnetic pollution and information leakage; and the microwave absorption diatom ooze coating material can be used at wall surfaces of buildings such as electromagnetic shielding darkrooms, residential power distribution rooms, military meeting rooms and secret rooms, television towers, broadcasting rooms, radars, and satellite communication launching pads.
Owner:ZHEJIANG NORMAL UNIVERSITY
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