Inorganic dielectric powder for composite dielectric material and composite dielectric material
A dielectric material and dielectric technology, applied in fixed capacitor dielectrics, inorganic chemistry, inorganic insulators, etc., can solve the problems of difficult secondary processing, filling problems, coarse particles, etc.
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Embodiment 1
[0077] 44.1 g of a 0.5 mol / kg niobium ethoxide solution (toluene solvent) was added to 750 g of titanium butoxide (titan butoxide), and stirred to prepare a complex metal alkoxide additive solution. Put 2500g of water in a 10L reaction vessel, slowly add the complex metal alkoxide solution dropwise while stirring to carry out hydrolysis. 975 g of barium hydroxide octahydrate was added to 3000 g of water, dissolved at 80° C., and this aqueous solution was added dropwise to the suspension obtained here. Heat the container, adjust the heating rate to 10°C per hour, raise the temperature to 90°C, and keep it at 90°C for 1 hour, then stop heating and stirring, and then cool down. A Buchner funnel was installed on the filter bottle, and solid-liquid separation was performed while suctioning with an aspirator. In order to make the obtained synthetic powder have a barium-rich composition, while washing with an aqueous solution added with acetic acid, adjust the molar ratio of barium ...
Embodiment 2
[0081] Put 2500g of water in a 10L reaction vessel, add 2.6g of ammonium vanadate and stir to obtain a solution. While stirring this solution, 750 g of titanium butoxide (titan butoxide) was slowly added dropwise for hydrolysis. 975 g of barium hydroxide octahydrate was added to 3000 g of water, dissolved at 80° C., and this aqueous solution was added dropwise to the suspension obtained here. Heat the container, adjust the heating rate to 10°C per hour, raise the temperature to 90°C, and keep it at 90°C for 1 hour, then stop heating and stirring, and then cool down. A Buchner funnel was installed on the filter bottle, and solid-liquid separation was performed while suctioning with an aspirator. In order to make the obtained synthetic powder have a barium-rich composition, while washing with an aqueous solution added with acetic acid, adjust the molar ratio of barium to titanium to 1.000 to 0.005, then carry out solid-liquid separation, and dry the obtained filter cake at 120°...
Embodiment 3
[0085] 1000 g of water was put into a 10 L reaction vessel, and 9 g of calcium chloride dihydrate was added to obtain a solution. A mixed solution of 715 g of titanium butoxide and 175 g of zirconium butoxide was slowly added dropwise thereto for hydrolysis. 1250 g of barium hydroxide octahydrate was added to 2500 g of water, dissolved at 80° C., and this aqueous solution was added dropwise to the suspension obtained here. Heat the container, adjust the heating rate to 30°C per hour, raise the temperature to 90°C, and keep the temperature at 90°C for 1 hour, then stop heating and stirring, and then cool down. A Buchner funnel was installed on the filter bottle, and solid-liquid separation was performed while suctioning with an aspirator. In order to make the obtained synthetic powder have a barium-rich composition, while washing with an aqueous solution added with acetic acid, adjust the ratio of the total moles of barium and calcium to the total moles of titanium and zirconi...
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