Preparation method of ozone heterogeneous oxidized solid catalyst
A heterogeneous oxidation and solid catalyst technology, applied in the direction of catalyst activation/preparation, physical/chemical process catalysts, chemical instruments and methods, etc., can solve the problems of poor toxicity resistance, low catalyst adsorption, easy loss of catalytic activity, etc. Achieve strong adsorption, inhibit smelting out, improve anti-toxicity and catalytic activity
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Embodiment 1
[0007] Embodiment 1:1.35g lithium hypochlorite, 1.65g bis(acetylacetonate) beryllium, 140ml deionized water, join volume and be that in the sealable reactor of 500ml, stir and mix evenly, the weight concentration of this aqueous solution is 2.1%, times Lithium chlorate: bis(acetylacetonate) beryllium weight ratio = 1:1.2; add deionized water to wash to neutral, dry at 103°C to remove moisture, and then sieve 2.75g wheat rice of -200 mesh to +400 mesh standard sieve Weight of limestone, 3.75g wollastonite, 4.75g dolomite, 5.75g calcite, 6.75g fly ash, 7.75g coal gangue, lithium hypochlorite and bis(acetylacetonate) beryllium (3g): weight of multi-material ( 31.5g) = 1:10.5, heat up to 36°C, continue stirring for 3.2h, filter, dry at 103°C and obtain 31g of pore-enlarging modified carrier; put 31g of pore-enlarging modified carrier into a 500ml ultrasonic reactor, Then add 3.25g tetradecyltributylammonium chloride dissolved in 100ml deionized water solution, the weight concentra...
Embodiment 2
[0008] Embodiment 2:0.24g lithium hypochlorite, 0.36g bis(acetylacetonate) beryllium, 10ml deionized water, join volume and be that in the sealable reactor of 100ml, stir and mix evenly, the weight concentration of this aqueous solution is 5.7%, times Lithium chlorate: bis(acetylacetonate) beryllium weight ratio = 1:1.5; add deionized water to wash to neutral, dry at 103°C to remove moisture, and then sieve 1.45g wheat rice of -200 mesh to +400 mesh standard sieve Weight of limestone, 1.65g wollastonite, 1.85g dolomite, 2.05g calcite, 2.25g fly ash, 2.45g coal gangue, lithium hypochlorite and bis(acetylacetonate) beryllium (0.6g): weight of porous material (11.7g)=1:19.5, heat up to 48°C, continue to stir for 5.8h, filter, dry at 105°C and obtain 11.5g of pore-enlarging modified carrier; in a 100ml ultrasonic reactor, put the pore-enlarging modified carrier 11.5g, then add 2.2g tetradecyltributylammonium chloride and be dissolved in the aqueous solution of 26ml deionized water...
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