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370 results about "Lithium hypochlorite" patented technology

Lithium hypochlorite is the colorless, crystalline lithium salt of hypochlorous acid with the chemical formula of LiClO. It is used as a disinfectant for pools and a reagent for some chemical reactions.

Dual layer tablet, method of making and use thereof

A method for treating a recirculating water system which comprises introducing into said water system a multifunctional, multilayer tablet, wherein the multilayer tablet comprises a fast dissolving layer and a slow dissolving layer, wherein said fast dissolving layer releases a combination of active ingredients including a member selected from the group consisting of lithium hypochlorite, calcium hypochlorite, trichloroisocyanuric acid (TCCA), anhydrous sodium dichloroisocyanurate, sodium persulfate, potassium persulfate, potassium monopersulfate, sodium monopersulfate, and mixtures thereof, and at least one of a clarifier, chelating agent, sequesterant, algaestat, water softener, algaecide, corrosion inhibitor, scale inhibitor, flocculent, disintegrant, dispersant, colorant, dissolution control agent, fragrance, or surfactant and, wherein said slow dissolving layer includes a member selected from the group consisting of trichloroisocyanuric acid (TCCA), calcium hypochlorite, 1,3-dichloro-5,5-dimethylhydantoin (DCDMH), 1,3-dibromo-5,5-dimethylhydantoin (DBDMH), 1-bromo-3-chloro-5,5-dimethylhydantoin (BCDMH), 1,3-dichloro-5-ethyl-5-methylhydantoin (DCEMH), 1,3-dibromo-5-ethyl-5-methylhydantoin (DBEMH), 1-bromo-3-chloro-5-methyl-5-ethylhydantoin (BCEMH), and mixtures thereof, and at least one of a clarifier, chelating agent, sequesterant, algaestat, water softener, algaecide, corrosion inhibitor, scale inhibitor, flocculent, disintegrant, dispersant, colorant, dissolution control agent or surfactant.
Owner:BIO LAB

Dual layer tablet, method of making and use thereof

A method for treating a recirculating water system which comprises introducing into said water system a multifunctional, multilayer tablet, wherein the multilayer tablet comprises a fast dissolving layer and a slow dissolving layer, wherein said fast dissolving layer releases a combination of active ingredients including a member selected from the group consisting of lithium hypochlorite, calcium hypochlorite, trichloroisocyanuric acid (TCCA), anhydrous sodium dichloroisocyanurate, sodium persulfate, potassium persulfate, potassium monopersulfate, sodium monopersulfate, and mixtures thereof, and at least one of a clarifier, chelating agent, sequesterant, algaestat, water softener, algaecide, corrosion inhibitor, scale inhibitor, flocculent, disintegrant, dispersant, colorant, dissolution control agent, fragrance, or surfactant and, wherein said slow dissolving layer includes a member selected from the group consisting of trichloroisocyanuric acid (TCCA), calcium hypochlorite, 1,3-dichloro-5,5-dimethylhydantoin (DCDMH), 1,3-dibromo-5,5-dimethylhydantoin (DBDMH), 1-bromo-3-chloro-5,5-dimethylhydantoin (BCDMH), 1,3-dichloro-5-ethyl-5-methylhydantoin (DCEMH), 1,3-dibromo-5-ethyl-5-methylhydantoin (DBEMH), 1-bromo-3-chloro-5-methyl-5-ethylhydantoin (BCEMH), and mixtures thereof, and at least one of a clarifier, chelating agent, sequesterant, algaestat, water softener, algaecide, corrosion inhibitor, scale inhibitor, flocculent, disintegrant, dispersant, colorant, dissolution control agent or surfactant.
Owner:BIO LAB

Preparation method of ozone heterogeneous oxidation solid catalyst

The invention relates to a preparation method of a solid catalyst for ozone heterogeneous oxidation, which belongs to the technical fields of environmental protection and chemical catalysts. The preparation method is to use attapulgite, diopside, talc, crystal soda, aluminum hydroxide and lapis lazuli porous materials as carriers, and after the carrier is modified by lithium hypochlorite and bis(acetylacetonate) beryllium to expand pores, add The surface active agent trioctylmethyl ammonium chloride is subjected to surface activation treatment under the action of ultrasonic waves, and then the ultrasonic surface activation carrier is mixed with the composite mineralizer borax and potassium sulfate in a hydrothermal reaction kettle, and the catalytic activity auxiliary agent precursor three (3 ‑Trifluoroacetyl‑D‑camphor) praseodymium (III), promethium tricyclopentadienyl, terbium triacetate hydrate, holmium oxalate decahydrate rare earth organometallic compound, catalytic active center component precursor common transition metal organic compound fuma Iron ferrous acid, nickel citrate and noble metal compound silver dithiocyanate (I) potassium, terpyridyl ruthenium chloride hexahydrate, hydrothermal under the action of emulsifier trimethylaminoethanol stearate ammonium iodide After the reaction, the reaction product is dried to remove moisture, and burned at a certain temperature in a muffle furnace to obtain a solid catalyst for ozone heterogeneous oxidation.
Owner:SICHUAN NORMAL UNIVERSITY

Preparation method of lithium hypochlorite

The invention relates to a preparation method of lithium hypochlorite. The preparation method of lithium hypochlorite includes the following steps: S1, chlorine is introduced into alkali metal hydroxide solution to react to form a first solution, wherein the molar ratio of chlorine to alkali metal hydroxide is not less than 20:1; S2, the first solution is distilled; the distillate is condensed atthe temperature of between -5 and 10 DEG C to obtain hypochlorous acid solution with the concentration of hypochlorous acid not less than 35wt%; S3, the prepared hypochlorous acid solution is mixed with the prepared lithium hydroxide suspension at the temperature of between 0 and 20 DEG C to react to obtain a lithium hypochlorite mixed solution; S4, the lithium hypochlorite mixed solution is evaporated and crystallized under the vacuum state and at the temperature of between 30 and 60 DEG C; the lithium hypochlorite crystal and the mother liquid are separated; the lithium hypochlorite crystalis dried to obtain the lithium hypochlorite. By the method, the concentration of various impurities can be reduced to a maximum extent, the purity and the yield of the product are improved, the production cost is reduced, the production process is simplified, and the method is an environment-friendly and economical preparation method of lithium hypochlorite.
Owner:FIRST RARE MATERIALS CO LTD

Preparation method for solid catalyst for ozone heterogeneous oxidization

The invention relates to a preparation method for a solid catalyst for ozone heterogeneous oxidization and belongs to the technical field of an environment-friendly and chemical catalyst. The preparation method comprises the following steps: taking a perlite, albite, montmorillonite, sylvine, illite and ulexite porous material as a carrier; modifying the carrier by broaching with lithium hypochlorite and bis(acetylacetone) beryllium, and then adding surfactant nonylphenol diquaternary ammonium salt and performing surface activating treatment under the effect of ultrasonic wave; performing hydrothermal reaction on an ultrasonic surface activated carrier, a compound mineralizer including borax and potassium sulphate, catalytic activated assistant precursors, including 1,1,1-trifluoroacetylacetone neodymium, terbium acetate hydrate, holmium oxalate hydrate and tri[N,N-bi(trimethyl silyl)amide] erbium rare-earth metal organic compound and catalytic active core component precursors, including common transition metal organic compound cobalt gluconate, nickel citrate, ammonium zirconium carbonate and precious metal chemical complex tetraammine dichloropalladium in a hydrothermal reaction kettle under the effect of octadecyl dimethyl hydroxypropyl ammonium chloride used as an emulsifier; drying and dewatering the reaction product; burning in a muffle furnace under a certain temperature, thereby acquiring the solid catalyst for ozone heterogeneous oxidization.
Owner:SICHUAN NORMAL UNIVERSITY

Preparation method of ozone heterogeneous oxidation solid catalyst

The invention relates to a preparation method of an ozone heterogeneous oxidation solid catalyst, and belongs to the technical field of environmental protection and chemical catalysts. The preparation method comprises the steps of taking activated carbon, carnallite, potassium feldspar, szaibelyite, pulverized fuel ash and a coal gangue porous mineral material as carriers; after bearizing and modifying the carriers through lithium hypochlorite and bis(acetylacetone) beryllium, adding a surface active agent dimethyl hexadecyl ethyl ammonium ethyl sulfate for carrying out surface activation treatment under an ultrasonic action; then carrying out hydrothermal reaction on the ultrasonic surface activated carriers, a compound mineralizing agent prepared from borax and potassium sulphate, samarium acetylacetonate, tri(4,4,4-trifluoro-1-(2-thiophene)-1,3-butanedione) europium, holmium oxalate decahydrate, thulium trifluoromethane sulfonate (III) rare-earth metal compound catalytic active auxiliary, cobalt gluconate, L-aspartic acid molybdenum, potassium dicyanoargentate (I) and a terpyridyl ruthenium chloride hexahydrate transition metal catalytic activity center component in a hydrothermal reaction kettle under the action of an emulgator hexadecyl dimethylamine ethyl sulfate; drying a reaction product to remove moisture, and firing in a muffle furnace at a certain temperature to obtain the ozone heterogeneous oxidation solid catalyst.
Owner:SICHUAN NORMAL UNIVERSITY

Preparation method of ozone heterogeneous oxidation solid catalyst

The invention relates to a preparation method of a solid catalyst for ozone heterogeneous oxidation, which belongs to the technical fields of environmental protection and chemical catalysts. The preparation method is to use attapulgite, diopside, montmorillonite, sylvite, amazonite and lithium limestone porous materials as carriers, and after the carrier is modified by lithium hypochlorite and bis(acetylacetonate) beryllium to expand pores, Add surfactant dioctadecylmethyl-2-hydroxyethylammonium chloride to carry out surface activation treatment under the action of ultrasonic waves, then ultrasonic surface activation carrier is mixed with composite mineralizer borax and potassium sulfate in a hydrothermal reaction kettle, Precursors of catalytic activity promoter tris(3-trifluoroacetyl-D-camphor) praseodymium(III), 1,1,1-trifluoroacetylacetonate neodymium, tris(6,6,7,7,8,8, 8‑heptafluoro‑2,2‑dimethyl‑3,5‑octenedione) Dysprosium (III), holmium oxalate decahydrate rare earth metal organic compound, catalytic active center component precursor common transition metal organic compound fuma Iron ferrous acid, nickel citrate, copper glutamate and precious metal compound potassium gold tetrachloride are subjected to hydrothermal reaction under the action of emulsifier dimethylaminoethanol palmitate ammonium chloroacetate. In the muffle furnace, burn at a certain temperature to obtain a solid catalyst for ozone heterogeneous oxidation.
Owner:SICHUAN NORMAL UNIVERSITY

Ozone heterogeneous oxidation solid catalyst preparation method

The invention relates to a preparation method of a solid catalyst for ozone heterogeneous oxidation, which belongs to the technical fields of environmental protection and chemical catalysts. The preparation method is to use γ-alumina, barite, activated carbon, carnallite, dolomite and calcite porous materials as carriers, and after the carrier is modified by lithium hypochlorite and bis(acetylacetonate) beryllium to expand pores, add surface active The agent ditetradecyldimethyl ammonium chloride is subjected to surface activation treatment under the action of ultrasonic waves, and then the ultrasonic surface activation carrier is combined with the composite mineralizer borax and potassium sulfate in a hydrothermal reaction kettle, and the catalytic activity auxiliary agent precursor four ( 2,2,6,6-tetramethyl-3,5-heptanedionate)cerium(IV), tris(3-trifluoroacetyl-D-camphor)praseodymium(III), thulium trifluoromethanesulfonate (III), Tris(trifluoromethanesulfonylimide) ytterbium rare earth metal organic compound, catalytic active center component precursor common transition metal organic compound lysine manganese, copper glutamate and noble metal compound silver dithiocyanate (1) Potassium acid, trisodium hexanitroso rhodium, carry out hydrothermal reaction under the effect of emulsifier 2,6-bis(diethylaminomethyl)-4-nonylphenol-epichlorohydrin quaternary ammonium salt, After the reaction product is dried to remove moisture, it is burned in a muffle furnace at a certain temperature to obtain a solid catalyst for ozone heterogeneous oxidation.
Owner:SICHUAN NORMAL UNIVERSITY

Method for preparing ozone heterogeneous phase oxidized solid catalyst

The invention relates to a preparation method of a solid catalyst for ozone heterogeneous oxidation, which belongs to the technical fields of environmental protection and chemical catalysts. The preparation method is to use diatomite, kyanite, brucite, serpentine, aluminum hydroxide and lapis lazuli porous materials as carriers, and the carrier is modified by lithium hypochlorite and bis(acetylacetonate) beryllium. , adding the surfactant lauryl dimethyl hydroxyethyl ammonium chloride to carry out surface activation treatment under the action of ultrasonic waves, and then the ultrasonic surface activation carrier is mixed with the composite mineralizer borax and potassium sulfate in the hydrothermal reaction kettle, the catalytic activity Auxiliary precursor tris (hexafluoroacetylacetonate) yttrium (III) dihydrate, tricyclopentadiene promethium, holmium oxalate decahydrate, tris (trifluoromethanesulfonimide) ytterbium rare earth metal organic compound, catalytic active center Component precursors Common transition metal organic compound pyruvate isonicotinoyl hydrazone vanadium, cobalt gluconate and noble metal compound dichloro tetraammine palladium, tetrachloro iridium dihydrate, in emulsifier dioctadecyl dimethyl ammonium bromide The hydrothermal reaction is carried out under the action, and the reaction product is dried to remove moisture, and then burned at a certain temperature in a muffle furnace to obtain a solid catalyst for ozone heterogeneous oxidation.
Owner:SICHUAN NORMAL UNIVERSITY

Preparation method of ozone heterogeneous oxidation solid catalyst

The invention relates to a preparation method of an ozone heterogeneous oxidation solid catalyst and belongs to the technical field of environment protection and chemical catalysts. The preparation method includes: using a diatom purifier, kyanite, aluminum hydroxide, celestite, fly ash and coal gangue as the carriers, using lithium hypochlorite and bis(acetylacetone) beryllium to perform pore expansion on the carriers, adding chlorinated dodecyl dimethyl hydroxyethyl ammonium to activate the carriers under ultrasonic action, allowing the carriers to have hydrothermal reaction with compound mineralizer including borax and potassium sulfate, catalytic activity promoter precursors including tri(hexafluoroacetylacetone) yttrium(III) dihydrate, acetylacetone samarium, tri(4, 4, 4-trifluoro-1-(2-thiophene)-1, 3-butanedione) europium and tri(6, 6, 7, 7, 8, 8, 8-heptafluoro-2, 2-dimethyl-3, 5-octene diketone) dysprosium(III), and catalytic activity central precursors including pyruvic acid isonicotinoyl hydrazone vanadium, nickel citrate, cupric glutamate and dipotassium hexachloroosmate in a hydrothermal reaction kettle under the effect of N-dodecyl dimethyl-N'-dodecyl-dimethyl-2-hydroxypropyl ammonium dichloride, drying to remove moisture, and burning in a muffle furnace to obtain the ozone heterogeneous oxidation solid catalyst.
Owner:SICHUAN NORMAL UNIVERSITY

Preparation method of ozone heterogeneous oxidation solid catalyst

The invention relates to a preparation method of a solid catalyst for ozone heterogeneous oxidation, which belongs to the technical fields of environmental protection and chemical catalysts. Use medical stone, wollastonite, dolomite, calcite, sodium saltpeter and dolomite as the carrier, expand the pores with lithium hypochlorite and bis(acetylacetonate) beryllium, add surfactant tetradecyltributylammonium chloride The activation treatment is carried out under the action of ultrasonic waves, and then the carrier is mixed with the composite mineralizer borax and potassium sulfate in a hydrothermal reactor, and the precursors of the catalytic activity auxiliary agent scandium(III) isopropoxide, tri(4,4,4-trifluoro ‑1‑(2‑thiophene)‑1,3‑butanedione) europium, thulium(III) trifluoromethanesulfonate, lutetium carbonate hydrate, catalytic active center precursor titanocene ring-substituted salicylic acid complex, Zinc lactate, catechol ethylenediamine tungsten complex and iridium tetrachloride dihydrate are subjected to hydrothermal reaction under the action of emulsifier dimethyl hexadecylethyl ammonium ethyl sulfate, dried to remove moisture and then dried in horse Ignition in a Furnace to obtain a solid catalyst for ozone heterogeneous oxidation.
Owner:SICHUAN NORMAL UNIVERSITY

Method for preparing ozone heterogeneous oxidation solid catalysts

The invention relates to a preparation method of a solid catalyst for ozone heterogeneous oxidation, which belongs to the technical fields of environmental protection and chemical catalysts. The preparation method is to use attapulgite, diopside, sepiolite, feldspar, perlite and albite porous materials as carriers, and the carrier is modified by lithium hypochlorite and bis(acetylacetonate) beryllium for pore expansion. , adding the surfactant dieicosyldimethylammonium chloride to carry out surface activation treatment under the action of ultrasonic waves, and then the ultrasonic surface activation carrier is mixed with the composite mineralizer borax and potassium sulfate in the hydrothermal reaction kettle, and the catalytic activity assistant Precursors tetrakis(2,2,6,6-tetramethyl-3,5-heptanedionate)cerium(IV), tris(4,4,4-trifluoro-1-(2-thiophene)-1 ,3-butanedione) europium, tris(6,6,7,7,8,8,8-heptafluoro-2,2-dimethyl-3,5-octenedione) dysprosium(III), Tris[N,N-bis(trimethylsilane)amine]erbium rare earth organometallic compound, catalytic active center component precursor common transition metal organic compound manganese lysine, ammonium zirconium carbonate and noble metal compound palladium dichlorotetraammine , iridium tetrachloride dihydrate, under the action of emulsifier m-nitrobenzyl dimethyl ammonium bromide, carry out hydrothermal reaction, after the reaction product is dried to remove moisture, it is burned in a muffle furnace at a certain temperature to obtain ozone Homogeneous oxidation of solid catalysts.
Owner:SICHUAN NORMAL UNIVERSITY

Ozone heterogeneous oxidation solid catalyst preparation method

InactiveCN107051476ACarbonization strengthens microporous structureCarbonization strengthens the microporous structure by hydrothermal reactionCatalyst carriersWater contaminantsUltrasound - actionRare earth metal compounds
The invention belongs to the technical field of environment protection and chemical catalysts and relates to an ozone heterogeneous oxidation solid catalyst preparation method. The preparation method includes: taking porous mineral materials including activated carbon, carnallite, potassium feldspar, camsellite, illite and ulexite as carriers; subjecting the carriers to lithium hypochlorite and bis(acetylacetone)beryllium broaching modification; adding surfactant methacryloyloxyethyltrimethyl ammonium chloride for surface activation under the action of ultrasonic waves; subjecting the carriers subjected to ultrasonic surface activation to hydrothermal reaction, with a complex mineralizer composed of borax and potassium sulfate, catalytic activity auxiliary agents including samarium acetylacetonate, tri(4,4,4-trifuloro-1-(2-thiophene)-1,3-butanedione)europium, terbium acetate hydrate and tris[N,N-bis(trimethylsilane)amine]erbium rare earth metal compounds and catalytic activity central components including cobalt gluconate, L-aspartic acid molybdenum, ammonium zirconium carbonate, cis-dichlorodiamineplatinum transition metals, in a hydrothermal reactor under the action of stearamidopropyl dimethylamine lactate serving as an emulsifying agent; drying reaction products to remove moisture, and firing in a muffle furnace at a certain temperature to obtain an ozone heterogeneous oxidation solid catalyst.
Owner:SICHUAN NORMAL UNIVERSITY

Preparation method for solid catalyst for ozone heterogeneous oxidization

The invention relates to a preparation method for a solid catalyst for ozone heterogeneous oxidization and belongs to the technical field of an environment-friendly and chemical catalyst. The preparation method comprises the following steps: by taking medical stone, wollastonite, activated carbon, carnallite, coal ash and gangue as carriers, modifying the carrier by broaching with lithium hypochlorite and bis(acetylacetone) beryllium, and then adding a surfactant, tetradecyl tributyl ammonium chloride, and performing surface activating treatment under the effect of ultrasonic wave; performing hydrothermal reaction on the carriers, compound mineralizers including borax and potassium sulphate, catalytic activated assistant precursors including isopropoxy scandium (III), tri(4,4,4-trifluoro-1-(2-thiophene)-1,3-butanedione) europium, terbium acetate hydrate and lutetium carbonate hydrate, and catalytic active core component precursors including dicyclopentadienyl titanium substituted salicylic acid complex, zinc lactate, ammonium zirconium carbonate and precious metal chemical complex potassium dicyanoargentate in a hydrothermal reaction kettle under the effect of tri-hexadecyl methyl-ammonium chloride used as an emulsifier; drying and dewatering the reaction product; burning in a muffle furnace under a certain temperature, thereby acquiring the solid catalyst for ozone heterogeneous oxidization.
Owner:SICHUAN NORMAL UNIVERSITY
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