Wheat protein regenerated cellulose fiber and preparation method thereof
A technology for regenerating cellulose and wheat protein, applied in the direction of cellulose/protein conjugated rayon, etc., can solve the problems affecting the quality of protein fibers, poor comfort of protein fibers, destroying protein structure, etc., and achieve textile processing and wear performance. Better, avoid a lot of loss, the effect of short process flow
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Embodiment 1
[0035] A kind of preparation method of wheat protein regenerated cellulose fiber of the present embodiment, comprises the steps:
[0036] (1) Wheat protein powder with a particle size of 1 μm is added to a mixed aqueous solution of sodium dodecylbenzenesulfonate and sodium polyethylene glycol alkylaryl ether sulfonate, wherein sodium dodecylbenzenesulfonate The mass ratio with polyethylene glycol alkyl aryl ether sulfonate sodium is 1.5:1, the mass of sodium dodecylbenzene sulfonate and polyethylene glycol alkyl aryl ether sulfonate total mass and wheat protein powder The ratio is 1:100, put the above mixed solution into the blending barrel, the blending barrel is an adjustable agitator with a cycloid pinwheel, the stirring blade is a spiral stirring blade, stir up and down, and the stirring rate is 100 rpm. Stir for 60 minutes at a temperature of 30°C to quickly disperse the protein powder in the solution, and filter through a plate and frame filter to obtain a dispersion of ...
Embodiment 2
[0046] A kind of preparation method of wheat protein regenerated cellulose fiber of the present embodiment, comprises the steps:
[0047] (1) Wheat protein powder with a particle size of 1.5 μm is added to a mixed aqueous solution of sodium dodecylbenzenesulfonate and sodium polyethylene glycol alkylaryl ether sulfonate, wherein dodecylbenzenesulfonic acid The mass ratio of sodium and polyethylene glycol alkyl aryl ether sulfonate sodium is 2:1, the total mass of sodium dodecylbenzene sulfonate and polyethylene glycol alkyl aryl ether sulfonate and wheat protein powder The mass ratio is 1:75, put the above mixed solution into the blending barrel, the blending barrel is an adjustable agitator with a cycloid pinwheel, the stirring blade is a spiral stirring blade, stir up and down, the stirring rate is 150 rpm, Stir at a temperature of 30°C for 60 minutes to quickly disperse the protein powder in the solution, and filter through a plate and frame filter to obtain a dispersion of...
Embodiment 3
[0057] A kind of preparation method of wheat protein regenerated cellulose fiber of the present embodiment, comprises the steps:
[0058] (1) Wheat protein powder with a particle size of 2 μm is added to a mixed aqueous solution of sodium dodecylbenzenesulfonate and sodium polyethylene glycol alkylaryl ether sulfonate, wherein sodium dodecylbenzenesulfonate The mass ratio with polyethylene glycol alkyl aryl ether sulfonate sodium is 2.5:1, the mass of sodium dodecylbenzene sulfonate and polyethylene glycol alkyl aryl ether sulfonate total mass and wheat protein powder The ratio is 1:50, put the above mixed solution into the blending barrel, the blending barrel is an adjustable agitator with a cycloid pinwheel, the stirring blade is a spiral stirring blade, stir up and down, and the stirring speed is 200 rpm, at Stir for 60 minutes at a temperature of 30°C to quickly disperse the protein powder in the solution, and filter through a plate and frame filter to obtain a dispersion ...
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