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Preparation method of ultrathin adiabatic and insulated flexible non-woven fabrics resistant to 1000 degrees

A non-woven fabric and thermal insulation technology, which is applied in the direction of non-woven fabrics, textiles, papermaking, fiber types, etc., can solve the problems of continuous production, long-term use, and burnt supports

Active Publication Date: 2020-06-26
苏州格威姆新材料科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Insulation materials, such as alkali-free glass fiber products, have a softening point of 600°C and cannot be used for a long time at a high temperature of 1000°C; carbon fiber products can withstand temperatures up to 1000°C, but cannot be used in environments with power discharge; aramid products, para-aramid Lun 1414 has a temperature resistance of 500°C and cannot be used at a high temperature of 1000°C for a long time, and the price is relatively expensive; rock wool products have a thermal conductivity of about 0.03W / (m k) at room temperature and have good thermal insulation, but they are too thick for thermal insulation protection It takes too much space to be used in the field of small mobile devices, and its weather resistance is not good. It needs partial replacement after two years of use in daily environment
[0004] The heat insulation function can also be realized by the heat insulation coating. The best heat insulation coating can withstand high temperature of 1000°C, but once the heat insulation coating is burned through, the underlying support will be burned quickly, and it can only be sprayed on the support when used. On the body, the coating can be firmly combined with the support after 6 to 8 hours of natural curing, and the process time is too long to continue production

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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  • Preparation method of ultrathin adiabatic and insulated flexible non-woven fabrics resistant to 1000 degrees
  • Preparation method of ultrathin adiabatic and insulated flexible non-woven fabrics resistant to 1000 degrees
  • Preparation method of ultrathin adiabatic and insulated flexible non-woven fabrics resistant to 1000 degrees

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Experimental program
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Effect test

Embodiment 1

[0035] A preparation method of ultra-thin 1000°C heat-insulating flexible non-woven fabric, comprising the following steps,

[0036] S1) The non-metallic crystal minerals are melted and purified at a high temperature of 1500 ° C, and rare metal zirconium compounds (mass concentration 1.0%) and metal lithium compounds (mass concentration 0.3%) are added, and the diameter is 7 μm and the length is 4 mm. Grade glass fiber, which can be formed into high temperature resistant fiber;

[0037] S2) combing the high temperature resistant fiber into a thin cotton web with a uniform thickness of 2 mm by physical opening;

[0038] S3) Apply the solvent-resistant glue stock solution on the thin cotton net by the gravure transfer coating method. The solvent-resistant glue stock solution is compounded by water-based epoxy-modified polyurethane resin and soft water. The mass solubility of the two is 50% and 50% respectively. The amount of glue is 6%. After high temperature reaction, the orig...

Embodiment 2

[0042] A preparation method of ultra-thin 1000°C heat-insulating flexible non-woven fabric, comprising the following steps,

[0043] S1) The non-metallic crystal minerals are melted and purified at a high temperature of 1500°C, and rare metal titanium compounds (mass concentration 0.5%) and metal molybdenum compounds (mass concentration 0.3%) are added, and the fiber diameter is 11 μm and the length is 6 mm. Basalt fiber can be formed into high temperature resistant fiber;

[0044] S2) combing the high temperature resistant fiber into a thin cotton web with a uniform thickness of 5mm by physical opening;

[0045] S3) Apply the solvent-resistant glue stock solution on the thin cotton net by flat padding method. The solvent-resistant glue stock solution is compounded by water-based butadiene rubber, water-based silicone rubber and soft water. The mass solubility of the three is respectively 10%, 25% and 65%, the sizing amount is 10%, the glue stock solution is polymerized into ...

Embodiment 3

[0049] A preparation method of ultra-thin 1000°C heat-insulating flexible non-woven fabric, comprising the following steps,

[0050] S1) The non-metallic crystal minerals are melted and purified at a high temperature of 1500°C, and rare metal zirconium compounds (mass concentration 1.0%) and metal lithium compounds (mass concentration 0.3%) are added, and the S grade with a diameter of 7 μm and a length of 4 mm is produced by centrifugal spinning method Glass fibers and silica fibers with a diameter of 9 μm and a length of 6 mm are mixed to form a high-temperature-resistant fiber composite material according to the fiber weight ratio of 50% and 50%;

[0051] S2) Carding the high temperature resistant fiber composite material into a thin cotton web with a uniform thickness of 3 mm by physical opening;

[0052] S3) The solvent-resistant glue stock solution is applied on the thin cotton net by vacuum suction method, and the solvent-resistant glue stock solution is compounded by w...

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Abstract

The invention discloses a preparation method of ultrathin adiabatic and insulated flexible non-woven fabrics resistant to 1000 degrees. The method comprises the following steps of S1) melting and purifying nonmetallic crystal mineral, and adding rare metal compounds to prepare high-temperature resistant fiber; S2) opening to card the high-temperature resistance fiber into thin webs with uniform thickness; S3) applying solvent resistance stock glue solution on the thin webs for drying and dehydration to prepare solvent resistance high-temperature resistant porous cotton, and preparing high-temperature resistance fiber non-woven rolls; S4) uniformly dispersing adiabatic powder in a 100% alcohols solvent to form a mixed solution, and soaking the high-temperature resistance fiber non-woven rolls in the mixed solution in a vacuum mixing kettle for reverse reduction reaction; and S5) recovering the residual alcohols solvent after reaction by using low-temperature vacuum centrifugation to prepare the finished non-woven fabrics. The non-woven fabrics prepared by the invention are ultrathin, ultra-light, resistant to 1000 degrees, adiabatic and resistant to alcohols solvents with 100% concentration, have excellent dry and wet strength, and are capable of maintaining complete structure, electrical insulation and explosion protection.

Description

technical field [0001] The invention relates to the technical field of functional non-woven fabrics, in particular to a preparation method of an ultra-thin flexible non-woven fabric resistant to heat insulation at 1000°C. Background technique [0002] Thermal insulation material refers to the material that can block the transfer of heat flow, also known as thermal insulation material. Traditional thermal insulation materials, such as glass fiber, polyurethane foam, rock wool, silicate, etc.; new thermal insulation materials, such as airgel felt, vacuum panels, etc., which are used for building envelope or thermal equipment to resist heat flow transfer A material or a composite of materials includes both heat insulating materials and cold insulating materials. On the one hand, thermal insulation materials satisfy the heat storage environment of building space or thermal equipment, and on the other hand, they also play a key role in the thermal management and safety protectio...

Claims

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Application Information

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IPC IPC(8): D06M11/46D04H1/64D04H1/4382D04H1/4209D04H1/4218
CPCD06M11/46D04H1/64D04H1/4382D04H1/4209D04H1/4218D06M2200/00
Inventor 倪洁
Owner 苏州格威姆新材料科技有限公司
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