The invention discloses a method for preparing dilute
nitric acid,
sponge tin and polymeric aluminum through spent
tin-
fading liquid. The method comprises the steps that 1, the spent
tin-
fading liquid is heated through a steam spacer bush, and cycled feeding and reduced pressure
distillation are carried out to obtain dilute
nitric acid and tin slime; 2, water is added into the tin slime, a flocculant solution is added, stirring is carried out, and supernate and lower-layer tin slime are recycled; 3, the tin slime is collected, the step 2 is repeatedly executed to obtain lower-layer tin slime A; the supernate in the step 2 and supernate in the step 3 are mixed to obtain supernate B; 4, the supernate B is placed in an electrolytic bath for
electrolysis and recycling of
copper, and
electrolysis tail liquid can be used as a dilute
nitric acid product through concentration and enrichment; 5, concentrated
hydrochloric acid is added into the low-layer tin slime A, and stirring and dissolving are carried out to obtain a solution C; 6, water is added into the solution C, an aluminum sheet is placed in, the prepared flocculant solution is added, filtering is carried out, and the
sponge tin and the polymeric aluminum are obtained. The
processing technology is easy to implement, no secondary
solid waste is produced, the dilute nitric acid, the
sponge tin and the polymeric
aluminum can be obtained at the same time, and
economic benefits are good.