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107results about How to "Avoid demulsification" patented technology

Emulsified acrylic acid modified asphalt cement group waterproof coating material and method for producing the same

The invention relates to an acrylic acid modified asphalt cement-based and water-proof coating and a preparation method. The emulsified acrylic acid modified asphalt cement-based and water-proof coating consists of component A and component B; wherein, the mixture ratio of the component A to the component B is from 1 : 0.5 to 1.5 (in weight); wherein, the raw materials of component A and the weight percentage thereof are respectively as follows: acrylic emulsion or amphetamine emulsion accounting for 40 to 70 percent, emulsified asphalt accounting for 10 to 50 percent, filler accounting for 8 to 20 percent, accessory ingredient accounting for 0.1 to 3 percent and water accounting for 1 to 19.0 percent; the raw materials of component B and the weight percentage thereof are as follows respectively: cement accounting for 70 to 100 percent and filler accounting for 0 to 30 percent. The acrylic acid modified asphalt cement-based and water-proof coating has the advantages of strong binding power with the base, high tensile strength, large unit extension, low cost and environment protection.
Owner:WUHAN YANGGUANG CONSTR NEW MATERIAL

Water-based facing type fireproof paint and preparation method thereof

The invention discloses water-based facing type fireproof paint. The water-based facing type fireproof paint is prepared from the following raw materials in mass fraction: 18.0-20.0wt% of film forming matter, 23-23.5wt% of a carbon forming catalyst, 10-11wt% of a carbon forming agent, 12-13wt% of a foaming agent, 9-11wt% of pigment filler, 0.49-1.13wt% of auxiliaries, 20-27.5wt% of water, 0-0.8wt% of trisodium phosphate and 0-0.4wt% of a silane defoaming agent. The invention further discloses a preparation method of the water-based facing type fireproof paint. The water-based facing type fireproof paint prepared by the preparation method disclosed by the invention has good fireproof performance, good water resistance, strong adhesive force for a combustible matrix and good decorativeness, and can be used for surface coating of buildings and decorative materials.
Owner:HEBEI CHENYANG INDAL & TRADE GROUP CO LTD

Cyclosporine compound eye drops and preparation method thereof

The invention relates to a cyclosporine-containing composition and a preparation method thereof. The compound eye drops are prepared from cyclosporine, anti-inflammatory or antibiotic drugs, a surfactant, a stabilizer, a thickener, an isoosmotic adjusting agent, a pH adjusting agentr and water or oil, the preparation is a mixed suspension agent or an emulsion, and one or two of a high pressure homogenization method and a wet grinding technique is / are combined for use in the preparation method. The cyclosporine compound eye drops have the advantages that the ophthalmic tolerance is excellent, the drug utilization degree is high, the tear secretion of people suffering from xerophthalmia can be effectively improved, the tear film is stabilized, the anti-inflammation function of the anti-inflammatory or antibiotic drugs and the immunoregulation function of cyclosporine can be synergistically exerted, xerophthalmia can be effectively treated, and the compound eye drops have a better treatment effect compared with the separate application of cyclosporine.
Owner:NKD PHARMA CO LTD

AKD (alkyl ketene dimer) starch and preparation method thereof

The invention relates to an AKD (alkyl ketene dimer) starch and a preparation method thereof. The method is implemented by selecting native corn starch as a raw material of starch through the following steps of: (1) adding the native corn starch into a reactor; (2) mixing an oxidant, a synergistic agent and water so as to obtain a solution; (3) injecting the solution obtained in the step (2) into the reactor in the step (1); and (4) carrying out standing, heating, heat preservation, cooling and sieving on a reactant obtained in the step (3) so as to obtain a finished product. The pH value of the AKD starch prepared by using the method disclosed by the invention is 6.5-8.5; and the viscosity of paste (6%) of the AKD starch at the temperature of 60 DEG C is less than or equal to 30mPa.s. The method is environmental-friendly, energy-saving, mild in reaction conditions, and easy to operate.
Owner:ZHEJIANG YIZHI STARCH

Rubber modified asphalt waterproof coating material, preparation method and uses thereof

The invention discloses a rubber modified asphalt waterproof coating material, which is prepared by mixing the following components: asphalt, rubber, an asphalt regenerant, an emulsifier, a stabilizer, water and other auxiliary agents. The invention further discloses a preparation method and applications of the rubber modified asphalt waterproof coating material. According to the present invention, in the rubber modified asphalt waterproof coating material preparation process, by using the asphalt regenerant, the added rubber can be fully fused with the asphalt, such that the modified asphaltwith high rubber content cannot segregate, and the asphalt regenerant can greatly reduce the high-temperature viscosity of the modified asphalt so as to reduce the emulsification difficulty of the modified asphalt with high rubber content; by using the preparation process comprising secondary pH value adjustment, the high solid content emulsified product can be prepared in the case of the low emulsifier adding amount; and by adding the stabilizer to the product of the invention, the occurrence of demulsification can be avoided so as to ensure the storage stability of the product at a later stage.
Owner:XI NIU PI WATERPROOFING TECH CO LTD

Preparation method of polyaniline-graphene hollow microspheres

The invention discloses a preparation method of polyaniline-graphene hollow microspheres. Firstly, isoamyl nitrite and sulfanilic acid are utilized to sulfonate graphene, the obtained sulfonated graphene is used as a Pickering emulsifier, water dispersion liquid of the obtained sulfonated graphene serves as a water phase, and toluene or an aniline monomer serves as an oil phase to perform emulsification, an oil-in-water (O / W) emulsion is obtained, then an oxidizing agent ammonium persulfate is added to trigger aniline polymerization, and the polyaniline-graphene hollow microspheres can be obtained after the oil phase toluene is removed. The polyaniline-graphene hollow microspheres are prepared by adopting a Pickering emulsion method. The preparation method is simple and efficient, and the prepared polyaniline-graphene hollow microsphere material with a three-dimensional hollow structure has larger specific surface area and a shorter ion and electron transmission path compared with a polyaniline-graphene composite material with a two-dimensional structure and has a greater potential application value on the aspects of catalysis, micro-reactors, sensing, energy storage materials and the like.
Owner:JIANGNAN UNIV

Multifunctional environment-friendly waterproof paint

The invention discloses multifunctional environment-friendly waterproof paint. The paint comprises, by weight, 25-35 parts of waterborne acrylic emulsion, 10-20 parts of butylbenzene emulsion, 10-20 parts of titanium dioxide, 5-10 parts of light calcium carbonate, 2-5 parts of ceramic fibers, 2-5 parts of molybdenum disulfide, 1-3 parts of dispersants, 0.1-2 parts of adhesion promoters, 0.1-1 part of an ultraviolet absorbent, 0.1-1 part of an antioxidant, 0.1-1 part of a defoamer, 0.5-5 parts of thickeners, 1-2 parts of coalescing agents and 10-25 parts of water. The multifunctional environment-friendly waterproof paint simultaneously has good adhesive force and mechanical properties, is good in ageing resistance, cracking resistance and temperature adaptability, is free of toxin, and is excellent in comprehensive performance.
Owner:班戈江龙玛曲实业有限公司

Multi-core hollow energetic microspheres for emulsion explosive and preparation method of multi-core hollow energetic microspheres

The invention relates to an energetic sensitizer for an emulsion explosive, in particular to an energetic additive coated with hollow microspheres for the emulsion explosive, and belongs to the fieldof energetic materials. The multi-core hollow energetic microspheres for the emulsion explosive are prepared from the following components in parts by weight: 10-50 parts of polymer monomers, 5-15 parts of an expansion agent and 5-80 parts of an energetic additive. A preparation method comprises the following steps: firstly, the polymer monomers, an initiator, a cross-linking agent and a foaming agent are mixed into an oil phase, then the energetic additive is added to the oil phase, the mixture is evenly mixed and then is dispersed in a water phase and suspended in a high-pressure reactor forpolymerization, heating is performed for curing, and thermal expandable multi-core composite energetic microspheres are obtained; finally, heating is performed for foaming and expanding, cooling is performed, and the multi-core hollow energetic microspheres are obtained. The multi-core hollow energetic microspheres can have dual effects of hot spots and the energetic additive in the emulsion explosive, and a shell can improve storage stability of the energetic additive and safety of the high-power emulsion explosive.
Owner:ANHUI UNIV OF SCI & TECH

Polymer cement waterproof material and preparation method thereof

The invention relates to a polymer cement waterproof material and a preparation method thereof. The polymer cement waterproof material comprises silicate cement, a polyacrylate / polyurethane composite emulsion, a water reducing agent, fibers, river sands and other materials according to a certain weight proportion. The polymer cement waterproof material has the characteristics, such as high strength and easiness of adhesion to wet substrate, of cement gel materials, and also has the characteristics, such as high elasticity and good water resistance, of polymer coatings. The polymer cement waterproof material is mainly applied to waterproofing in various industrial constructions, civil constructions, bridges, tunnels, traffic transportation and other industries and fields.
Owner:CHANGSHA UNIVERSITY OF SCIENCE AND TECHNOLOGY

Polyurethane emulsion, preparation method thereof and glass fiber sizing agent

The invention provides a polyurethane emulsion. The polyurethane emulsion is prepared from the following components in percentage by weight: 25-40 percent of polyester diol, 10-30 percent of polyether glycol, 2-10 percent of micromolecular diol, 30-40 percent of aliphatic diisocyanate, 2-10 percent of an amine chain extender and 0-6 percent of a solvent, wherein the micromolecular dihydric alcohol is prepared from dihydric alcohol with the number of carbon atoms being 2-10. The polyurethane emulsion is good in stability and is a nonionic polyurethane emulsion. When being used for preparing a glass fiber sizing agent, the polyurethane emulsion can not generate mutual action with ions ionized from other components of the sizing agent, so that the polyurethane emulsion is prevented from generating demulsifcation, the phenomena of sedimentation and caking of the sizing agent are prevented, and the obtained glass fiber sizing agent is good in stability. The invention provides a preparation method of the polyurethane emulsion and the glass fiber sizing agent.
Owner:CHONGQING POLYCOMP INT

Aqueous mono-component matte varnish and preparation method thereof

The invention discloses an aqueous mono-component matte varnish and a preparation method thereof. The invention belongs to the field of paints. The varnish comprises components of, by weight: 40 to 50 parts of an aqueous polyurethane dispersion, 20 to 30 parts of polyacrylic acid modified polyurethane, 0.1 to 0.5 parts of a moistening agent, 1.0 to 2.0 parts of a thickening agent, 0.1 to 0.5 parts of an antifoaming agent, 2.0 to 8.0 parts of a dulling agent, 0.1 to 0.5 parts of a leveling agent, 0.1 to 2.0 parts of a film forming auxiliary agent, and 1.0 to 5.0 parts of water. The varnish provided by the invention has excellent luster, appearance, fouling resistance, chemical resistance, and mechanical properties. The varnish can be applied in construction in combination with other paints such as emulsion paint. The application of the varnish is easy and diverse.
Owner:CHENGDU BEIDA PAINT

Modified waterborne polyaniline epoxy resin coating and preparation method thereof

The invention relates to a modified waterborne polyaniline epoxy resin coating. The modified waterborne polyaniline epoxy resin coating comprises 36-45 parts of epoxy resin, 12-20 parts of hydrochloric acid, 6-15 parts of aniline, 18-30 parts of ammonium persulfate, 9-26 parts of acrylic acid, 2-11 parts of dodecylbenzene sulfonic acid, 6-17 parts of polyamide resin, 25-45 parts of N-allylmethylamine and 22-40 parts of diethanol amine. The modified waterborne polyaniline epoxy resin coating has the advantages that a water-soluble redox system is used for initiating double-bond curing, so that the problems of system emulsion breaking and layering are avoided effectively; the coating is excellent in anti-corrosion performance and highly resistant to scratch and pitting; the coating with excellent physical and chemical performance is excellent in bonding strength for the surfaces of metal and non-metal materials, good in dielectric performance and small in setting shrinkage ratio.
Owner:GUANGXI UNIV

Method for preparing large-diameter high-sphericity polymer hollow micro-spheres

The invention discloses a method for preparing large-diameter high-sphericity polymer hollow micro-spheres. The method has the advantages that curing speed reducing and rotary curing processes are organically combined with one another, curing containers are sealed in procedures for preparing polymer hollow micro-spheres by the aid of microfluidic technologies, the quantities of dual-emulsion particles in external water phases and the quantities of preliminarily added organic solvents are changed, diffusion of the organic solvents towards the external water phases can be suppressed by the aid of the solubility of the organic solvents in the external water phases, the curing speeds of dual-liquid droplet can be reduced, and spheroidization of the dual-emulsion particles can be promoted; horizontal inclination angles, rotation modes and the rotational speeds of rotary flasks are controlled, accordingly, dispersion states of the dual-emulsion particles in the external water phases can be controlled, adhesion, coalescence and emulsion breaking of the dual-emulsion particles due to mutual collision can be prevented, non-spheroidization tendency of the dual-emulsion particles can be lowered, and the large-diameter high-sphericity polymer hollow micro-spheres can be prepared; the large-diameter high-sphericity polymer hollow micro-spheres can be applied to laser inertial confinement fusion physical experiments.
Owner:LASER FUSION RES CENT CHINA ACAD OF ENG PHYSICS

Waterborne epoxy asphalt coating and preparation method thereof

InactiveCN111978815AExcellent anti-corrosion performance and bonding performanceGood water resistanceAnti-corrosive paintsEpoxy resin coatingsPolyamideCorrosion resistant
The invention provides a waterborne epoxy asphalt coating. The coating comprises a component A and a component B. The component A is prepared from the following raw materials in parts by weight: 15-18parts of deionized water, 0.2-0.5 part of a pH regulator, 0.3-0.5 part of anti-sagging auxiliary agent, 0.2-0.3 part of a wetting agent, 1.1-1.3 parts of a dispersing agent, 0.1-0.2 part of a defoaming agent, 3-5 parts of talcum powder, 10-13 parts of precipitated barium sulfate, 0.5 part of carbon black, 6-10 parts of iron oxide black, 3-5 parts of antirust pigment, 24-28 parts of epoxy resin, 4-6 parts of silica sol, 1-2 parts of propylene glycol monomethyl ether, 0.2-0.4 part of a flatting agent, 0.4-0.6 part of a flash rust inhibitor, 0.7-1 part of a thickener, 15-20 parts of emulsified asphalt and 2-3 parts of a coupling agent. The component B is an aliphatic amine modified polyamide polymer. The mass ratio of the component A to the component B is 12:1. The thickness of a film formedby one-time spraying of the coating can reach 150 microns, and the coating has excellent corrosion resistance, sagging resistance and chemical resistance.
Owner:北京红狮科技发展有限公司

Sand-in-water multicolor paint and preparation method thereof

The invention relates to the technical field of coatings, and provides a sand-in-water multicolor coating and a preparation method thereof. The sand-in-water thermal insulation coating provided by theinvention comprises base paint, a protective glue solution and a continuous phase, wherein the base paint is prepared from the following components in parts by weight: 0.6-0.65 part of cellulose, 0.5-1 part of inorganic color paste, 40-50 parts of quartz sand, 3.5-4 parts of a filler, 2.5-3 parts of acrylic emulsion, 10-11 parts of silicon dioxide dispersion liquid, 0.3-0.4 part of protective glue and 30-36 parts of water. The sand-in-water multicolor paint has good stability and long storage period, meets the requirements of inorganic paint standards for buildings on the content of macromolecular organic matters, and can meet the requirements of energy conservation, environmental protection, safety, fire prevention and the like, so that a formed paint film has rich and full patterns, high simulation degree and vivid stone effect.
Owner:珠海展辰新材料股份有限公司

Alcohol-free transparent perfume composition

The invention provides an alcohol-free transparent perfume composition which comprises nanoemulsion, water and other auxiliaries, wherein the nanoemulsion comprises the following materials in parts by weight: 5-20 parts of essential oil, 8-12 parts of polyoxyethylene surfactants, 5-8 parts of phosphate surfactants, 4-7 parts of polyglycerol ester surfactants, 0.5-1.2 parts of glycerol and 15-20 parts of water; and grain size of the nanoemulsion is 10 nm-100nm. According to the invention, transparent water-based perfume emulsion is formed by dispersing oil-soluble essential oil in water through compounding effect of the polyoxyethylene surfactants, the phosphate surfactants, and the polyglycerol ester surfactants, so that a problem that organic solvents such as alcohol are used as perfume solvents is avoided, thereby avoiding stimulus and harms on the skin; and nanoemulsion grain size in the nanoemulsion is distributed between 10 nm and 100nm, so that stability is good, and the nanoemulsion is prevented from breaking of emulsion.
Owner:AGATE PERFUME MINGGUANG

Transparent aqueous monocomponent priming paint and preparation method thereof

The invention which discloses a transparent aqueous monocomponent priming paint and a preparation method thereof belongs to the coating field. The formula of the priming paint comprises, by weight, 40-50 parts of an aqueous polyurethane dispersion, 20-30 parts of polyacrylic acid modified polyurethane, 0.1-0.5 parts of a wetting agent, 1.0-2.0 parts of a thickening agent, 0.1-0.5 parts of an antifoaming agent, 5.0-15.0 parts of a filler, 0.1-0.5 parts of a leveling agent, 0.1-2.0 parts of a film forming assistant and 1.0-5.0 parts of water. The priming paint of the invention has the advantages of excellent luster and appearance, good contamination resistance and chemical resistance, excellent mechanical performance, realization of simultaneous construction with other paints of an emulsion paint and the like, easy operation, and diversification.
Owner:CHENGDU BEIDA PAINT

Method for preparing cement asphalt (CA) mortar for China railway track system (CRTS) II slab ballastless tracks

The invention discloses a method for preparing cement asphalt (CA) mortar for China railway track system (CRTS) II slab ballastless tracks, which comprises the following steps of: (1) mixing cement with fine sand, an expanding agent and aluminum powder according to proportion to prepare dry CA mortar powder; and (2) sequentially adding a poly carboxylic acid serving as a high-performance water reducing agent, an antifoaming agent and silica sol into water for uniform stirring, adding the dry CA mortar powder for uniform stirring, and adding asphalt emulsion for uniform stirring to obtain the CA mortar for the CRTS II slab ballastless tracks. The method has the advantages of: (1) avoiding cement particles competitively absorbing an emulsifier in the asphalt emulsion, and preventing the asphalt emulsion in the CA mortar from being demulsified to cause bleeding; and (2) reducing the using amount of the asphalt emulsion and the using amount of the water on the basis of ensuring flowability, and strengthening the strength of the CA mortar on the basis of meeting an elastic modulus of the CA mortar.
Owner:ZHEJIANG UNIV

High weather resistant and flame-retardant cable

The invention discloses a high weather resistant and flame-retardant cable, which comprises a conductor, an insulating layer cladding the conductor, a packing layer cladding the insulating layer, a shielding layer cladding the packing layer, an armor layer cladding the shielding layer and an outer sheath cladding the armor layer. The outer sheath comprises the following raw materials by weight part: 45-48 parts of styrene butadiene rubber, 25-27 parts of chloroprene rubber, 17-20 parts of natural rubber, 10-13 parts of phase change control microcapsule, 0.8-1.2 parts of sulfur powder, 1.6-2.4 parts of an accelerator AA, 2.5-2.8 parts of an accelerator MZ, 8-11 parts of hard clay, 6-9 parts of sepiolite, 6-8 parts of lanthanum oxide, 5-7 parts of mica powder, 2.6-3 parts of a monoalkoxy pyrophosphate type titanate coupling agent, 2.4-2.8 parts of coconut oil, 3-6 parts of naphthenic oil, 4-6 parts of antimony trioxide, 3-5 parts of melamine, 4-6 parts of red phosphorus masterbatch, 5-8 parts of barium stearate, 1.5-2.5 parts of an anti-aging agent H, and 1.3-1.6 parts of an anti-aging agent DFC-34.
Owner:ANHUI NANYANG NEW MATERIAL TECH CO LTD

Acidic oil-in-water emulsion composition with low water activity, and preparation method and application of acidic oil-in-water emulsion composition

The invention discloses an acidic oil-in-water emulsion composition with low water activity. The acidic oil-in-water emulsion composition comprises the following components in parts by weight: 30-60 parts of vegetable oil, 5-15 parts of polyalcohol, 0.45-2.4 parts of a thickening agent, 2.55-5 parts of an acid agent and 24-59 parts of other base materials. On the basis that oil content is not increased, the polyalcohol of a special content is added to a formula for replacing part of water, so that the polyalcohol interacts with free water and prevents free water from generating bound water, and the content of the free water in a system is reduced; in addition, through compounding of the thickening agent of the special content, the condition that the water activity is reduced so that the stickiness of the system is increased can be controlled, the stickiness is controlled to a stickiness range operable for an industrialized production machine, and the emulsion breaking phenomenon causedby high stickiness, uneven cutting emulsifying or excessive heat is avoided. The technology is improved in the following aspects: raw materials and auxiliary materials which can generate interactionin advance mixing are separated, the feeding sequence is reasonably arranged, the acid agent is firstly added to simplify the operation technology, the homogenizing time is shortened, and the efficiency is improved.
Owner:GUANGZHOU HAODAO FOOD CO LTD

High-resolution water-based flexible printing ink and preparation method thereof

The invention discloses a high-resolution water-based flexible printing ink comprising ink paste and acrylic emulsion. The ink is characterized in that the ink paste comprises the following components in parts by weight: 20 to 30 parts of water-based acrylic resin, 30 to 60 parts of pigment, 2 to 8 parts of dispersant 760W, 10 to 20 parts of water, 10 to 15 parts of ethanol, and 0.5 to 1 part of defoaming agent. The invention further discloses a preparation method for the ink. The quantity of the pigment is increased in the ink paste of the ink disclosed by the invention, and meanwhile, the dispersant 760W is adopted, so that a large dose of pigment can be well dispersed, and the ink has good stability and good dyeing property. The ink can reach more than 100 resolution cables and can be used for directly printing line boards, and the inking effect is similar to an offset printing effect. The third dimension of printed pictures can be reflected, and the pictures are exquisite and vivid. Moreover, the ink disclosed by the invention is water-based ink, so the ink accords with the national environmental protection policy, and can achieve the printing effect of an oil-based ink.
Owner:CHONGQING HONGYUAN PRINTING INK

Environment-friendly coating for exterior wall and preparation method thereof

The invention belongs to the technical field of environment-friendly coatings and relates to an environment-friendly coating for an exterior wall and a preparation method thereof. The environment-friendly coating for the exterior wall comprises the following raw materials in parts by weight: 40 to 50 parts of an acrylic emulsion, 20-30 parts of polyether polyol, 20-30 parts of a filler, 10-20 parts of carboxymethyl betaine, 5-10 parts of isocyanate, 5-10 parts of ceramic fibers, 5-10 parts of nanometer silicon dioxide, 5-8 parts of a surfactant, 3-6 parts of a plasticizer, 1-3 parts of a drying agent, 1-2 parts of an anti-aging agent and 0.5-1 part of an anti-ultraviolet agent, wherein the anti-aging agent is prepared from zirconium oxide, nanometer titanium dioxide and modified graphene according to a mass ratio of (10-5): (4-8): 1. The environment-friendly coating is non-toxic, odorless, green and safe, has good elasticity, flexibility, waterproofness, aging resistance, abrasion resistance and ultraviolet resistance, short curing time, good hardness and long service life, can be directly painted, and is convenient to operate and applicable to exterior walls.
Owner:青川源泰建材科技有限公司

Two-component rubber modified asphalt waterproof coating material, preparation method and applications

The invention discloses a two-component rubber modified asphalt waterproof coating material, a preparation method and applications, wherein the two-component rubber modified asphalt waterproof coatingmaterial comprises a first component and a second component according to a mass ratio of 1:(0.1-1.0), the first component is prepared by mixing the following components by mass: 25.8-56% of asphalt,6-15.4% of rubber, 6-24.5% of an asphalt regeneration agent, 0.8-4.0% of an emulsifier, 0.03-5.0% of a stabilizer, 0 -5.0% of other auxiliary agents, and the balance of water, the sum of the mass percentages of the asphalt and the asphalt regeneration agent is 46-63%, and the second component is one or a plurality of materials selected from active fillers and inert fillers. According to the present invention, by using the asphalt regeneration agent, the added rubber can be fused with the asphalt so as not to cause segregation phenomenon, and the asphalt regeneration can greatly reduce the hightemperature viscosity of the modified asphalt, such that the emulsification difficulty of the modified asphalt with the high rubber ratio can be lowered.
Owner:XI NIU PI WATERPROOFING TECH CO LTD

Degradable core-shell type oxidized calcium alginate gel microsphere, and preparation method and application thereof

The invention belongs to the technical field of materials, and particularly relates to a degradable core-shell type oxidized calcium alginate gel microsphere, and a preparation method and applicationthereof. According to the preparation method disclosed by the invention, the degradable core-shell type oxidized calcium alginate gel microsphere is prepared on the basis of micro-fluidic control; andan inner oil-phase fluid, a water-phase fluid and an outer oil-phase fluid form oil / water / oil double emulsion droplets, an acidic oil phase fluid containing organic acid is introduced into the downstream position of the oil / water / oil double emulsion droplets, calcium hydrochloride nanoparticles in a water phase of the oil / water / oil double emulsion droplets are rapidly dissolved, and free calciumions are released, so oxidized alginate in a water phase and the calcium ions are initiated to undergo rapid cross-linking so as to form a gelatinous oxidized alginate layer, and the degradable core-shell type oxidized calcium alginate gel microsphere is obtained. The degradable core-shell type oxidized calcium alginate gel microsphere prepared by the preparation method has the advantages that a size structure is uniform and monodispersity is high.
Owner:SUN YAT SEN UNIV

Environment-friendly waterproof coating material and preparation method thereof

The invention belongs to the technical field of environment-friendly coating materials, and relates to an environment-friendly waterproof coating material and a preparation method thereof. The environment-friendly waterproof coating material is prepared from the following raw materials in parts by weight: 40-50 parts of an acrylic resin, 30-40 parts of an epoxy resin, 20-30 parts of polyether polyol, 15-25 parts of polyvinyl alcohol, 10-20 parts of a filler, 5-8 parts of a water-soluble adhesive, 4-6 parts of carbon fiber, 3-8 parts of an auxiliary agent, 3-5 parts of nano silicon dioxide, 3-5parts of calcium oxide and 1-3 parts of a drying agent, wherein the drying agent is prepared from the following raw materials in parts by weight: 30 to 40 parts of propylene glycol diacetate, 20 to 30 parts of a polybutenoic acid ester polymer, 10 to 15 parts of microcrystalline cellulose and 3 to 5 parts of cerous sulfate. The waterproof coating material disclosed by the invention is non-toxic,odorless, environmentally-friendly and safe, has good elasticity, impact resistance, wear resistance, flexibility and waterproofness, and can be quickly cured into a film so as to substantially shorten the drying and curing time, so that the next procedure can be quickly implemented, and the construction efficiency is remarkably improved.
Owner:青川源泰建材科技有限公司

Method for preparing energetic hollow microspheres by microwave heating method

The invention relates to a method for preparing energetic hollow microspheres, in particular to a method for preparing energetic hollow microspheres through microwave heating, and belongs to the fieldof energetic materials. An energetic hollow microsphere prepared by a microwave heating method mainly comprises the following components in parts by weight: 1-15 parts of an expanding agent, 1-10 parts of a wave-absorbing material, 60-95 parts of an energetic additive and 10-30 parts of a polymer monomer. The method includes: mixing a polymer monomer, an initiator, a cross-linking agent and a foaming agent to form an oil phase; then adding an energetic additive and a wave-absorbing material into the oil phase, uniformly mixing the components, dispersing the components in the water phase, carrying out suspension polymerization in a high-pressure reaction kettle, then heating and curing the product to obtain energetic microspheres, and finally carrying out microwave-assisted heating for foaming and expansion, and cooling the product to obtain the energetic hollow microspheres. Different from a traditional direct heating method with temperature gradient, the microwave heating method hasthe advantages that the temperature gradient is different, wherein the microwave can enable the energetic microspheres containing the wave-absorbing material to start to be heated and expanded at thesame time, so that the uniformity of the particle size of the final energetic hollow microspheres is guaranteed, and meanwhile breakage of part of the energetic microspheres caused by uneven heating is avoided.
Owner:ANHUI UNIV OF SCI & TECH

Preparation method of core-shell acrylic emulsion for color digital ink-jet printing

The invention discloses a preparation method of a core-shell acrylic emulsion for color digital ink-jet printing. The preparation method comprises the steps of the preparation of a monomer solution A, the preparation of a monomer solution B, polymerization reaction, and the like. By using the preparation method, the stability of a polymer emulsion can be improved, especially the viscosity is not increased with the increase of storage time, and obtained products are excellent in wet color fastness, good in coating binding force and high in strength. By using a method for core-shell emulsion polymerization, used acrylic functional monomers are all polymerized in a core of an emulsion microsphere, and carboxyl does not exist in a shell formed by emulsion polymerization, so that a situation that hydroxyl in PVA and carboxyl in polymers interact to cause the demulsification of the polymers can be avoided, thereby improving the stability of weak solvent dispersion liquid.
Owner:李娟 +1

Instant emusifying burner using fuel oil/light oil

The instantaneously fuel oil / light oil emulsifying burner includes burning unit, light oil tank, heavy oil storing tank, steam source and water tank, and inside the burning unit, there are oil emulsifying nozzle and oil igniting nozzle. The oil emulsifying nozzle is provided with oil jet in front part, atomizing steam inlet, emulsifying water inlet and heavy oil inlet in the back part, steam-water mixing chamber, oil-steam mixing chamber steam-water channel and heavy oil channel inside it. The present invention can save fuel oil andp revent pollution to atmosphere, and may be used in various oil burning boilers, heating furnace and kiln.
Owner:陈永元

Liquid non-fluorescent lubricant for well drilling

The invention discloses a liquid non-fluorescent lubricant for well drilling. The lubricant is prepared from 50-60 parts of white oil, 6-12 parts of sulfonated palm oil, 4-8 parts of vegetable oil acid, 5-12 parts of octaphenyl polyoxyethyiene-10, 12-18 parts of sorbide oleate, 6-15 parts of chloralkane. The lubricant is prepared by taking the white oil as an oil base, the sulfonated palm oil as asynthesized anionic surfactant and the octaphenyl polyoxyethyiene-10, the sorbide oleate and the like which are taken as a nonionic surfactant are used as auxiliary materials, finally the efficient and environmentally friendly non-fluorescent lubricant capable of resisting salt is obtained, and the extreme pressure lubrication coefficient can reach 98%; the viscosity coefficient of a mud cake canreach 70%; the lubricant can be used for horizontal wells and large inclined wells, the compatibility between the lubricant and other drilling fluid materials is good, and the lubricant has good lubricating performance in the drilling fluid system; the non-fluorescent grade or the fluorescence grade is extremely low, and the lubricant can better cooperate with the specific operation of geologicallogging and the like.
Owner:SICHUAN ZHENGRONG IND +1

High-strength concrete shrinkage reducing agent

InactiveCN109956698ALarge adsorption capacityImprove group distributionIonActive agent
The invention discloses a high-strength concrete shrinkage reducing agent, and belongs to the technical field of building material. The high-strength concrete shrinkage reducing agent contains both positive ion groups and negative ion groups, is capable of improving distribution of carboxylate anion groups and effective adsorption on cement particles, increasing concrete strength, and preventing drying shrinkage cracking. According to a preparation method, tween-20 is added into a prepared mechanical reinforcing active agent for combination, so that emulsion demulsification is prevented, concrete porosity is reduced, and concrete internal mechanical performance and strength are increased. A prepared active agent capable of regulating surface tension contains amphoteric groups, so that concrete material drying shrinkage is reduced effectively. A plasticizing activator is adopted to increase concrete slurry fluidity firstly for water reducing slump retaining, plant oil is added to fill internal pores for improvement of density, and drying shirinkage prevention efficiency is increased. The high-strength concrete shrinkage reducing agent is capable of solving problems in the prior artthat shrinkage cracks still exist after adding of the concrete slump retaining agent, and influences on concrete strength are eliminated.
Owner:雷洪伍
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