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51results about How to "Uniform activation" patented technology

Method for synthesizing ultrafine calcium carbonate by utilizing carbide slag

The invention relates to a method for synthesizing ultrafine calcium carbonate by utilizing carbide slag. The method comprises the following steps of: (1) dissolving carbide slag: uniformly mixing carbide slag with water in a ratio of (1:6)-(1:20) to ensure that the carbide slag is fully dissolved into a turbid liquid, wherein the water content of the carbide slag is 20-45%; (2) carrying out impregnation reaction: adding ammonium chloride into the turbid liquid of the carbide slag for uniformly mixing, wherein the mass ratio of carbide slag to ammonium chloride is (1:0.7)-(1:2.5), after the impregnation reaction is finished, filtering and removing the slag to obtain a clear calcium chloride solution; and (3) carrying out carbonization reaction: adding a crystal form control agent into a calcium chloride solution for fully dissolving, introducing CO2 into the solution to carry out carbonization reaction till the pH (potential of Hydrogen) value of the reaction solution is less than or equal to 7 to obtain ultrafine calcium carbonate slurry, wherein the crystal form control agent is one or more than two mixtures of sulfate, chloride, citrate, sodium dodecyl benzene sulfonate, pyrophosphate, oleic acid, ammonium citrate, N-methyl pyrrolidone and maleic acid.
Owner:SINOMA INT ENG +1

Preparation method of bone inducing porous titanium artificial bone

The invention relates to a preparation method of bone inducing porous titanium artificial bone. The method comprises the following steps: a porous titanium block is processed into a required shape and is washed; the surface is activated; the porous titanium block is put into acid solution which is prepared by sulfuric acid, hydrochloric acid and deionized water to be processed and then is put into alkali solution of sodium hydroxide; or put into acid solution which is prepared by hydrofluoric acid, nitric acid and deionized water to be processed and is then put into hydrogen peroxide solution; or put into acid solution which is prepared by hydrofluoric acid, nitric acid and deionized water to be processed and is then put into hydrogen peroxide solution which contains tantalum pentachloride; the method is characterized in that the surface of the porous titanium can be activated uniformly without pre-depositing a calcium phosphate layer, when being soaked in simulated body fluid at 36.5DEG C, bone-like apatite can be induced to deposit in 28 days; and bone inductivity can be given to the porous titanium artificial bone. The bone inducing porous titanium artificial bone is used for repairing, replacing or reinforcing bone tissue and can reinforce the regeneration of the bone tissue and the interfacial bond of the implant site; and the process is simple and the operation is convenient.
Owner:SICHUAN UNIV

Production method of cellulose acetate

The invention belongs to the field of polymer chemistry, and relates to a preparation method of cellulose acetate. The cellulose acetate obtained by the method has low turbidity and high viscosity. The method comprises the following steps of: A, activating 1 weight part of cellulose by using 8 to 20 weight parts of glacial acetic acid at the temperature of between 20 and 60 DEG C; B, adding 0.005 to 0.05 weight part of catalyst and 3 to 6 weight parts of acetic anhydride; C, adding 0.5 to 1.5 weight parts of high-concentration acetic acid solution at the temperature of between 10 and 25 DEG C, and reacting till the content of the acetic acid is 60.5 to 62.5 percent, wherein the high-concentration acetic acid solution is 80 mass percent acetic acid; D, adding 0.5 to 1.5 weight part of 5 to 15 weight percent aqueous solution of acetate, and reacting for 1 to 3 hours at the temperature of between 20 and 50 DEG C; and E, filtering, settling and granulating. The preparation method is simple and convenient in the production process and easy in operation; the reaction time is shortened; the prepared product has high substitution degree, namely the content of the acetic acid is more than or equal to 60.0 percent; the product has high viscosity, namely the falling ball viscosity is more than or equal to 70 seconds; and the cellulose acetate is particularly suitable for manufacturing polarizing films in optical elements.
Owner:LUZHOU NORTH CHEM IND

Method for synthesizing ultrafine calcium carbonate by utilizing carbide slag

The invention relates to a method for synthesizing ultrafine calcium carbonate by utilizing carbide slag. The method comprises the following steps of: (1) dissolving carbide slag: uniformly mixing carbide slag with water in a ratio of (1:6)-(1:20) to ensure that the carbide slag is fully dissolved into a turbid liquid, wherein the water content of the carbide slag is 20-45%; (2) carrying out impregnation reaction: adding ammonium chloride into the turbid liquid of the carbide slag for uniformly mixing, wherein the mass ratio of carbide slag to ammonium chloride is (1:0.7)-(1:2.5), after the impregnation reaction is finished, filtering and removing the slag to obtain a clear calcium chloride solution; and (3) carrying out carbonization reaction: adding a crystal form control agent into a calcium chloride solution for fully dissolving, introducing CO2 into the solution to carry out carbonization reaction till the pH (potential of Hydrogen) value of the reaction solution is less than or equal to 7 to obtain ultrafine calcium carbonate slurry, wherein the crystal form control agent is one or more than two mixtures of sulfate, chloride, citrate, sodium dodecyl benzene sulfonate, pyrophosphate, oleic acid, ammonium citrate, N-methyl pyrrolidone and maleic acid.
Owner:SINOMA INT ENG +1

Uniform internal heating stirring type activation kiln

The invention discloses a uniform internal heating stirring type activation kiln, and belongs to the field of activated carbon. The uniform internal heating stirring type activation kiln comprises a kiln body, a feeding mechanism, a flow guide stirring mechanism, a water seal mechanism, a discharging mechanism and a hot blast stove, and the feeding mechanism is arranged on the side wall of the kiln body; the kiln main body mainly comprises a kiln upper cover and a kiln lower body, the kiln lower body mainly comprises a hot-blast stove body, a hot-blast stove shell and a lower body shell fixedly connected with the hot-blast stove shell, and the flow guide stirring mechanism is connected in the lower body shell; the kiln has a stirring effect and also has the effect of transporting activators; when the flow guide stirring paddles rotate to any place, the activators is conveyed to any place; the flow guide stirring paddles are uniformly distributed in the material layer; the activated material layer with the thickness of two meters is simultaneously stirred from inside to outside, is simultaneously heated and is in contact with the activators so that the activation is uniform, the specific surface area of the activated carbon is large, the activation time is shortened, and the single-machine productivity is high.
Owner:舒克孝

Method for preparing super capacitor active carbon by utilizing acid sludge pitch

The invention provides a method for preparing super capacitor active carbon by utilizing acid sludge pitch. The method comprises the following steps that acid sludge pitch is smashed to obtain acid sludge pitch powder; the acid sludge pitch powder is placed in a basic solution to be mixed, the mixture is subjected to dispersion, homogenizing and emulsifying, and emulsion of the acid sludge pitch and the basic solution is obtained; the emulsion is placed into an activating oven to be dried and dehydrated, and then carbonized and activated at the high temperature and under protection of nitrogen; the activated product is washed till to be neutral, and then subjected to vacuum rotation drying, and the super capacitor active carbon is obtained. The acid sludge pitch being taken as the raw material is cheap and easy to get, and can be reused, and thus the pollution of the acid sludge pitch to the environment can be reduced. The acid sludge pitch has the rich acidic functional groups, and has the good polarity, the acid sludge pitch particles can be in contact with the basic solution in the nano size in the homogeneous emulsion, the mass transferring resistance is overcome, and thus theactivation process can be operated evenly.
Owner:佛山市光烨环保科技有限公司

Production method of cellulose acetate

The invention belongs to the field of polymer chemistry, and relates to a preparation method of cellulose acetate. The cellulose acetate obtained by the method has low turbidity and high viscosity. The method comprises the following steps of: A, activating 1 weight part of cellulose by using 8 to 20 weight parts of glacial acetic acid at the temperature of between 20 and 60 DEG C; B, adding 0.005to 0.05 weight part of catalyst and 3 to 6 weight parts of acetic anhydride; C, adding 0.5 to 1.5 weight parts of high-concentration acetic acid solution at the temperature of between 10 and 25 DEG C, and reacting till the content of the acetic acid is 60.5 to 62.5 percent, wherein the high-concentration acetic acid solution is 80 mass percent acetic acid; D, adding 0.5 to 1.5 weight part of 5 to15 weight percent aqueous solution of acetate, and reacting for 1 to 3 hours at the temperature of between 20 and 50 DEG C; and E, filtering, settling and granulating. The preparation method is simple and convenient in the production process and easy in operation; the reaction time is shortened; the prepared product has high substitution degree, namely the content of the acetic acid is more than or equal to 60.0 percent; the product has high viscosity, namely the falling ball viscosity is more than or equal to 70 seconds; and the cellulose acetate is particularly suitable for manufacturing polarizing films in optical elements.
Owner:LUZHOU NORTH CHEM IND

A method for preparing activated carbon for supercapacitors by using acid residue pitch

The invention provides a method for preparing super capacitor active carbon by utilizing acid sludge pitch. The method comprises the following steps that acid sludge pitch is smashed to obtain acid sludge pitch powder; the acid sludge pitch powder is placed in a basic solution to be mixed, the mixture is subjected to dispersion, homogenizing and emulsifying, and emulsion of the acid sludge pitch and the basic solution is obtained; the emulsion is placed into an activating oven to be dried and dehydrated, and then carbonized and activated at the high temperature and under protection of nitrogen; the activated product is washed till to be neutral, and then subjected to vacuum rotation drying, and the super capacitor active carbon is obtained. The acid sludge pitch being taken as the raw material is cheap and easy to get, and can be reused, and thus the pollution of the acid sludge pitch to the environment can be reduced. The acid sludge pitch has the rich acidic functional groups, and has the good polarity, the acid sludge pitch particles can be in contact with the basic solution in the nano size in the homogeneous emulsion, the mass transferring resistance is overcome, and thus theactivation process can be operated evenly.
Owner:佛山市光烨环保科技有限公司

A kind of solar heat storage material with kaolin as supporting matrix and its preparation method

The invention discloses a solar heat storage material taking kaolin as a supporting basal body and a preparation method of the solar heat storage material. Kaolin which is different in microstructure and paraffin are taken as materials, surface of the kaolin is activated by virtue of microwave acid treatment, and further is compounded with the paraffin to obtain the heat storage material. Heat storage capacity of the material is 84J.g<-1>-107J.g<-1>, and a heat conductivity coefficient of the material is adjustable in a range of 0.65 W.m<-1>.K<-1> to 0.78 W.m<-1>.K<-1>. The solar heat storage material disclosed by the invention is reasonable in proportion, simple in processing process, and capable of effectively improving binding force between a phase-change material and a supporting basal body; with effective broadening heat storage performance, the prepared heat storage material has excellent thermal circulation performance, satisfies requirements of recycling and applying in more fields, and expands application field of the kaolin-base heat storage material; kaolin in different structures which is formed by utilizing mineralizing condition difference of minerals is utilized, so that the prepared solar heat storage material is adjustable in heat storage capacity and heat conductivity coefficient, and suitable for large-scale industrial production.
Owner:CENT SOUTH UNIV
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