Manganese-based composite positive electrode material and preparation method therefor
A composite positive electrode material, manganese-based technology, applied in the direction of battery electrodes, electrical components, electrochemical generators, etc., can solve the problems of low specific capacity, poor battery life, low battery specific energy, etc., to achieve high tap density, High packing density, the effect of increasing the specific capacity
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Embodiment 1
[0035] At room temperature, use 500 g of 95% ethanol to dissolve 1.7 g of phenolic resin into a solution; then add 5 g of spinel lithium manganate whose particle size is concentrated at 0.3-10 microns, stir to form a suspension, and then add manganese acetate, Add lithium hydroxide, chromium nitrate, and lanthanum nitrate, and control the atomic ratio of lithium, lanthanum, chromium, and manganese to 1.91:0.03:0.03:0.97. Stir for 30 minutes, dissolve lithium hydroxide with 350g of water, add, stir at constant temperature to form a suspension;
[0036] Heat the above suspension to 80°C for treatment, so that the phenolic resin will evenly bond and coat the deposit on the surface of the spinel lithium manganate particles. The treatment time is until the solvent is completely evaporated to obtain the precursor;
[0037] Put the above-mentioned precursor in a microwave kiln, heat treatment with nitrogen as a protective gas, the linear flow rate of nitrogen in the microwave kiln is...
Embodiment 2
[0040] At room temperature, use 300 g of 95% ethanol to dissolve 0.85 g of phenolic resin into a solution; then add 5 g of spinel lithium manganate whose particle size is concentrated at 0.3-10 microns, stir to form a suspension, and then add manganese acetate, Add lithium hydroxide, chromium nitrate, and lanthanum nitrate, and control the atomic ratio of lithium, lanthanum, chromium, and manganese to 1.91:0.03:0.03:0.97. Stir for 30 minutes, dissolve lithium hydroxide with 125g of water, add, stir at constant temperature to form a suspension;
[0041] Heat the above suspension to 60°C for treatment, so that the phenolic resin will evenly bond and coat the deposit on the surface of the spinel lithium manganate particles. The treatment time is until the solvent is completely evaporated to obtain the precursor;
[0042] Put the above-mentioned precursor in a horse boiling furnace, heat treatment with nitrogen as a protective gas, the linear flow rate of nitrogen in the horse boi...
Embodiment 3
[0045] At room temperature, 500 g of 95% ethanol was used to dissolve 0.85 g of phenolic resin into a solution; then 5 g of spinel lithium manganate with a particle size of 0.3-10 microns was added, stirred to form a suspension, and manganese acetate, Add lithium hydroxide, chromium nitrate, and lanthanum nitrate, and control the atomic ratio of lithium, lanthanum, chromium, and manganese to 1.55:0.15:0.15:0.85. Stir for 30 minutes, dissolve lithium hydroxide with 250g of water, add, stir at constant temperature to form a suspension;
[0046] Heat the above suspension to 80°C for treatment, so that the phenolic resin will evenly bond and coat the deposit on the surface of the spinel lithium manganate particles. The treatment time is until the solvent is completely evaporated to obtain the precursor;
[0047] Put the above-mentioned precursor in a microwave oven, heat treatment with nitrogen as a protective gas, the linear flow velocity of nitrogen in the microwave oven is not ...
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