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Waterborne heat-insulating flame-retardant multifunctional nano coating and preparation method thereof

A nano-coating and multi-functional technology, which is applied in the direction of fireproof coatings, epoxy resin coatings, polyurea/polyurethane coatings, etc., can solve the problems of coating stain resistance and weather resistance, the waterproof performance is difficult to meet the requirements, and the waterproof performance cannot be achieved Requirements and other issues, to achieve the effect of smooth surface, low cost, low production and production costs

Inactive Publication Date: 2010-09-08
长沙新凯化工有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The main problem of this type of coating is that the coating is relatively late, the construction requirements are high, and the heat insulation effect is not significant enough; secondly, due to the high porosity of the coating, although the coating of the above heat insulation coating is relatively thick, its waterproof performance is still difficult. fulfil requirements
In addition, these heat-insulating coatings have not paid much attention to the stain resistance of the coating.
The patent application number is CN200410048047.1, which reduces the thermal conductivity by adding hollow ceramics to achieve heat insulation effect, but the coating uses the solvent xylene, which is harmful to the environment
The patent application number CN02134827.8 is a water-based heat-insulating coating using styrene-acrylic emulsion; the patent application number CN03147361.X only uses kaolin as the main filler to achieve heat insulation, and the heat insulation effect is relatively poor; the patent application number is The patent of CN95101625.3 achieves heat insulation effect by using talcum powder and waterproof heat insulation powder
However, these existing inventions rarely consider the stain resistance and weather resistance of the coating, and the waterproof performance cannot meet the requirements in addition.
[0005] In summary, single-function heat-insulating coatings have their own advantages and disadvantages. Therefore, a composite heat-insulating coating with multiple heat-insulating mechanisms is developed, which integrates three functions of heat resistance, reflection and radiation. Thin-layer multi-functional thermal insulation coatings with high emissivity are the development trend of building thermal insulation coatings in the future, but the research on the above coatings has not been reported at home and abroad.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0039] First, weigh 50 grams each of nano-powder (titanium dioxide, nano-titanium dioxide-coated hollow glass microspheres, nano-titanium dioxide-coated hollow ceramic microspheres, nano-antimony-doped tin dioxide (ATO)), 400 grams of water, and 100 grams of ethanol , 100 grams of isopropanol, 100 grams of n-butanol, 100 grams of propylene glycol methyl ether acetate and 1 gram of dispersant, then water, ethanol, isopropanol, n-butanol and propylene glycol methyl ether acetate are added in the disperser, and then , then add a dispersant, and finally add nano-powder, after dispersing for 2 hours, you can get 1001 grams of nano-slurry with good dispersion, and the solid content in the slurry is about 30%;

[0040] Then take by weighing 7500 grams of synthetic water-based resins prepared by polyurethane, 200 grams of film-forming aids, 100 grams of fiber brucite powder, 200 grams of coupling agents, 100 grams of defoamers, 100 grams of leveling agents and 100 grams of wetting agen...

Embodiment 2

[0042] First, weigh 50 grams each of nano-powder (titanium dioxide, nano-titanium dioxide-coated hollow glass microspheres, nano-titanium dioxide-coated hollow ceramic microspheres, nano-antimony-doped tin dioxide (ATO)), 300 grams of water, and 80 grams of ethanol , 80 grams of isopropanol, 80 grams of n-butanol, 80 grams of propylene glycol methyl ether acetate and 1 gram of dispersant, then water, ethanol, isopropanol, n-butanol and propylene glycol methyl ether acetate are added in the disperser, and then , then add a dispersant, finally add nano-powder, and disperse for 2 hours to obtain 1001 grams of nano-indium tin oxide slurry with good dispersibility, and the solid content in the slurry is about 40%;

[0043]Take by weighing 3000 grams of synthetic water-based resins prepared by each 1000 grams of epoxy resin, silicone acrylic resin, and pure acrylic resin, 200 grams of film-forming aids, 100 grams of fiber brucite powder, 200 grams of coupling agent, and 100 grams of ...

Embodiment 3

[0045] First, weigh 50 grams each of nano-powder (titanium dioxide, nano-titanium dioxide-coated hollow glass microspheres, nano-titanium dioxide-coated hollow ceramic microspheres, nano-antimony-doped tin dioxide (ATO)), 200 grams of water, and 60 grams of ethanol , 60 grams of isopropanol, 60 grams of n-butanol, 60 grams of propylene glycol methyl ether acetate and 2 grams of dispersant, then water, ethanol, isopropanol, n-butanol and propylene glycol methyl ether acetate are added in the disperser, and then , then add dispersant, finally add nano powder, disperse for 2 hours, you can get 1001 grams of nano slurry with good dispersibility, the solid content in the slurry is about 50%;

[0046] Take by weighing 1400 grams of synthetic water-based resins prepared by each 350 grams of silicone acrylic resin, ammonium polyphosphate, melamine, and pentaerythritol, 100 grams of film-forming aids, 50 grams of fiber brucite powder, 50 grams of coupling agents, and 50 grams of defoame...

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Abstract

The invention relates to a waterborne heat-insulating flame-retardant multifunctional nano coating and a preparation method thereof. The coating consists of the following components in part by weight: 48 to 52 parts of waterborne resin and 30 to 50 parts of nano pigment fillers (nano titanium dioxide, nano titanium dioxide-coated hollow glass microspheres, nano titanium dioxide-coated hollow ceramic microspheres and nano antimony-doped tin dioxide (ATO) particles), size and auxiliary materials such as film-forming additive and coupling agent. The preparation method includes the steps that: the nano fillers and the size are first dipped into the waterborne resin, the auxiliary materials are then sequentially added and stirred, and thereby the heat-insulating flame-retardant multifunctional nano coating is obtained. The processing technique is simple, the component proportion is reasonable, and the prepared coating has the advantages of high heat resistance, high reflectivity, high radiative heat conductivity, certain fire resistance, high-efficient heat insulation, excellent mechanical and chemical properties, environment-friendliness, stain resistance, flame retardance and energy saving. The coating can be coated on outside facilities such as outer walls and building roofs.

Description

technical field [0001] The invention relates to a water-based heat-insulating and flame-retardant multifunctional nano-coating and a preparation method thereof. The invention belongs to the technical field of nanometer functional coatings. Background technique [0002] my country's building thermal insulation coatings began to be developed and applied in the late 1980s. At that time, thermal insulation coatings for some irregularly shaped high-temperature pipes and equipment surfaces were mainly developed. The products put into use include "coated composite silicate thermal insulation material", "composite silicate thermal insulation coating", "magnesium silicate thermal insulation material", "rare earth thermal insulation coating" and so on. Because this type of coating needs to be resistant to high temperatures, it is generally not possible to use organic base materials, but to use inorganic silicate materials that can withstand a certain temperature, such as cement and w...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09D175/04C09D163/00C09D133/00C09D7/12C09D5/00C09D5/18
Inventor 陶勇杨金三李妮龚斌琳胡伟张明
Owner 长沙新凯化工有限公司
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