Preparation method of sewage corrosion and scale inhibitor
A technology for corrosion and scale inhibitor and sewage, which is applied in the field of preparation of sewage corrosion and scale inhibitor, can solve the problems of low scale inhibition rate, low elution rate of heavy metal ions and high corrosion rate of sewage corrosion and scale inhibitor, and achieves Good biodegradability, good dehydration performance, good heat resistance effect
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Embodiment 1
[0027] The first step: weighing according to the ratio of parts by mass: 100 parts of reverse osmosis water, 16 parts of ammonium persulfate, 6 parts of perchloric acid, 4 parts of phosphorus trichloride, 5 parts of sodium sulfonate, and methyl benzotriazole 3 parts, 5 parts of expanded graphite, 8 parts of disodium hydroxyethylene diphosphonate, 10 parts of dimethylamine, 15 parts of acrylic acid, 30 parts of acrylamide, 7 parts of zinc chloride, 8 parts of ammonium carbonate, lignosulfonic acid 3 parts sodium, 1 part isopropanol.
[0028] Step 2: Dry the expanded graphite, sodium sulfonate and zinc chloride in a constant temperature drying oven at 80°C for 35 minutes, then put them into the grinder and grind them for 30 minutes, and roast them at 600°C for 10 minutes after the grinding is complete. .
[0029]The third step: the roasted product is put into the reaction with a thermometer, heating device, reflux condenser and agitator with reverse osmosis water, phosphorus tr...
Embodiment 2
[0033] The first step: weighing according to the ratio of parts by mass: 100 parts of reverse osmosis water, 20 parts of ammonium persulfate, 10 parts of nitric acid, 8 parts of phosphorus trichloride, 15 parts of sodium sulfonate, 5 parts of tolyl benzotriazole , 25 parts of expanded graphite, 12 parts of disodium hydroxyethylene diphosphonate, 20 parts of dimethylamine, 25 parts of acrylic acid, 50 parts of acrylamide, 11 parts of zinc chloride, 10 parts of ammonium carbonate, 7 parts of sodium lignosulfonate Parts, 5 parts of isopropanol.
[0034] Step 2: Dry the expanded graphite, sodium sulfonate and zinc chloride in a constant temperature drying oven at 100°C for 45 minutes, then put them into the grinder and grind them for 40 minutes, and roast them at 700°C for 30 minutes after the grinding is complete .
[0035] The third step: the roasted product is put into the reaction with a thermometer, heating device, reflux condenser and agitator with reverse osmosis water, ph...
Embodiment 3
[0039] The first step: weighing according to the ratio of parts by mass: 100 parts of reverse osmosis water, 18 parts of ammonium persulfate, 8 parts of hydrogen peroxide, 6 parts of phosphorus trichloride, 10 parts of sodium sulfonate, 4 parts of tolyl benzotriazole , 15 parts of expanded graphite, 10 parts of disodium hydroxyethylene diphosphonate, 15 parts of dimethylamine, 20 parts of acrylic acid, 40 parts of acrylamide, 9 parts of zinc chloride, 9 parts of ammonium carbonate, 5 parts of sodium lignosulfonate 3 parts, 3 parts of isopropanol.
[0040] Step 2: Dry the expanded graphite, sodium sulfonate and zinc chloride in a constant temperature drying oven at 90°C for 40 minutes, then put them into the grinder and grind them for 35 minutes, and roast them at 650°C for 20 minutes after the grinding is complete. .
[0041] The third step: the roasted product is put into the reaction with a thermometer, heating device, reflux condenser and agitator with reverse osmosis wate...
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