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Non-oxidized type compound bactericide for water treatment and preparation method thereof

A compound fungicide, non-oxidative technology, applied in the fields of fungicides, botanical equipment and methods, sterilization/microdynamic water/sewage treatment, etc. Degradation and other problems, to achieve the effect of efficient sterilization and algae killing, not easy to drug resistance, and simple synthesis method

Inactive Publication Date: 2015-04-01
SUZHOU YOUJUN ENVIRONMENTAL SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0010] In view of the above technical problems, the present application provides a non-oxidative compound bactericide for water treatment and its preparation method, which solves the problems of existing water treatment bactericidal agents with high toxicity, easy degradation, poor sterilization and algae killing effect, and easy to produce drug resistance. question

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] Weigh 100 parts of glutaraldehyde according to the ratio of parts by weight; 10 parts of acrylic acid-2-acrylamide-2-methylpropanesulfonic acid copolymer; 20 parts of tetradecyldimethylbenzyl ammonium chloride; 40 parts of bisphosphonic acid; 5 parts of water; 5 parts of PBTCA; 0.5 parts of butyl diphenylamine; 0.5 parts of sulfonic acid; 40 parts of polyol phosphonate; 20 parts of PESA; 15 parts of sodium; 1 part of bisbenzotriazole; 10 parts of sodium benzoate; 20 parts of acrylic acid-hydroxypropyl acrylate copolymer.

[0026] Put polyol phosphonate, bisbenzotriazole alcohol, sodium benzoate and acrylic acid-hydroxypropyl acrylate copolymer into a four-neck flask and heat to 30°C, stir for 60 minutes, add acrylic acid-2-acrylamide-2-methylpropane The sulfonic acid copolymer, hydroxyethylidene diphosphonic acid and PBTCA were heated to 40°C and reacted for 80 minutes.

[0027] Add glutaraldehyde and the remaining raw materials, heat up to 50°C, and compound for 2 hou...

Embodiment 2

[0030]Weigh 100 parts of glutaraldehyde according to the ratio of parts by weight; 30 parts of acrylic acid-2-acrylamide-2-methylpropanesulfonic acid copolymer; 80 parts of tetradecyldimethylbenzyl ammonium chloride; 60 parts of bisphosphonic acid; 45 parts of water; 25 parts of PBTCA; 2.5 parts of butyl diphenylamine; 2.5 parts of sulfonic acid; 60 parts of polyol phosphonate; 60 parts of PESA; 35 parts of sodium; 20 parts of bisbenzotriazole; 20 parts of sodium benzoate; 40 parts of acrylic acid-hydroxypropyl acrylate copolymer.

[0031] Put polyol phosphonate, bisbenzotriazole alcohol, sodium benzoate and acrylic acid-hydroxypropyl acrylate copolymer into a four-neck flask and heat to 40°C, stir for 90 minutes, add acrylic acid-2-acrylamide-2-methylpropane Sulfonic acid copolymer, hydroxyethylidene diphosphonic acid and PBTCA were heated to 50°C and reacted for 100 minutes.

[0032] Add glutaraldehyde and remaining raw materials, heat up to 70°C, and compound for 6 hours t...

Embodiment 3

[0035] Weigh 100 parts of glutaraldehyde according to the ratio of parts by weight; 15 parts of acrylic acid-2-acrylamide-2-methylpropanesulfonic acid copolymer; 40 parts of tetradecyl dimethyl benzyl ammonium chloride; 45 parts of bisphosphonic acid; 15 parts of water; 10 parts of PBTCA; 1 part of butyl diphenylamine; 1 part of sulfonic acid; 45 parts of polyol phosphonate; 30 parts of PESA; 20 parts of sodium benzoate; 5 parts of bisbenzotriazole; 12 parts of sodium benzoate; 25 parts of acrylic acid-hydroxypropyl acrylate copolymer.

[0036] Put polyol phosphonate, bisbenzotriazole alcohol, sodium benzoate and acrylic acid-hydroxypropyl acrylate copolymer into a four-neck flask and heat to 30°C, stir for 60 minutes, add acrylic acid-2-acrylamide-2-methylpropane Sulfonic acid copolymer, hydroxyethylidene diphosphonic acid and PBTCA were heated to 40°C and reacted for 85 minutes.

[0037] Add glutaraldehyde and remaining raw materials, heat up to 55°C, and compound for 3 hou...

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PUM

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Abstract

The invention discloses a non-oxidized type compound bactericide for water treatment and a preparation method thereof. The non-oxidized type compound bactericide is prepared by the steps of weighing glutaraldehyde, acrylic acid-2-acrylamide-2-methyl propane sulfonic acid copolymer, tetradecyl benzyl dimethyl ammonium chloride, etidronic acid, water, PBTCA, a polymerization inhibitor, sulfonic acid, polyol phosphonate ester, PESA, a dispersant, sodium tungstate, bitertanol, sodium benzoate and acrylic acid-hydroxy-propyl acrylate copolymer in parts by weight, and mixing uniformly. The product is 100% water-soluble, and has a sterilizing rate of 99.9-100% to escherichia coli, staphylococcus aureus, candida albicans, neisseria gonorrhoeae, penicillium notatum, aspergillus, saprophytic bacteria and salmonella; and the sterilizing rate is 98-100% after the bactericide is placed for one month at 50-60 DEG C, the sterilizing rate is 97.9-99.9% after the bactericide is placed for half a year at 40-50 DEG C, and the sterilizing rate is 97.5-99.5% after the bactericide is placed for 1-2 years at room temperature.

Description

technical field [0001] The application belongs to the field of environmental protection reagent technology, and in particular relates to a non-oxidative compound bactericide for water treatment and a preparation method thereof which is non-toxic and has a remarkable bactericidal effect. Background technique [0002] Water treatment bactericide is also called bactericide and algicide, sludge stripper or anti-sludge agent. A class of chemicals that can inhibit the growth of bacteria, algae and microorganisms in water to prevent the formation of microbial slime and cause harm to the system. Including oxidizing fungicides, such as chlorine, sodium hypochlorite, bleaching powder, ozone, chloramine, etc.; non-oxidizing fungicides, such as dodecyl dimethyl benzyl ammonium chloride, dodecyl dimethyl benzyl bromide Ammonium, dithiocyanomethane, etc.; heavy metal compounds, such as mercuric oxide, mercuric chloride, mercuric fluoride, etc.; slime fungicides, such as rosin amine, hydr...

Claims

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Application Information

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IPC IPC(8): A01N59/16A01N35/02A01P1/00A01P3/00A01P13/00C02F1/50A01N33/12
Inventor 夏戊君凌云陆赛君金可心陈亮程胜凌天阳陆鼎
Owner SUZHOU YOUJUN ENVIRONMENTAL SCI & TECH
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