Non-oxidized type compound bactericide for water treatment and preparation method thereof
A compound fungicide, non-oxidative technology, applied in the fields of fungicides, botanical equipment and methods, sterilization/microdynamic water/sewage treatment, etc. Degradation and other problems, to achieve the effect of efficient sterilization and algae killing, not easy to drug resistance, and simple synthesis method
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Embodiment 1
[0025] Weigh 100 parts of glutaraldehyde according to the ratio of parts by weight; 10 parts of acrylic acid-2-acrylamide-2-methylpropanesulfonic acid copolymer; 20 parts of tetradecyldimethylbenzyl ammonium chloride; 40 parts of bisphosphonic acid; 5 parts of water; 5 parts of PBTCA; 0.5 parts of butyl diphenylamine; 0.5 parts of sulfonic acid; 40 parts of polyol phosphonate; 20 parts of PESA; 15 parts of sodium; 1 part of bisbenzotriazole; 10 parts of sodium benzoate; 20 parts of acrylic acid-hydroxypropyl acrylate copolymer.
[0026] Put polyol phosphonate, bisbenzotriazole alcohol, sodium benzoate and acrylic acid-hydroxypropyl acrylate copolymer into a four-neck flask and heat to 30°C, stir for 60 minutes, add acrylic acid-2-acrylamide-2-methylpropane The sulfonic acid copolymer, hydroxyethylidene diphosphonic acid and PBTCA were heated to 40°C and reacted for 80 minutes.
[0027] Add glutaraldehyde and the remaining raw materials, heat up to 50°C, and compound for 2 hou...
Embodiment 2
[0030]Weigh 100 parts of glutaraldehyde according to the ratio of parts by weight; 30 parts of acrylic acid-2-acrylamide-2-methylpropanesulfonic acid copolymer; 80 parts of tetradecyldimethylbenzyl ammonium chloride; 60 parts of bisphosphonic acid; 45 parts of water; 25 parts of PBTCA; 2.5 parts of butyl diphenylamine; 2.5 parts of sulfonic acid; 60 parts of polyol phosphonate; 60 parts of PESA; 35 parts of sodium; 20 parts of bisbenzotriazole; 20 parts of sodium benzoate; 40 parts of acrylic acid-hydroxypropyl acrylate copolymer.
[0031] Put polyol phosphonate, bisbenzotriazole alcohol, sodium benzoate and acrylic acid-hydroxypropyl acrylate copolymer into a four-neck flask and heat to 40°C, stir for 90 minutes, add acrylic acid-2-acrylamide-2-methylpropane Sulfonic acid copolymer, hydroxyethylidene diphosphonic acid and PBTCA were heated to 50°C and reacted for 100 minutes.
[0032] Add glutaraldehyde and remaining raw materials, heat up to 70°C, and compound for 6 hours t...
Embodiment 3
[0035] Weigh 100 parts of glutaraldehyde according to the ratio of parts by weight; 15 parts of acrylic acid-2-acrylamide-2-methylpropanesulfonic acid copolymer; 40 parts of tetradecyl dimethyl benzyl ammonium chloride; 45 parts of bisphosphonic acid; 15 parts of water; 10 parts of PBTCA; 1 part of butyl diphenylamine; 1 part of sulfonic acid; 45 parts of polyol phosphonate; 30 parts of PESA; 20 parts of sodium benzoate; 5 parts of bisbenzotriazole; 12 parts of sodium benzoate; 25 parts of acrylic acid-hydroxypropyl acrylate copolymer.
[0036] Put polyol phosphonate, bisbenzotriazole alcohol, sodium benzoate and acrylic acid-hydroxypropyl acrylate copolymer into a four-neck flask and heat to 30°C, stir for 60 minutes, add acrylic acid-2-acrylamide-2-methylpropane Sulfonic acid copolymer, hydroxyethylidene diphosphonic acid and PBTCA were heated to 40°C and reacted for 85 minutes.
[0037] Add glutaraldehyde and remaining raw materials, heat up to 55°C, and compound for 3 hou...
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