Preparation method of dioscorea opposita thunb slime polysaccharide and resistant starch
A technology of resistant starch and yam, which is applied in the field of agricultural product processing, can solve the problems of less continuous and integrated production reports and low yield of resistant starch, and achieve good dimensional stability, short processing time and high purity. Effect
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Embodiment 1
[0031] Molecularly imprinted membrane preparation: With polypropylene membrane as the base membrane, 9 parts of molecularly imprinted template mucus polysaccharide of Chinese yam, 7 parts of functional monomer 4-vinylphenol, 3.5 parts of initiator benzoyl peroxide, 22 parts of crosslinking agent Sodium hexametaphosphate and 6 parts of porogen ethyl acetate are mixed to obtain a mixed solution, the polypropylene film is placed in the mixed solution, sealed with nitrogen gas, shaken in a water bath, dried in an oven at 30°C, and the volume ratio is 8:1.0 ethanol - elution with acetic acid solvent to remove the template molecules, that is, to obtain molecularly imprinted membranes.
[0032] Raw material pretreatment: take fresh Chinese yam, wash and peel, protect the color, slice, crush and homogenize with a tissue grinder, and then put the homogenate into a high-voltage pulsed electric field for extraction for 4.5 minutes, and the electric field strength is 23V / cm, the pulse ti...
Embodiment 2
[0038] Molecularly imprinted membrane preparation: Polypropylene membrane was used as the base membrane, 6 parts of molecularly imprinted template mucus polysaccharide of Chinese yam, 8 parts of functional monomer 4-vinylphenol, 4 parts of initiator benzoyl peroxide, 23 parts of cross-linking agent Sodium hexametaphosphate and 10 parts of porogen ethyl acetate are mixed to obtain a mixed solution, the polypropylene film is placed in the mixed solution, sealed with nitrogen gas, shaken in a water bath, and dried in an oven at 40°C, using ethanol with a volume ratio of 5:1.0 - elution with acetic acid solvent to remove the template molecules, that is, to obtain molecularly imprinted membranes.
[0039] Raw material pretreatment: take fresh Chinese yam, wash and peel, protect the color, slice, crush and homogenize with a tissue grinder, and then put the homogenate into a high-voltage pulsed electric field for extraction for 4 minutes, and the electric field strength is 20V / cm , t...
Embodiment 3
[0045] Molecularly imprinted membrane preparation: With polypropylene membrane as the base membrane, 8 parts of molecularly imprinted template mucus polysaccharide of Chinese yam, 10 parts of functional monomer 4-vinylphenol, 3 parts of initiator benzoyl peroxide, 20 parts of crosslinking agent Sodium hexametaphosphate and 7 parts of porogen ethyl acetate are mixed to obtain a mixed solution, the polypropylene film is placed in the mixed solution, sealed with nitrogen gas, shaken in a water bath, and dried in an oven at 38°C, using ethanol with a volume ratio of 9:1.0 - elution with acetic acid solvent to remove the template molecules, that is, to obtain molecularly imprinted membranes.
[0046] Raw material pretreatment: take fresh Chinese yam, wash and peel, protect the color, slice, crush and homogenize with a tissue grinder, and then put the homogenate into a high-voltage pulsed electric field for extraction for 5 minutes, and the electric field strength is 18V / cm , the pu...
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