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46 results about "Pyrifluquinazon" patented technology

Insecticide composition mixed with amides pesticide

The invention relates to insecticide composition in the field of pesticide mixture. The effective constituent of the insecticide composition mixed with amides pesticide is formed by mixture of novel pyrifluquinazon and one of four amide compounds, wherein the weight ratio of the novel pyrifluquinazon to the one of the four amide compounds is 1-90:90-1, and a preferential weight ratio is 1-45:60-5. Mass ration of the effective constituent of the insecticide composition mixed with amides pesticide is 1%-90% and a preferential mass ration is 5%-65%. The other composition of the insecticide composition mixed with amides pesticide is auxiliary component which is allowed and acceptable in pesticide. The insecticide composition mixed with amides pesticide can be prepared into emulsion in water, microemulsion, missible oil, suspending agents, wettable powder, micro-capsule suspending agents, and water dispersible granule. Due to the fact that the effective constituent of the insecticide composition is formed by the mixture of the pyrifluquinazon and the one of the amides compounds, the insecticide composition mixed with the amides pesticide can effectively prevent lepidopteron, such as plutella xylostella, beet armyworms, prodenia litura, cotton bollworms and mealybug and homoptera piercing-sucking mouthpart insects, such as aphids, aleyrodidaes, and leafhopper.
Owner:HAILIR PESTICIDES & CHEM GRP

Determining method of Pyrifluquinazon residual quantity

The invention relates to a determining method of Pyrifluquinazon residual quantity. The method comprises the following steps: homogeneously extracting residual Pyrifluquinazon in a sample by using acetonitrile or an acetonitrile solution containing 1% acetic acid; after dispersed purification of an extracting liquid by using an ethidene diamine-N-propyl silane (PSA) and octadecyl silane bonded phase (C18) matrix, detecting by gas chromatography-negative chemical ionization-chromatography (GC-NCI-MS); and establishing a corrected standard curve by using a blank substrate solution without to-be-detected pesticides, and quantifying by an external standard method. According to the method provided by the invention, the average recovery rate is 88.7-96.1%, the average relative standard deviation (RSD) is 4.7-6.9% and the detection limit is lower than 0.81 microg/kg. The determining method has the advantages of being simple and convenient to operate, quick, high in sensitivity, good in repeatability and accurate to qualify and quantify and can satisfy the technical requirement on safety detection of corresponding products in countries such as Korea, Japan and European Union, and thus a powerful technical support for guaranteeing the food safety of people in China and healthy development of foreign export trade is provided.
Owner:INSPECTION & QUARANTINE TECH CENT SHANDONG ENTRY EXIT INSPECTION & QUARANTINE BUREAU

A kind of assay method of pyrifluquinazon residue

The invention discloses a determination method for Pyrifluquinazon residual quantity. The method is mainly used for determining the content of residual Pyrifluquinazon in complex matrix food and agricultural products such as cereal grains and animal derived foods. Homogeneous extraction of residual Pyrifluquinazon in samples is carried out by using acetonitrile or an acetonitrile solution containing 1% of acetic acid, after purification and concentration with a C18 / PSA solid-phase extraction column, gas chromatography-negative chemical ion source-mass spectrometry (GC-NCI-MS) detection is carried out, a corrected standard curve is established by adopting a blank substrate solution which does not contain a pesticide to be tested, and quantization is carried out by an external standard method. According to the method, the average recovery rate is 75.1%-80.2%, the average relative standard deviation (RSD) is 4.8%-8.0%, the detection limit is lower than 2.77 microg / kg, and the determination method has the advantages of easiness, convenience and quickness in operation, good impurity removal effect, high sensitivity, marked characteristics, good repeatability, and accurate qualification and quantization. The determination method can meet the technical requirement of countries such as Japan, European Union and South Korea for 0.01mg / kg residue limit in corresponding food safety testing, namely 'uniform standard', so as to provide powerful technical support for guaranteeing the food safety of Chinese people and the healthy development of export trade.
Owner:INSPECTION & QUARANTINE TECH CENT SHANDONG ENTRY EXIT INSPECTION & QUARANTINE BUREAU
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