The invention relates to a guiding sieve plate float valve tower, belonging to a gas-liquid mass-transfer separation plant in chemical process. The guiding sieve plate float valve tower disclosed herein mainly comprises a tower body (1), a tower plate (2), a down-flow plate (7), a seal pan (9), etc., wherein the liquid inlet of the tower plate (2) is provided with a bubbling promoter (6), the plate surface of the tower plate is provided with a floating tongue (3), a guiding pore (4), a sieve pore (5) and a float valve. According to the invention, when the gas velocity is low, the float valve on the tower plate is not open, gas only passes through the guiding pore (4), the sieve pore (5) and the floating tongue (3); when the gas velocity increases to a certain level, the float valve is open, and the opening height of the float valve increases gradually with the increase of the gas velocity. The guiding sieve plate float valve tower disclosed herein has the advantages of simple structure, low cost, and greatly raised operation flexibility and separation efficiency.