Gas generating agent composition capable of lowering combustion temperature and keeping shape, preparation method, application and gas generator
The technology of a gas generating agent and composition, which is applied in the field of gas generators and automobile airbag gas generators, can solve the problems of short ignition delay period, high energy consumption, and can not be well maintained, and achieves increased packing density and thermal stability. Good performance, the effect of reducing the surface area
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[0064] The preparation method of the gas generant composition which reduces the combustion temperature and maintains the appearance of the present invention specifically comprises the following steps:
[0065] (1) Mix guanidine nitrate, basic copper nitrate, amidinourea copper nitrate, ammonium perchlorate and aluminum hydroxide to obtain the first material. Mix in mixing equipment, mixing time ≥ 5min; mixing equipment can be V-shaped mixer, three-dimensional multi-directional motion mixer, automatic lifting hopper mixer, vibrating mill, ribbon mixer or acoustic resonance mixer.
[0066] (2) Add water to the first material and carry out wet mixing for 20min-60min to obtain the second material, wherein the amount of water added is 6%-15% of the total mass of the first material, preferably distilled water. The equipment for wet mixing is a kneader or a mixer, for example, a horizontal kneader, a vertical kneader, a ribbon mixer or an acoustic resonance mixer can be selected.
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Embodiment 1
[0097] The gas generant composition comprises the following components in mass percent:
[0098]
[0099] After these components are weighed, they are compressed into discs with a diameter of 5mm and a thickness of 1.9mm by wet granulation and a rotary tablet press. The specific preparation method is: guanidine nitrate, basic copper nitrate, amidinourea copper nitrate, Ammonium chlorate and aluminum hydroxide are mixed by mixing equipment to obtain the first material; the first material is added to 10% distilled water for 30 minutes of wet kneading to obtain the second material, and the second material is passed through a 10-mesh screen to obtain the third material ; The third material is dried until the water content is less than 0.5% of the total mass of the third material, and the fourth material is obtained by passing through a 10-mesh screen again; adding talcum powder to the fourth material, and performing the process by a rotary tablet press Material forming.
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Embodiment 2
[0106] The gas generant composition comprises the following components in mass percent:
[0107]
[0108] After these components are weighed, they are compressed into discs with a diameter of 5mm and a thickness of 1.9mm by wet granulation and a rotary tablet press. The specific preparation method is: guanidine nitrate, basic copper nitrate, amidinourea copper nitrate, Ammonium chlorate and aluminum hydroxide are mixed by mixing equipment to obtain the first material; the first material is added to 15% distilled water for 40 minutes of wet kneading to obtain the second material, and the second material is passed through a 40-mesh screen to obtain the third material ; The third material is dried until the water content is less than 0.5% of the total mass of the third material, and the fourth material is obtained by passing through a 40-mesh screen again; adding talcum powder to the fourth material, and performing the process by a rotary tablet press Material forming.
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