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453 results about "Potassium perchlorate" patented technology

Potassium perchlorate is the inorganic salt with the chemical formula KClO₄. Like other perchlorates, this salt is a strong oxidizer although it usually reacts very slowly with organic substances. This, usually obtained as a colorless, crystalline solid, is a common oxidizer used in fireworks, ammunition percussion caps, explosive primers, and is used variously in propellants, flash compositions, stars, and sparklers. It has been used as a solid rocket propellant, although in that application it has mostly been replaced by the higher performance ammonium perchlorate. KClO₄ has the lowest solubility of the alkali metal perchlorates (1.5 g in 100 mL of water at 25 °C).

Environment protection coal-saving agent for cement vertical kiln

InactiveCN101463283AIncrease the amount of kilnAvoid hypoxiaSolid fuelsLiquid wasteCoal
The invention provides an environmental-friendly coal-saving agent for a cement shaft kiln, comprising the following raw materials by weight portion: 3-7 portions of a coal combusting low-temperature modifying agent, 2-6 portions of a compound sulphur-fixing agent, 0.5-0.96 portion of a combusting inductive agent, 3-7 portions of a raising agent, 56-96 portions of a combusting poising agent, and 5-15 portions of a highly-efficient sulphur-fixing agent. The coal combusting low-temperature modifying agent can be potassium permanganate, potassium chlorate, potassium perchlorate, sodium chlorate, sodium nitrate and the like; the compound sulphur-fixing agent can be sodium carbonate, calcium oxide and the like; the raising agent can be waste liquor of paper mill containing Na or/and Ca sulphonate and the like; and the combusting poising agent can be a chemical waste reducing substance containing sodium chloride and the like. The method solves the problems of environmental pollution and resource waste in the prior art, uses compatibility of multiple chemical raw material of 6-10 percent and chemical waste to prepare the coal-saving agent with small dosage and fast effect to be added to the production of the cement shaft kiln in trace quantity, and has the advantages of resource conservation by using waste, coal conservation and consumption reduction, and reduction of dust and SO2 discharge and environmental pollution.
Owner:陶小勇

Sulfur-free and pearlite-free firecracker reagent and preparation method thereof

The invention discloses a sulfur-free and pearlite-free firecracker reagent and a preparation method thereof. The reagent comprises the following mass components: 35-65 percent of A component and 35-65 percent of B component, wherein the A component comprises the mass compositions: a mixture formed by 20-50 percent of potassium perchlorate, 0-30 percent of potassium nitrate and 30-50 percent of barium nitrate and a complexing agent occupying 1-5 percent of the mixture, and the B component comprises the mass compositions: 50-80 percent of aluminum powder, 10-25 percent of charcoal powder and 10-25 percent of organic foaming powder. The burning rate of a firecracker prepared from the reagent is more than 98 percent, the sound level value is no less than 100dB and is no more than 140dB, the time the gas product pressure rises from 0.69MPa to 2.07MPa is 1.74ms, a pH value of the pyrotechnic composition is 5-9, the moisture is no more than 1.5 percent, the hygroscopicity is no more than 2.0 percent, the thermal stability is 75 DEG C plus / minus 2 DEG C, the firecracker has no decomposition phenomenon under the condition of 48h, the friction sensitivity is no more than 40 percent, and the impact sensitivity of the pyrotechnic composition is no more than 0 percent. The key is that the reagent reduces the environmental pollution without harm to human bodies and has great application prospect.
Owner:HUNAN VOCATIONAL INST OF SAFETY TECH +1

Novel preparation method of netaglinide oxazolone

The invention discloses a novel preparation method of netaglinide oxazolone shown in the formula (IV), which comprises the following steps: under the action of a catalyst A, enabling 3-fluorine-4-morpholine phenyl isocyanate shown in the formula (I) to react with (R)-epoxy chloropropane to obtain a compound (II), wherein the catalyst A is magnesium diiodide, magnesium dibromide, magnesium dichloride, magnesium perchlorate or magnesium trifluoromethanesulfonic acid; enabling the compound (II) to react with sodium azide to obtain a compound (III); reducing the compound (III) by hydrogenation, and then, acetylating the reduced compound (III) to obtain the compound (IV). In the invention, the low-cost and environment-friendly catalyst (Lewis acid magnesium) is used for catalyzing the cycloaddition reaction of the (R)-epoxy compound and the isocyanate to establish a mother nucleus structure of the netaglinide oxazolone by one step, thus the prepared netaglinide oxazolone has high stereoselectivity, does not need rigorous operation conditions, such as low temperature, no water, no oxygen and the like, has the advantages of moderate reaction conditions, simple and convenient operation, high utilization ratio of atoms, environment protection, low production cost and the like, and is suitable for industrialized production.
Owner:ZHEJIANG UNIV OF TECH

Manufacturing method for heating material uniformly heating used for thermal battery and application thereof

The invention relates to a manufacturing method for a heating material uniformly heating used for a thermal battery and application thereof. The method comprises: pouring analytical pure grade potassium perchlorate into a high-energy ball-milling cup, adding appropriate water to prepare a slurry, placing a zirconia ball, performing high-energy ball milling, and then putting ball-milled powders into a freeze dryer to dehydrate, and then crushing using a pulverizer to obtain ultrafine potassium perchlorate, pouring active iron powders into an inert atmosphere glove box, adding an inorganic potassium salt, and then mixing the active iron powders and the inorganic potassium salt using a physical or chemical method, to form potassium-containing iron powders; finally, mixing the ultrafine potassium perchlorate and the potassium-containing iron powders according to a certain ratio. The method is beneficial to widening a heating region of a heating material, to release heat more uniformly, thereby weakening thermal shock amount on a positive electrode material of a thermal battery in an initial working phase of the material, and improving utilization rate of the positive electrode materialof the battery.
Owner:航天江南集团有限公司 +1

Sulfur-smoke-free powder composition and preparation method thereof

InactiveCN103214322ADisadvantages of Avoiding Cryogenic DecompositionSolve the disadvantage of easy moisture absorptionExplosivesNitro compoundBarium nitrate
The invention discloses a sulfur-smoke-free firework powder composition and a preparation method thereof. According to the powder composition, potassium perchlorate and barium nitrate are used as oxidants, and a nitro-compound is used as a flammable agent, so that the safety and environment-friendliness of the firework production are greatly improved, the production cost of the firework powder is lowered, and various indexes are excellent through the detection. The preparation method of the sulfur-smoke-free firework powder composition is simple and mainly comprises the simple processes of mixing, pelletizing, drying and screening. According to the sulfur-smoke-free firework powder composition and the preparation method thereof disclosed by the invention, the problems that the conventional black powder is poor in safety, easy to absorb moisture, large in production risk and the like are solved. The sulfur-smoke-free firework powder composition has the advantages of having an emission effect better than that of black powder, achieving zero-exhaustion of sulfur dioxide and the like. The sulfur-smoke-free firework powder composition is extensively applicable to preparing firework propellant powder and 3-8-inch powder of large festive fireworks.
Owner:LIUYANG HELI HIGH TECH DEV CO LTD

Polishing solution for ultra-precise low-damage polish of large size diamond wafer and preparation thereof

The invention belongs to the superhard material polishing technical field and discloses polishing solution used for ultraprecise and low-damage polishing of a large-scale diamond wafer and a method for preparing the same. The method is characterized in that: oxidants with strong oxidbillity including chromium trioxide, ammonium persulphate, potassium permanganate, potassium dichromate, oxydol, potassium ferrate, potassium perchlorate and so on are adopted as main compositions; a proper amount of abrasive material is added for preparing the polishing solution; and micro-removal of surface material of the diamond wafer can be realized by means of chemical and mechanical composite action at normal temperature or low temperature. Moreover, the polishing effect of the polishing solution can be improved by addition of proper amount of catalyst, stabilizer, dispersant and so on as well. The polishing solution and the method have the advantages that: the polishing solution prepared has the advantages of high polishing efficiency, good polishing quality, good stability and so on; and the ultraprecise and low-damage polishing of the large-scale diamond wafer can be realized at the normal temperature or the low temperature.
Owner:DALIAN UNIV OF TECH

Blasting fuse of high-safety firecracker and preparation method thereof

The present invention relates to a preparation method of a safe firing cable of firecrackers. In the method, yarn is used as a carrier to infuse the following medicines, which are used raw materials, according to the following steps. The medicines comprise potassium perchlorate, potassium terephthalic acid, ammonium dichromate, polyethylene alcohol, moisture resistant agent, charcoal and sulfur. The method has the following steps: the potassium perchlorate, the potassium terephthalic acid, the ammonium dichromate, the charcoal, the sulfur and the polyethylene alcohol are arranged in a container according to the weight ratio; water with a certain proportion is added into the container; the mixture is stirred so that the medicines can be dissolved in the water; then the moisture resistant agent is added; and the mixture is mixed well; the yarn is infused in the container, taken out and then sent to a drying device to be dried; thus the safe firing cable can be prepared. In the method, the yarn is used as the carrier to infuse the medicines of the firing cable; the production is simple; the amount of the medicines is reduced; the method is safe; and the cost is reduced. The application of the potassium perchlorate has the advantages of low oxygen content, low decomposition temperature, excellent stability and low sensitivity. Thus the application of the potassium perchlorate is superior to the application of potassium chlorate. The firing cable solves the problems of storage, transportation and insecurity in use.
Owner:醴陵神马花炮有限公司

Fireworks product

The invention relates to a fireworks product, which comprises an outer cylinder with a sealed end, and an inner cylinder arranged in the outer cylinder, wherein the sealed end of the outer cylinder is provided with a small hole for an outer igniter cord; the inside of the outer cylinder is provided with propellant powder; the inner cylinder is provided with a small hole for an inner igniter cord; the inner igniter cord is contacted with the propellant powder; and the inside of the inner cylinder is provided with propellant powder. The fireworks product contains effective powder comprising red light powder, unpacking powder, igniting powder, sounding powder and black powder, wherein the red light powder comprises 43 percent of potassium perchlorate, 30 percent of powered alloy, 20 percent of strontium carbonate, 7 percent of hexachlorobenzene and 7 percent of phenolic resin; the unpacking powder comprises 50 percent of potassium perchlorate, 30 percent of powered alloy and 20 percent of aluminum powder; the igniting powder comprises 18 percent of potassium perchlorate, 7 percent of powered alloy, 12 percent of brimstone, 47 percent of potassium nitrate and 16 percent of charcoal; the sounding powder comprises 18 percent of powered alloy, 3 percent of brimstone, 5 percent of potassium nitrate, 52 percent of minium and 22 percent of copper oxide; and the black powder comprises 7 percent of potassium perchlorate, 6 percent of powered alloy, 9 percent of brimstone, 60 percent of potassium nitrate and 18 percent of charcoal. The fireworks product can generate flowery red light when set off, and simultaneously has high safety.
Owner:王生宝
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