Scaling powder for nickel-plating alloy soft soldering tin wire core and preparation method of scaling powder
A nickel-plated layer and flux technology, which is applied in the field of flux and its preparation for nickel-plated alloy solder wire cores, can solve problems such as low insulation resistance, low welding strength, and solder joint corrosion, and achieve surface insulation High resistance value, high tensile strength value, weak corrosion effect
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Embodiment 1
[0032] Composition of the present invention and component weight percentage content thereof are as follows:
[0033] (1) Hydrogenated rosin 74.0%
[0034] (2) Water-white rosin 7.0%
[0035] (3) Glutaric acid 2.0%
[0036] (4) Palmitic acid 4.0%
[0037] (5) Triethylenetetramine 3.0%
[0040] (8) Cyclohexylamine hydrobromide hydrochloride 1.5%
[0041] (9) Octylphenol polyoxyethylene ether 0.5%
[0042] (10) Benzotriazole 1.0%
[0043] (11) 2,6-di-tert-butyl-4-methylphenol (BHT) 1.0%
[0044] Preparation method: Add powdered zinc stearate, zinc chloride, glutaric acid, palmitic acid, cyclohexylamine hydrobromide hydrochloride, benzotriazole, BHT in the reactor according to the above weight ratio, and continuously stir 15 minutes; then slowly add the above mixed powder into the molten rosin, fully and continuously stir at 140±5°C for 20 minutes to obtain a light yellow liquid; when the temperature drops to ...
Embodiment 2
[0046] Composition of the present invention and component weight percentage content thereof are as follows:
[0047] (1) Water white rosin 73.0%
[0048] (2) Hydrogenated rosin 6.0%
[0049] (3) Adipic acid 3.0%
[0050] (4) Stearic acid 5.0%
[0051] (5) Diethylenetriamine 3.0%
[0052] (6) Bismuth chloride 1.0%
[0053] (7) Copper naphthenate 5.0%
[0054] (8) Dibromobutene ethanol 1.2%
[0055] (9) Alkylphenol polyoxyethylene ether 0.8%
[0056] (10) Imidazole 1.0%
[0057] (11) 2,6-di-tert-butyl-4-methylphenol (BHT) 1.0%
[0058] Preparation method: add copper naphthenate, bismuth chloride, adipic acid, stearic acid, bismuth chloride, dibromobutene alcohol, imidazole, BHT into the reactor according to the above weight ratio, and continuously stir for 20 minutes, then Slowly add the above mixed powder into the molten rosin, and stir continuously at 140±5°C for 20 minutes to obtain a light yellow liquid; when the temperature drops to 110°C, add diethylenetriamine an...
Embodiment 3
[0060] Composition of the present invention and component weight percentage content thereof are as follows:
[0061] (1) Water white rosin 66.0%
[0062] (2) Disproportionated rosin 9.8%
[0063] (3) Succinic acid 3.0%
[0064] (4) Lauric acid 7.0%
[0065] (5) Triethanolamine 3.5%
[0066] (6) Nickel chloride 0.8%
[0067] (7) Copper stearate 5.5%
[0068] (8) Hexadecyltrimethylammonium bromide 0.9%
[0069] (9) FC-4430 0.5%
[0070] (10) Piperazine 1.0%
[0071] (11) 2,6-di-tert-butyl-4-methylphenol (BHT) 1.0%
[0072] Preparation method: Add copper stearate, nickel chloride, succinic acid, lauric acid, piperazine, cetyltrimethylammonium bromide, and BHT into the reactor according to the above weight ratio, and continuously stir for 15 minutes; Then slowly add the above mixed powder into the molten rosin, fully and continuously stir at 140±5°C for 15 minutes to obtain a light green liquid; when the temperature drops to 110°C, then add triethanolamine and FC-4430 and...
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