A method for metallizing the surface of a ceramic substrate and a high-power LED base
A technology of LED base and ceramic substrate, which is applied in the parts of lighting device, cooling/heating device of lighting device, lighting auxiliary device, etc., can solve the problem of poor density and thermal conductivity of ceramic substrate, complex metallization process, and coating The problem of low bonding force with the ceramic substrate can achieve the effect of low cost, simple preparation process and good density.
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[0022] The preparation method of ceramic substrate of the present invention is illustrated as follows:
[0023] First prepare the glassy functional additive powder, select two or more of the oxides of A, A is aluminum, magnesium, silicon, barium, calcium, titanium, vanadium, chromium, manganese, iron, cobalt, nickel, copper , zinc, niobium, molybdenum, technetium, ruthenium, rhodium, palladium, silver, cadmium, tantalum, tungsten, rhenium, osmium, iridium, platinum, gold, indium, tin, antimony, lead or bismuth, two or more A The oxides are mixed in a certain proportion and dispersed by ball milling, for example, to prepare TiO 2 / CuO's glassy functional additive is TiO 2 Mix with CuO at a mass ratio of 1:1 or 1:2, the glassy functional additive of CaO / CoO is to mix CaO and CoO at a mass ratio of 1:1 or 1:2, Fe 2 o 3 The functional additive of / FeO / MgO is Fe 2 o 3 , FeO and MgO are mixed in a mass ratio of 1:1:1 or 1:2:1, FeO / SiO 2 / Fe 2 o 3 The glassy functional additi...
Embodiment 1
[0036] First prepare ceramic substrate, the concrete composition of described ceramic substrate is: the Al of 96wt% 2 o 3 Ceramic body, 0.5wt% CuO / TiO functional aid, wherein the mass ratio of CuO to TiO is 1:1, and 3.5wt% sintering aid, said sintering aid is Y 2 o 3 The mixture mixed with MgO at a mass ratio of 3:1. The green body is prepared by tape casting and sintered; the specific method is as follows, first, 100g of the above-mentioned ceramic substrate powder, 50g of solvent (mixed with ethanol and xylene at a mass ratio of 1:1), and dispersant (glyceryl trioleate) Put 3g into a ball mill for 12 hours of ball milling. After the ball milling, add 6g of binder (PVB) and 5g of plasticizer (polyethylene glycol and dibutyl phthalate in a mass ratio of 1:1) Mixing), and 0.1g defoamer for secondary ball milling, the ball milling time is 16h; after ball milling, filter and carry out vacuum degassing for 25min, then cast the obtained slurry under the tape casting machine, and...
Embodiment 2
[0038] In this example, the functional additive is CaO / CoO glassy powder accounting for 0.5wt% of the total weight of the ceramic substrate, wherein the mass ratio of CaO to CoO is 1:1; other processes are the same as in Example 1.
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