The invention discloses a preparation method of
chlorophyllin copper potassium salt, which comprises the following steps: (1) pretreatment of coarse silkworm excrement: screening,
winnowing, crushing and screening the coarse silkworm excrement to obtain purified silkworm excrement
powder; (2)
impurity removal by a water method and acidic
copper substitution: adjusting the pH value of the silkworm excrement
powder, heating, carrying out copperization, carrying out
water extraction and separating to obtain a precipitate; (3)
drying and
organic solvent extraction: performing
vacuum drying on the precipitate, and extracting and separating with an
organic solvent to obtain an
organic solvent extracting solution; (4)
saponification and
precipitation: carrying out vacuum concentration on the extracting solution, heating and saponifying with
potassium hydroxide, cooling and separating to obtain a
chlorophyll copper potassium salt crude product; and (5) washing and
drying the crude product: carrying out low-temperature washing, separation and
vacuum drying on the crude product by using an organic
solvent to obtain the
chlorophyllin copper potassium salt product. The method is easy to implement, convenient to operate, outstanding in product characteristic, easy in equipment
type selection and matching, high in product additional value and good in economic benefit, and the prepared potassium copper
chlorophyllin is high in yield, high in purity, high in sanitary safety, good in
solubility and low in cost and can be used for mechanically preparing the potassium copper chlorophyllin.