The invention discloses a preparation method of a
germanium selenide nano material and application of the
germanium selenide nano material. The preparation method of the
germanium selenide nano material comprises the following steps of: mixing GeI4 and
oleylamine, and sequentially carrying out magnetic stirring, vacuumizing, heating and heat preservation; and injecting
selenourea into the mixture of GeI4 and
oleylamine, refluxing the reaction mixture at a high temperature in an
inert gas environment, cooling to
room temperature, washing with
acetone,
alcohol and deionized water in sequence, and
drying to obtain
germanium selenide nanoparticles. According to the preparation method of the
germanium selenide nano material,
selenourea and GeI4 are subjected to a
redox reaction in an
oleylamine solvent at a high temperature to synthesize
germanium selenide nano particles, the germanium selenide nano particles are cooled to
room temperature, washed with
acetone,
alcohol and deionized water and dried to obtain the germanium selenide nano
particle material, and the whole preparation method is simple to operate, environment-friendly,
pollution-free and easy for industrial production. The germanium selenide nano material disclosed by the invention is applied to degradation of organic pollutants.