The invention discloses a
thermogravimetric analysis device and method for high-
humidity multi-component
atmosphere reaction
kinetics research, and belongs to the technical field of
thermogravimetric analysis instruments.The device comprises a reaction module, a
heating furnace, a weighing module, a gas distribution module and an analysis module; the reaction module is vertically arranged in the
heating furnace, the core is a reaction
pipe main body with an open lower part, and the side surface is connected with a gas inlet
pipe and a sampling
pipe from top to bottom; the weighing module is located below the reaction module and comprises a weighing balance, a
water cooling unit and a weighing supporting rod, and the
water cooling unit can control a
water vapor condensation area and stabilize the temperature of the balance; the gas distribution module can provide a multi-component reaction
atmosphere containing
water vapor with controllable concentration; the analysis module can detect
tail gas components in real time. The device can realize low gas-
solid mass transfer resistance, high-
humidity environment stable control, wide-particle-size sample measurement and rapid heating and cooling, and is suitable for high-
humidity multi-component
atmosphere gas-
solid reaction kinetic research in the fields of
combustion,
catalysis, adsorption and the like.