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117 results about "Cyflumetofen" patented technology

Cyflumetofen-containing insecticidal/acaricidal composition

The invention belongs to the field of pesticide insecticidal/acaricidal compositions, in particular to a cyflumetofen-containing insecticidal/acaricidal composition. Aiming at the practical problems that the using amount of a pesticide is large, cost is high, the resistance of pests is easy to generate due to reuse, and the like in the conventional singly used propargite and pyridaben for preventing and controlling harmful acarids, the invention provides the cyflumetofen-containing insecticidal/acaricidal composition. The technical scheme is that: the cyflumetofen-containing insecticidal/acaricidal composition comprises active ingredients A and B, wherein A is cyflumetofen, and B is one of the pyridaben and the propargite. The insecticidal/acaricidal composition has the advantages that: after the cyflumetofen is compounded with the propargite or the pyridaben, the insecticidal/acaricidal composition has obvious synergy and persistent prevention and control effects; the using amount of the pesticide is reduced, the residual amount of the pesticide on crops is reduced, and environmental pollution is abated; and the insecticidal/acaricidal composition is safe for human and animals and has high environmental compatibility, and the pesticide resistance of the harmful acarids is difficult to generate.
Owner:青岛泰生生物科技有限公司

Synthesis method of acaricide cyflumetofen intermediate p-tert-butyl phenylacetonitrile

The invention discloses a synthesis method of an acaricide cyflumetofen intermediate p-tert-butyl phenylacetonitrile, and belongs to the field of pesticide preparation. The synthesis method is characterized in that a reaction is performed on 4-tert-butyl halobenzene and cyanoacetate to obtain the p-tert-butyl phenylacetonitrile. A reaction process comprises the following steps: 1), under a protective gas condition, uniformly mixing the cyanoacetate, organic alkali and a solvent A, raising the temperature to 80-105 DEG C, controlling the pressure to be 3-5 atmospheric pressures, adding a solution of the tert-butyl halobenzene and a solvent B in three batches within 20-40 min, then controlling the reaction temperature to be 95-120 DEG C, controlling the reaction pressure to be 4-7 atmospheric pressures, carrying out a reaction for 1-3 hours, then adding deionized water, controlling the reaction temperature to be 130-150 DEG C, controlling the reaction pressure to be 6-9 atmospheric pressures, and continuing the reaction for 4-6 hours; 2), removing the solvents from a system by using a rotary evaporator, then transferring a remainder to water, adding a solvent C, stirring, layering, collecting an organic phase, drying by using a drying agent, then filtering, collecting a filtrate, distilling the filtrate under reduced pressure, and collecting a fraction with the temperature of 78-79 DEG C (0.1 torr) to obtain the p-tert-butyl phenylacetonitrile. According to the synthesis method, the steps are few, the yield is relatively high and the pollutant emission is less.
Owner:SHANDONG ACADEMY OF PESTICIDE SCI +1
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