The invention discloses a CsPbBr3 material purification method based on a solution method, and belongs to the technical field of
semiconductor material preparation. According to the method, firstly, CsBr is purified through an anti-
solvent recrystallization technology, and
impurity elements such as Li, Na, K, Rb, P, S, I and Cl are effectively removed; meanwhile, PbBr2 is purified by adopting an ultrasonic
water washing method, so that the content of elements such as Ca and Tl is remarkably reduced; then CsPbBr3 is purified through a
dimethyl sulfoxide-based inverse temperature
crystallization method, and
impurity elements such as Li, Mg, Ca, Sr, Ba, B, Al, Si, Se, Tl, Bi, Cr, Mn, Fe, Ni and Cu are successfully removed; finally, the CsPbBr3
raw material is further purified through a cooling
crystallization method based on a 48wt% HBr
aqueous solution, and residues of K, Rb, Ba, Zn, Tl, Bi, P, S, Cl and I elements are remarkably reduced. The method is simple in steps and controllable in process, and a feasible technical scheme worthy of popularization is provided for preparing the high-purity
semiconductor radiation detector.