A kind of anti-corrosion nano insulation felt and its preparation method and application
A corrosion-resistant and nano-technology, applied in the field of nano-insulation felt and its preparation, can solve the problems of poor corrosion resistance, weak ability to resist the corrosion and damage of surrounding media, and it is difficult for nano-insulation felt to meet production process requirements.
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[0040] The present invention provides a method for preparing the corrosion-resistant nano-insulation blanket described in the above technical solution, comprising the following steps:
[0041] Fully disperse water, surfactants, organic binders, inorganic nanopowders and rare earth oxides to obtain a slurry;
[0042] Soaking the fiber blanket base material in the slurry and fully compounding to obtain a wet blank;
[0043] The wet billet is calcined and hydrophobically treated in sequence to obtain a corrosion-resistant nanometer thermal insulation felt.
[0044] The invention fully disperses water, surface active agent, organic binder, inorganic nanometer powder and rare earth oxide to obtain slurry. In the present invention, the surfactant is preferably selected from the group consisting of alkyl trimethyl ammonium, polyoxyethylene alkyl amine, alkyl dimethyl betaine, sodium dodecylbenzenesulfonate, cetyltrimethylammonium ammonium bromide, alkyl dimethyl amine oxide, glycer...
Embodiment 1
[0062] Weigh 160g of water, pour it into a beaker and start stirring, then add 0.024g of cetyltrimethylammonium bromide, 3.6g of styrene-acrylic emulsion, stir for 5min, then add 44.8g of ultrafine titanium dioxide nanopowder, 0.256g of oxidation Neodymium, high-speed stirring and dispersion for 30 minutes; then 28g with a thickness of 10mm and a bulk density of 160Kg / m 3 Infiltrate the glass fiber needle-punched blanket with a fiber length-to-diameter ratio of 700 into the prepared slurry, and roll it through a roller press with a pressure of 3MPa and a rolling time of 15s; The surface is leveled on the leveling machine and the thickness is determined to be 10mm; the wet embryo of the fixed thickness is placed in a blast drying oven at 150°C for 12 hours; h; Dilute 4.84g of hydrogen-containing silicone oil emulsion and water at a ratio of 1:3 by volume and spray it on the surface of the calcined composite felt, then put the composite felt into a blast drying oven at 110°C for...
Embodiment 2
[0065] Weigh 160g of water, pour it into a beaker and start stirring, then add 0.024g of cetyltrimethylammonium bromide, 3.6g of styrene-acrylic emulsion, stir for 5min, then add 44.8g of potassium hexatitanate whiskers, 0.256g Lanthanum oxide, stirred at high speed to disperse for 30 minutes; then 28g with a thickness of 10mm and a bulk density of 160Kg / m 3 Infiltrate the quartz fiber needle-punched blanket with a fiber length-to-diameter ratio of 3000 into the prepared slurry, and roll it through a roller press with a pressure of 3MPa and a rolling time of 15s; The surface is leveled on the leveling machine and the thickness is determined to be 10mm; the wet embryo of the fixed thickness is placed in a blast drying oven at 150°C for 12 hours; h; Dilute 4.71g of hydrogen-containing silicone oil emulsion and water in a ratio of 1:3 by volume and spray it on the surface of the calcined composite felt, then put the composite felt into a blast drying oven and dry at 110°C for 3 h...
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