Unlock instant, AI-driven research and patent intelligence for your innovation.

A kind of anti-corrosion nano insulation felt and its preparation method and application

A corrosion-resistant and nano-technology, applied in the field of nano-insulation felt and its preparation, can solve the problems of poor corrosion resistance, weak ability to resist the corrosion and damage of surrounding media, and it is difficult for nano-insulation felt to meet production process requirements.

Active Publication Date: 2022-04-15
山东鲁阳浩特高技术纤维有限公司
View PDF4 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Ordinary nano-insulation blankets generally use glass fibers or ceramic fibers as the base material, and then compound them with silica materials, including precipitated silica, fumed silica, micro-silica, etc., the insulation effect is acceptable, but the resistance Poor corrosion performance, especially for strong acid, strong alkali and high salinity environment, it is easy to cause the felt body to be eroded and peeled off, which will seriously damage the felt body and cause great damage to the protected equipment and pipelines; in addition, ordinary nano-insulation Felt is mainly used for thermal insulation of large-scale industrial equipment and pipelines, but the thermal insulation or anti-corrosion effect of sensitive small parts such as centrifugal pumps, solenoid valves, etc. is not significant
[0003] With the continuous development of my country's economy and rapid technological progress, petrochemical, electric power, metallurgy, transportation, non-ferrous building materials and other industries have put forward higher requirements for the use of thermal insulation materials. The application standard has been improved. For example, in the process of producing polysilicon by the improved Siemens method, silicon powder and high-purity hydrogen chloride undergo high-temperature reactions in the synthesis furnace, which requires that the insulation materials for wrapping equipment and pipelines have excellent acid corrosion resistance; etching wafer processing The process requires the use of high-purity hydrogen fluoride, and the corrosion resistance requirements for equipment and pipelines are also quite high. Therefore, it is difficult to meet the production process requirements for nano-insulation blankets prepared solely with silica powder as a filling material.
[0004] The existing silica nano-insulation blanket is mainly used in the field of refractory heat preservation, and its ability to resist the corrosion and damage of the surrounding medium is relatively weak. , High salinity environment, such as chlor-alkali chemical equipment, polysilicon industry, wafer and chip processing industry, marine ships, transportation equipment and other fields are severely restricted

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0040] The present invention provides a method for preparing the corrosion-resistant nano-insulation blanket described in the above technical solution, comprising the following steps:

[0041] Fully disperse water, surfactants, organic binders, inorganic nanopowders and rare earth oxides to obtain a slurry;

[0042] Soaking the fiber blanket base material in the slurry and fully compounding to obtain a wet blank;

[0043] The wet billet is calcined and hydrophobically treated in sequence to obtain a corrosion-resistant nanometer thermal insulation felt.

[0044] The invention fully disperses water, surface active agent, organic binder, inorganic nanometer powder and rare earth oxide to obtain slurry. In the present invention, the surfactant is preferably selected from the group consisting of alkyl trimethyl ammonium, polyoxyethylene alkyl amine, alkyl dimethyl betaine, sodium dodecylbenzenesulfonate, cetyltrimethylammonium ammonium bromide, alkyl dimethyl amine oxide, glycer...

Embodiment 1

[0062] Weigh 160g of water, pour it into a beaker and start stirring, then add 0.024g of cetyltrimethylammonium bromide, 3.6g of styrene-acrylic emulsion, stir for 5min, then add 44.8g of ultrafine titanium dioxide nanopowder, 0.256g of oxidation Neodymium, high-speed stirring and dispersion for 30 minutes; then 28g with a thickness of 10mm and a bulk density of 160Kg / m 3 Infiltrate the glass fiber needle-punched blanket with a fiber length-to-diameter ratio of 700 into the prepared slurry, and roll it through a roller press with a pressure of 3MPa and a rolling time of 15s; The surface is leveled on the leveling machine and the thickness is determined to be 10mm; the wet embryo of the fixed thickness is placed in a blast drying oven at 150°C for 12 hours; h; Dilute 4.84g of hydrogen-containing silicone oil emulsion and water at a ratio of 1:3 by volume and spray it on the surface of the calcined composite felt, then put the composite felt into a blast drying oven at 110°C for...

Embodiment 2

[0065] Weigh 160g of water, pour it into a beaker and start stirring, then add 0.024g of cetyltrimethylammonium bromide, 3.6g of styrene-acrylic emulsion, stir for 5min, then add 44.8g of potassium hexatitanate whiskers, 0.256g Lanthanum oxide, stirred at high speed to disperse for 30 minutes; then 28g with a thickness of 10mm and a bulk density of 160Kg / m 3 Infiltrate the quartz fiber needle-punched blanket with a fiber length-to-diameter ratio of 3000 into the prepared slurry, and roll it through a roller press with a pressure of 3MPa and a rolling time of 15s; The surface is leveled on the leveling machine and the thickness is determined to be 10mm; the wet embryo of the fixed thickness is placed in a blast drying oven at 150°C for 12 hours; h; Dilute 4.71g of hydrogen-containing silicone oil emulsion and water in a ratio of 1:3 by volume and spray it on the surface of the calcined composite felt, then put the composite felt into a blast drying oven and dry at 110°C for 3 h...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
densityaaaaaaaaaa
densityaaaaaaaaaa
densityaaaaaaaaaa
Login to View More

Abstract

The invention provides a corrosion-resistant nano-insulation blanket and its preparation method and application. The nano-insulation blanket includes inorganic nano-materials, rare earth oxides, hydrophobic materials and fiber blanket substrates; the inorganic nano-materials are selected from nano-titanium oxide, nano-oxidized One or more of zirconium, nano-zirconium silicate, potassium hexatitanate whisker, ultra-fine alumina powder, ultra-fine aluminum hydroxide powder, carbon black, silicon carbide and silicon nitride; inorganic nano-materials account for nano-thermal insulation 25-40% of the felt mass; rare earth oxides are selected from europium oxide, gadolinium oxide, dysprosium oxide, ytterbium oxide, yttrium oxide, neodymium oxide, terbium oxide, cerium oxide, lanthanum oxide, samarium oxide, erbium oxide, praseodymium oxide, One or more of holmium, lutetium oxide, scandium oxide and thulium oxide. The present invention adopts a specific content of a specific type of inorganic nano-material and is doped with rare earth oxides, so that the nano-insulation blanket has better corrosion resistance, and can be widely used in the temperature-resistant and anti-corrosion requirements of sensitive components such as centrifugal pumps and solenoid valves.

Description

technical field [0001] The invention belongs to the technical field of thermal insulation blankets, in particular to a corrosion-resistant nano thermal insulation blanket and its preparation method and application. Background technique [0002] Ordinary nano-insulation blankets generally use glass fibers or ceramic fibers as the base material, and then compound them with silica materials, including precipitated silica, fumed silica, micro-silica, etc., the insulation effect is acceptable, but the resistance Poor corrosion performance, especially for strong acid, strong alkali and high salinity environment, it is easy to cause the felt body to be eroded and peeled off, which will seriously damage the felt body and cause great damage to the protected equipment and pipelines; in addition, ordinary nano-insulation Felt is mainly used for thermal insulation of large-scale industrial equipment and pipelines, but the thermal insulation or anti-corrosion effect of sensitive small pa...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): C04B35/80C04B35/46C04B35/462C04B35/622C04B41/84
CPCC04B35/46C04B35/462C04B35/622C04B41/009C04B41/4905C04B41/84C04B2235/3224C04B2235/5216C04B2235/3227C04B2235/522C04B2235/5228C04B2235/3225C04B2235/9607C04B2235/96C04B35/803C04B41/4543C04B41/0072
Inventor 鹿晓琨王振宇张成贺刘超任大贵
Owner 山东鲁阳浩特高技术纤维有限公司