The invention relates to a scanning electrochemical
microscope sample stage for testing a multi-standard sample strip
electrolytic cell. The sample stage is formed by a Teflon carrier plate (the
electrolytic cell at the upper end) and a U-shaped support. The left end wall and the right end wall of the
electrolytic cell are respectively provided with a round hole for placing a counter
electrode anda
reference electrode respectively. The U-shaped support is fixed by screws with the carrier plate. Cylindrical small rods are riveted into the carrier plate in the
positive direction and the negative direction of the X-axis and the
positive direction of the Y-axis. The bottom surface is provided with a circular groove, the carrier plate at the center of the electrolytic
cell is provided with a circular hole and the circular groove, a rubber
gasket is placed in the groove, a
test sample is placed on the rubber
gasket, and then a
metal pressing piece is placed. Bolts on the U-shaped support are adopted for fixation, and a probe is used for scanning the sample at the circular hole. The sample stage is simple and quick in
sample preparation, convenient to remove and capable of testing multi-
standard samples under the premise that the
sample integrity is maintained. The tested sample can be reused for other
test analysis, the application field of the SECM is expanded, and the utilizationrate is improved.