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149results about How to "Improve rinsing efficiency" patented technology

A process for extracting uranium by ion exchange method with water closed loop

The invention provides a process for extracting uranium by the ion exchange method of water closed-circuit circulation, which first uses an acidic leaching agent to leach uranium ore; then uses a weakly basic anion exchange resin to perform ion exchange adsorption on the leaching solution to obtain a uranium-loaded resin and an adsorption tail liquid; leaching the loaded uranium resin, and recovering uranium products from the leaching liquid. It processes the loaded uranium resin according to the following steps: (1) wash the loaded uranium resin with an alkaline solution with a total carbonate or bicarbonate concentration of 0.5-1.5 mol / L; (2) wash the loaded uranium resin The resulting qualified uranium-containing eluting liquid is precipitated with NaOH; all the precipitated mother liquid is cooled by a refrigerator to remove sulfate and then returned to prepare eluent. The invention improves the traditional ion exchange uranium extraction process, that is, does not introduce chloride radicals or nitrate radicals in the leaching process of the uranium-loaded anion exchange resin, avoids adverse effects on the process flow, and realizes closed circuit circulation of process water at the same time, thereby achieving environmental protection requirements.
Owner:BEIJING RESEARCH INSTITUTE OF CHEMICAL ENGINEERING AND METALLURGY

Tunnel type continuous washing machine

The invention relates to a tunnel type continuous washing machine, and belongs to the field of washing equipment. The tunnel type continuous washing machine comprises a pre-washing area, a main washing area, a rinsing area and an after-treatment area, wherein a dewatering area is inserted between the main washing area and the rinsing area and comprises an inner barrel and an outer barrel; two panels are respectively fixed at an inlet and an outlet of the inner barrel; an inlet supporting steel ring and an outlet supporting steel ring are respectively fixed on surfaces, which are not fixed on the inner barrel, of the inlet panel and the outlet panel; the inlet supporting steel ring, the outlet supporting steel ring and the inner barrel are integrated; an optional one of the inlet supporting steel ring and the outlet supporting steel ring is connected with an external driving device; a conveying screw plate is fixed in the inner barrel; a through hole is formed in the inner wall of the inner barrel; and the inner barrel of the dewatering area is driven by an independent motor to rotate. By using the tunnel type continuous washing machine, the rinsing efficiency can be effectively improved; water consumed during rinsing is reduced; resources are saved; dewatered cloth grasses are easily rinsed cleanly; and a washing effect is obviously improved.
Owner:SHANGHAI WEISHI MACHINERY

Compound eluting agent for repairing organic matter and heavy metal compound contaminated soil, leaching method of compound eluting agent and eluting agent recycling process

The invention discloses an eluting agent for repairing organic matter and heavy metal compound contaminated soil, an eluting method of the compound eluting agent and an eluting agent recycling method,wherein the eluting agent is prepared by compounding Tween 80 and EDTA. The eluting method comprises the following steps: adding the eluting agent into the contaminated soil, oscillating, mixing, centrifugally separating an eluting solution, adding the compound eluting agent solution again into the soil subjected to first-time eluting, performing secondary elution, and repeating for four times. The eluting agent recycling method comprises the following steps: transferring the separated eluting solution into a photoelectric recovery device, adding sodium persulfate and sodium sulfate electrolytes, turning an ultraviolet lamp and a power supply for photoelectric treatment for 2.5 hours to selectively degrade organic matters in the eluting solution and recover heavy metals. The compound solution of the Tween 80 and EDTA-2 Na is used, a plurality of times of continuous eluting are carried out, a photoelectric synergistic persulfate method is adopted to regenerate the eluting agent, and the organic matter and heavy metal compound contaminated soil can be effectively repaired synchronously. The method has the characteristics of simple process, convenience operation, short time consumption, high efficiency and the like.
Owner:WUHAN UNIV

Method for preparing high-activity double-effect seed crystals from metatitanic acid

The invention discloses a method for preparing high-activity double-effect seed crystals from an intermediate product, namely metatitanic acid, of titanium dioxide. The method comprises the following steps of: with metatitanic acid as a raw material, preparing clear titanium sulfate liquid, cooling the clear titanium sulfate liquid, adding a diluent of the clear titanium sulfate liquid to alkaline liquor, controlling pH value to 7.5-9.0, filtering and washing the obtained product, carrying out secondary washing on the washed product, carrying out acid dissolving on hydrofluoric acid and hydrochloric acid for short time under the lower temperature to obtain the high-activity double-effect seed crystals with hydrolyzed seed crystal performance and calcined seed crystal performance. According to the invention, the required titanium source is from the intermediate product produced from the titanium dioxide powder, therefore the method has low cost and production stability; in seed crystals, non-rutile promoted seed crystals and rutile promoted seed crystals are appropriate in proportion and have dual effects of hydrolyzed seed crystals and calcimined seed crystals; when the method is used for titanium dioxide production, calcined seed crystals are unnecessary to be additionally produced, the working procedure of adding the calcined seed crystals in the bleaching process is reduced, the bleaching time is shortened, and the rinsing efficiency is improved at the same time. The seed crystals prepared by using the method disclosed by the invention have high activity, excellent performance and capability of meeting hydrolyzing and calcining requirements just by adding 2 % of seed crystals.
Owner:SICHUAN LOMON TITANIUM IND CO LTD

Washing system for removing lead in polluted soil

The invention discloses a washing system for removing lead in polluted soil. The washing system comprises ionic liquid containing choline chloride and urea and oxalic acid. A preparation method of the washing system comprises the following steps that the urea and the choline chloride are weighed correspondingly, subjected to vacuum drying, mixed evenly, and heated and stirred for 0.5 h in an oil bath at the temperature of 100 DEG C, and colorless and thick liquid, namely ionic liquid with the choline chloride and the urea, is obtained; and finally the oxalic acid and the ionic liquid with the choline chloride and the urea are fully and evenly mixed, so that the washing system is obtained. According to a use method of the washing system, the polluted soil is taken and added into the washing system for removing the lead in the polluted soil, mixing and vibration washing is carried out, and then remediation of the lead polluted soil is finished. The washing system for removing the lead in the polluted soil has the advantages of being low in cost, environmentally friendly, easy to prepare, efficient and the like, the washing efficiency is improved through the synergistic effect of the eutectic ionic liquid and the organic acid, and the washing system can be applied to treatment of soil in mining areas, and has good application prospects.
Owner:YUNNAN MINZU UNIV

Method for extracting uranium by using ion exchange fixed tower under alternate Ph condition

The invention relates to a method for extracting uranium by using an ion exchange fixed tower, in particular to a method for extracting uranium by using an ion exchange fixed tower under the alternate Ph condition. The method comprises the steps of absorbing uranium by barren resin and eluting the uranium-carried resin to obtain uranium, wherein the step of eluting the uranium-carried resin to obtain uranium also comprises the following stages of elution neutralization, qualified liquid elution, first barren elution and second barren elution. In the stage of elution neutralization, an alkali eluent is used to neutralize residual acid in the uranium-carried resin, and the feeding mode is lower liquid feeding; in the stage of qualified liquid elution, the feeding mode is upper liquid feeding; in the stage of first barren elution, the feeding mode is upper liquid feeding, and the effluent liquid is a first barren solution; and in the stage of second barren elution, the feeding mode is upper liquid feeding, and the effluent liquid is a second barren solution. The invention increases elution efficiency and shortens elution volume by dividing the step of eluting the uranium-carried resin to obtain uranium into the stages of elution neutralization and qualified liquid elution and by respectively using the upper liquid feeding mode and the lower liquid feeding mode.
Owner:BEIJING RESEARCH INSTITUTE OF CHEMICAL ENGINEERING AND METALLURGY
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