The invention provides a preparation method for extracting bamboo reed
cellulose and MXene composite regenerated fibers based on oxidation-ultrasonic
coupling, and belongs to the field of
biomass-based functional
fiber materials.The preparation method comprises the steps that after bamboo reed raw materials are cooked, the pH value of a
system is adjusted, the liquid carrying rate is controlled, oxidation and ultrasonic pretreatment is conducted, the raw materials are purified, and the bamboo reed
cellulose and MXene composite regenerated fibers are obtained; bamboo reed
cellulose is obtained; a composite
solution system is adopted for dissolving the
spinning solution, and a uniform
spinning solution is prepared; the preparation method comprises the following steps: uniformly dispersing MXene in a
spinning solution in proportion, and preparing the bamboo reed-based MXene composite
regenerated cellulose fiber by taking a
buffer solution as a coagulating bath and adopting wet spinning. The invention solves the problems of
high energy consumption, large
reagent dosage, low yield and easy damage of cellulose structure in the existing bamboo reed cellulose extraction, and the problems of insufficient cellulose purity, poor MXene
dispersity, poor interfacial compatibility, poor spinning solution stability and forming effect and the like in the MXene composite regenerated
fiber preparation.