The invention relates to a small-tube-
diameter carbon nano-tube purification device and a small-tube-
diameter carbon nano-tube purification method. The small-tube-
diameter carbon nano-tube purification device comprises a reaction kettle, a
heat exchanger, a secondary acid
storage tank, a
diffusion dialysis device and a pressure filter. The small-tube-diameter carbon nano-tube purification method comprises the following steps: adding acid liquid and small-tube-diameter carbon nano-tube
raw material powder into the reaction kettle to react, introducing a small-tube-diameter carbon nano-tube solution obtained after reaction into the pressure filter for pressure
filtration, performing water-washing and
drying on a small-tube-diameter carbon nano-tube in the pressure filter to obtain a small-tube-diameter carbon nano-tube finished product, introducing waste acid liquid filtered by virtue of pressure
filtration into the
diffusion dialysis device for purification, and introducing the purified acid liquid into the secondary acid
storage tank; introducing acid mist generated in the reaction kettle into the
heat exchanger for cooling, and introducing the cooled acid liquid into the secondary acid
storage tank; performing concentration adjustment on the acid liquid in the secondary acid storage tank and then introducing the acid liquid into the reaction kettle. According to the small-tube-diameter carbon nano-tube purification device and method disclosed by the invention, the acid mist generated in a purification process is cooled and recycled, and the waste acid liquid generated in a production process is purified and recycled, so that the environment
pollution caused by the acid mist and the waste acid liquid can be reduced, and the production cost can be reduced.