The invention discloses a method for recovering acid in chemical
polishing liquid cleaning water by combining resin adsorption and
diffusion dialysis, belongs to the technical field of
industrial waste liquid resourceful treatment, and aims to solve the technical problem that the purity and the concentration of purified acid recovered in the prior art need to be further improved. The method specifically comprises the following steps: introducing chemical
polishing liquid cleaning water into an adsorption unit to obtain a
dilute acid solution, introducing the
dilute acid solution into a
concentration unit for concentration to obtain recycled acid meeting the recycling standard of a chemical
polishing tank, and after the adsorption unit achieves adsorption saturation, passing through a cleaning unit and then introducing into a
desorption unit for
desorption to obtain the recycled acid meeting the recycling standard of the chemical polishing tank. The adsorption liquid is introduced into a
diffusion dialysis unit, purified acid and residual liquid are obtained, the finally obtained purified acid is circularly used for
desorption treatment, and the residual liquid is directly discharged after being neutralized and filtered. The preparation of the cation adsorption resin is combined with the process flow, so that the purity and the concentration of the recovered acid are improved.