The utility model relates to a kind of for preparing
flumetralin crystal form I production device, including high-pressure transformation crystallizer, and
tap water import and feeding port are set on high-pressure transformation crystallizer;High-pressure transformation crystallizer is equipped with transformation crystallizer jacket outside, and is equipped with transformation crystallizer coil
pipe inside, high-pressure transformation crystallizer kettle bottom is connected with
discharge pipe,
discharge pipe is connected with suction filter tank, suction filter tank lower liquid
discharge is connected with
mother liquor receiving tank,
mother liquor receiving tank is connected with
vacuum pumping device, and
mother liquor receiving tank lower liquid discharge is connected with high-pressure transformation crystallizer by mother liquor
circulating pump;Hot water circulating kettle is set with heating jacket outside, and hot water circulating kettle is connected with
hot water supply pipe, and
hot water supply pipe is connected with coil
pipe water inlet pipe and transformation
crystallization lower outlet pipe respectively by hot water pump, and cooling hot water return pipe is connected with hot water circulating kettle.The device structure is simple, and water is transformed into
crystal by high-pressure transformation crystallizer, avoid traditional
solvent transformation
crystallization solvent residue, lead to in
drying temperature process
solvent can dissolve part
crystal form 1 and produce steady-state crystal form 2, help to improve the purity and yield of transformation
crystallization production, suitable for industrial production use.