A method for characterizing a sample containing at least one compound, preferably a biological sample comprising at least one
metabolite, is proposed. In a first process step, a three-dimensional first set of data is generated by analyzing the sample by using at least one time resolved separation technique (214) and at least
mass one resolved separation technique (216). The set of data comprises at least one
signal I as a function of a
mass variable over a first range of measurement (420) and of a
time variable over a second range of measurement (422). In a second process step, the first range of measurement (420) is divided into at least two
mass variable intervals (424). For each mass
variable interval (424), an extracted
signal is selected, wherein the extracted
signal is a function of the
time variable. In a third process step, the second range of measurement (422) is divided into at least one
time variable interval (426). At least one characteristic value is selected for each time
variable interval (426) and for each extracted signal. Thus, a characteristic sample profile is generated, which comprises the at least one characteristic value as a function of the respective time
variable interval (426) and of the respective mass variable interval (424).