The invention provides an olefine
aldehyde intermediate and a synthetic method thereof, and a synthetic method of conopomorpha sinensis sex
pheromone, and belongs to the field of compound synthesis. According to the synthesis method of the olefine
aldehyde intermediate, provided by the invention, 1, 5-pentanediol is taken as a
raw material, and the high-yield olefine
aldehyde intermediate is obtained through
transesterification, first oxidation reaction,
Wittig reaction and Sagsa oxidation reaction; the yield of the olefine aldehyde intermediate can be further improved by limiting a catalytic
system and an auxiliary agent of the Sagsa oxidation reaction. Results of the embodiment show that the synthesis method provided by the invention does not adopt
alkyne compounds, the yield of the product in the Sagassa oxidation reaction stage can reach 81%, the total yield of the obtained olefine aldehyde intermediate can reach 48.5%, the sex
pheromone of conopomorpha sinensis prepared by adopting the olefine aldehyde intermediate can reach 39.8%, and the yield is high.