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34results about How to "Achieving Oxidation Removal" patented technology

Fiber/CNT(carbon nano tube)/TiO2 three-dimensional recyclable efficient catalytic material, as well as preparation and application thereof

The invention relates to a fiber / CNT(carbon nano tube) / TiO2 three-dimensional recyclable efficient catalytic material, as well as preparation and application thereof. A three-dimensional continuous structure is constructed on the surface of textile fiber by CNTs, and surfaces of the CNTs are loaded with nano TiO2. Preparation comprises: soaking fiber in a dispersion liquid containing CNT compound TiO2 and polyethylene glycol 2000, lasting reaction for 2-4 h at 60-80 DEG C, drying, washing with water, repeating processes of soaking, drying and washing with water for 3-5 times, and obtaining the material. The fiber / CNT / TiO2 three-dimensional recyclable efficient catalytic material is low in cost, the preparation method is simple, requirements on equipment is are low, and the operability is good; a water treatment agent provided by the invention can remove high-concentration organic pollutants in water, is suitable for advanced treatment of various wastewater, protects the environment, avoids secondary pollution, and has the advantages of being antibacterial, removing odor, absorbing other heavy metal ions, and the like.
Owner:DONGHUA UNIV

Method of preparing green advanced water treatment chemicals with carbon nano-tube compounded pucherite

The invention relates to a method of preparing green advanced water treatment chemicals with carbon nano-tube compounded pucherite. The method comprises the steps: (1) sequentially performing carboxylation, amination modification, 2, 4, 6-trifluoro-5-chloro-pyrimidine modification to carbon nano-tubes to obtain reaction type carbon nano-tubes; (2) adding bismuth salt, a stabilizer, a template agent and the reaction type carbon nano-tubes to phosphate buffer solution and stirring for 30-60 minutes to form turbid liquid; dissolving metavanadate into the phosphate buffer solution, and then adding to the turbid liquid to form transparent solution; and (3) filtering and drying to obtain the green advanced water treatment chemicals with carbon nano-tube compounded pucherite. The preparation method is low in price, simple in preparation, low in requirement on equipment and good in operability; the water treatment chemicals are capable of removing high-concentration organic pollutants in water, applicable to advanced treatment for various waste water, environmental-friendly and no secondary pollution and have the advantages of sterilization, deodorization and capability of absorbing other heavy metal ions.
Owner:DONGHUA UNIV +1

Fiber/CNT(carbon nano tube)/BiFeO3 three-dimensional recyclable efficient catalytic material, as well as preparation and application thereof

The invention relates to a fiber / CNT(carbon nano tube) / BiFeO3 three-dimensional recyclable efficient catalytic material, as well as preparation and application thereof. A three-dimensional continuous structure is constructed on the surface of textile fiber by CNTs, and surfaces of the CNTs are loaded with nano BiFeO3. Preparation comprises: soaking fiber in a dispersion liquid containing CNT compound BiFeO3 and polyethylene glycol 2000, lasting reaction for 2-4 h at 60-80 DEG C, drying, washing with water, repeating processes of soaking, drying and washing with water for 3-5 times, and obtaining the material. The fiber / CNT / BiFeO3 three-dimensional recyclable efficient catalytic material is low in cost, the preparation method is simple, requirements on equipment is are low, and the operability is good; a water treatment agent provided by the invention can remove high-concentration organic pollutants in water, is suitable for advanced treatment of various wastewater, protects the environment, avoids secondary pollution, and has the advantages of being antibacterial, removing odor, absorbing other heavy metal ions, and the like.
Owner:DONGHUA UNIV +1

Preparation method of carbon nano tube composite bismuth molybdate environmentally friendly and deep water treatment agent

The invention relates to a preparation method of a carbon nano tube composite bismuth molybdate environmentally friendly and deep water treatment agent. The preparation method comprises the following steps: (1), carboxylation and amination modification are performed on a carbon nano tube and 2,4,6-trifluoro-5-chloro-pyrimidine is modified to prepare a reaction type carbon nano tube; (2), bismuth salt, a stabilizer, a template agent and the reaction type carbon nano tube are added into a phosphate buffer solution, and stirring is performed for 30 to 60 min, so as to form turbid liquid; molybdate is dissolved into the phosphate buffer solution, and then the phosphate buffer solution is added into the turbid liquid, so as to form a transparent solution; (3), the product is obtained after filtering and drying. The preparation method provided by the invention has the advantages that the cost is low, the preparation method is simple, requirements for equipment are low, and the maneuverability is excellent; the water treatment agent can be used for removing high concentration organic pollutants in water, is suitable for deep treatment on various wastewater, environmental protection and zero secondary pollution are achieved, and the water treatment agent is antibacterial, deodorant and can absorb other heavy metal ions and the like.
Owner:DONGHUA UNIV +1

Preparation method for environment-friendly advanced water treatment agent by combining carbon nano tube and ZnIn2S4

The invention relates to a preparation method for an environment-friendly advanced water treatment agent by combining a carbon nano tube and ZnIn2S4. The preparation method includes the steps that firstly, carboxylation, aminated modification and 2, 4, 6-trifluoro-5-chloropyrimidine modification are sequentially conducted on the carbon nano tube to obtain a reaction type carbon nano tube; secondly, the nano ZnIn2S4, a stabilizer, a template agent and the reaction type carbon nano tube are added into phosphate buffered saline to be stirred for 30 min-60 min to form turbid liquid; thirdly, the turbid liquid is filtered and dried to obtain the environment-friendly advanced water treatment agent. The preparation method is low in cost, simple, low in equipment requirement and good in operability. The water treatment agent can be used for removing high-concentration organic pollutants in water, is suitable for advanced treatment of various kinds of wastewater, environmentally friendly and free of secondary pollution and has the advantages of being antibacterial, deodorant, capable of adsorbing other heavy metal ions and the like.
Owner:DONGHUA UNIV +1

Fiber/CNT(carbon nano tube)/Ag3PO4 three-dimensional recyclable efficient catalytic material, as well as preparation and application thereof

The invention relates to a fiber / CNT(carbon nano tube) / Ag3PO4 three-dimensional recyclable efficient catalytic material, as well as preparation and application thereof. A three-dimensional continuous structure is constructed on the surface of textile fiber by CNTs, and surfaces of the CNTs are loaded with nano Ag3PO4. Preparation comprises: soaking fiber in a dispersion liquid containing CNT compound Ag3PO4 and polyethylene glycol 2000, lasting reaction for 2-4 h at 60-80 DEG C, drying, washing with water, repeating processes of soaking, drying and washing with water for 3-5 times, and obtaining the material. The fiber / CNT / Ag3PO4 three-dimensional recyclable efficient catalytic material is low in cost, the preparation method is simple, requirements on equipment is are low, and the operability is good; a water treatment agent provided by the invention can remove high-concentration organic pollutants in water, is suitable for advanced treatment of various wastewater, protects the environment, avoids secondary pollution, and has the advantages of being antibacterial, removing odor, absorbing other heavy metal ions, and the like.
Owner:DONGHUA UNIV +1

Preparation method for environment-friendly advanced water treatment agent by combining carbon nano tube and WO3

The invention relates to a preparation method for an environment-friendly advanced water treatment agent by combining a carbon nano tube and WO3. The preparation method includes the steps that firstly, carboxylation, aminated modification and 2, 4, 6-trifluoro-5-chloropyrimidine modification are sequentially conducted on the carbon nano tube to obtain a reaction type carbon nano tube; secondly, the nano WO3, a stabilizer, a template agent and the reaction type carbon nano tube are added into phosphate buffered saline to be stirred for 30 min-60 min to form turbid liquid; thirdly, the turbid liquid is filtered and dried to obtain the environment-friendly advanced water treatment agent. The preparation method is low in cost, simple, low in equipment requirement and good in operability. The water treatment agent can be used for removing high-concentration organic pollutants in water, is suitable for advanced treatment of various kinds of wastewater, environmentally friendly and free of secondary pollution and has the advantages of being antibacterial, deodorant, capable of adsorbing other heavy metal ions and the like.
Owner:DONGHUA UNIV +1

Method for preparing carbon nano tube composite SrFeO3 green deep water treatment agent

The invention relates to a method for preparing a carbon nano tube composite SrFeO3 green deep water treatment agent. The method comprises the following steps: (1) sequentially performing carboxylated and aminated modification and 2,4,6-trifluoro-5-chloropyrimidine modification on carbon nano tubes, thereby obtaining reactive carbon nano tubes; (2) adding nanometer SrFeO3, a stabilizer, a template agent and the reactive carbon nano tubes into a phosphate buffer solution, stirring for 30-60 minutes, and forming a turbid liquid; and (3) filtering and drying, thereby obtaining the product. The method disclosed by the invention is low in cost, simple in preparation method, low in equipment requirements and high in operability. Moreover, the water treatment agent disclosed by the invention can remove high-concentration organic pollutants in water, is suitable for deep treatment of various kinds of wastewater, is environment-friendly, does not cause secondary pollution and has the advantages of bacteria resistance, deodorization, capacity of adsorbing other heavy metal ions and the like.
Owner:DONGHUA UNIV +1

Preparation method for laminated aluminum matrix composite material without residual pyrolytic carbon

The invention relates to a preparation method for a laminated aluminum matrix composite material without residual pyrolytic carbon. The preparation method for the laminated aluminum matrix composite material without residual pyrolytic carbon disclosed by the invention aims at solving the problems that in an existing laminated aluminum matrix composite material preparation process, a thickness control method is complex, thickness control is inaccurate, cost is high, interface combination performance of the laminated composition material is weak, a prefabricated body is prone to collapsing in acomposite material preparation process, and the prepared laminated aluminum matrix composite material has residual pyrolytic carbon. The preparation method comprises the steps: 1, weighing materials;2, preparing SiC slurry; 3, tape casting SiC nanowire raw sheets; 4, preparing the prefabricated body; 5, degreasing, preheating and removing residual pyrolytic carbon; 6, impregnating molten aluminum. According to the preparation method disclosed by the invention, oxidizing and removing the pyrolytic carbon is achieved, preheating time is shortened, the thickness control method is simple, the thickness is accurate, a technology is simple, aluminum foils can separate SiC nanowire layers and further can ensure integrity of a laminated structure of the composite material, and interface combination of the composite material is excellent.
Owner:HARBIN INST OF TECH

Fiber/CNT(carbon nano tube)/BiVO4 three-dimensional recyclable efficient catalytic material, as well as preparation and application thereof

The invention relates to a fiber / CNT(carbon nano tube) / BiVO4 three-dimensional recyclable efficient catalytic material, as well as preparation and application thereof. A three-dimensional continuous structure is constructed on the surface of textile fiber by CNTs, and surfaces of the CNTs are loaded with nano BiVO4. Preparation comprises: soaking fiber in a dispersion liquid containing CNT compound BiVO4 and polyethylene glycol 2000, lasting reaction for 2-4 h at 60-80 DEG C, drying, washing with water, repeating processes of soaking, drying and washing with water for 3-5 times, and obtaining the material. The fiber / CNT / BiVO4 three-dimensional recyclable efficient catalytic material is low in cost, the preparation method is simple, requirements on equipment is are low, and the operability is good; a water treatment agent provided by the invention can remove high-concentration organic pollutants in water, is suitable for advanced treatment of various wastewater, protects the environment, avoids secondary pollution, and has the advantages of being antibacterial, removing odor, absorbing other heavy metal ions, and the like.
Owner:DONGHUA UNIV +1

Preparation method for environment-friendly advanced water treatment agent by combining carbon nano tube and ferric vanadate

The invention relates to a preparation method for an environment-friendly advanced water treatment agent by combining a carbon nano tube and ferric vanadate. The preparation method includes the steps that firstly, carboxylation, aminated modification and 2, 4, 6-trifluoro-5-chloropyrimidine modification are sequentially conducted on the carbon nano tube to obtain a reaction type carbon nano tube; secondly, molysite, a stabilizer, a template agent and the reaction type carbon nano tube are added into phosphate buffered saline to be stirred for 30 min-60 min to form turbid liquid, metavanadate is dissolved in phosphate buffered saline to be added into the turbid liquid, and a transparent solution is formed; thirdly, the transparent solution is filtered and dried to obtain the environment-friendly advanced water treatment agent. The preparation method is low in cost, simple, low in equipment requirement and good in operability. The water treatment agent can be used for removing high-concentration organic pollutants in water, is suitable for advanced treatment of various kinds of wastewater, environmentally friendly and free of secondary pollution and has the advantages of being antibacterial, deodorant, capable of adsorbing other heavy metal ions and the like.
Owner:DONGHUA UNIV +1

Fiber/carbon nanotube/SrTiO3 three-dimensional recyclable efficient catalytic material and preparation and application thereof

The invention relates to a fiber / carbon nanotube / SrTiO3 three-dimensional recyclable efficient catalytic material and preparation and an application thereof. A multifunctional carbon nanotube is characterized in that a three-dimensional continuous structure is built on the surface of textile fibers, wherein the surface of the multifunctional nanotube is loaded with nano-SrTiO3. A preparation method for the fiber / carbon nanotube / SrTiO3 three-dimensional recyclable efficient catalytic material comprises the following steps: dipping the fibers in polyethylene glycol 2000 dispersion liquid containing carbon nanotube composite SrTiO3 and reacting at the temperature of 60 to 80 DEG C for 2 to 4 hours; drying; washing with water; repeatedly dipping; drying and washing with water for 3 to 5 times to obtain the fiber / carbon nanotube / SrTiO3 three-dimensional recyclable efficient catalytic material. The preparation method provided by the invention is low in cost, is simple, and has low requirements on equipment and high operability. A water treatment agent provided by the invention can be used for removing high-concentration organic pollutants from water, is suitable for deeply treating various waste water, is environmental-friendly and free from secondary pollution, and has the advantages of antibacterial property, deodorization and capability of adsorbing other heavy metal ions and the like.
Owner:DONGHUA UNIV +1

Method and device for removal of atmospheric fine particles

ActiveCN108479254AStrengthen the condensation effectAchieve killCombination devicesGas treatmentIonEnvironmental chemistry
The invention discloses a method and device for removal of atmospheric fine particles. Air is introduced into a reaction chamber, and ultrasonic atomization humidification is carried out to enable rapid growth of fine particles, a pulsed corona discharge device generates negative ions and free radicals to make fine particles charged, coagulation is accelerated and heterogeneous reaction is carriedout; an aerosol is further introduced into a spiral generator, under the action of a centrifugal force, liquid drops constantly entrain, dissolve and scour fine particles in the airflow, and accumulated liquid flows back to form a liquid film, the wet deposition process of atmospheric fine particles is strengthened continuously, and finally PM2.5 flows out from the lower end of the spiral generator along with the liquid drops. The method and device provided by the invention utilize the hygroscopic growth characteristics of atmospheric fine particles and the natural sedimentation process to remove atmospheric fine particles, are simple and efficient, not only can realize efficient removal of PM2.5 from the air, but also can purify formaldehyde and other gaseous pollutants in the air, and also have the functions of inactivating bacteria and viruses in the air, humidifying the air and the like.
Owner:PEKING UNIV

A preparation method of carbon nanotube composite bismuth tungstate green deep water treatment agent

The invention relates to a preparation method for an environment-friendly advanced water treatment agent by combining a carbon nano tube and dibismuth tris. The preparation method includes the steps that firstly, carboxylation, aminated modification and 2, 4, 6-trifluoro-5-chloropyrimidine modification are sequentially conducted on the carbon nano tube to obtain a reaction type carbon nano tube; secondly, bismuth salt, a stabilizer, a template agent and the reaction type carbon nano tube are added into phosphate buffered saline to be stirred for 30 min-60 min to form turbid liquid, tungstate is dissolved in the phosphate buffered saline to be added into the turbid liquid, and a transparent solution is formed; thirdly, the transparent solution is filtered and dried to obtain the environment-friendly advanced water treatment agent. The preparation method is low in cost, simple, low in equipment requirement and good in operability. The water treatment agent can be used for removing high-concentration organic pollutants in water, is suitable for advanced treatment of various kinds of wastewater, environmentally friendly and free of secondary pollution and has the advantages of being antibacterial, deodorant, capable of adsorbing other heavy metal ions and the like.
Owner:DONGHUA UNIV +1

Method for preparing rectorite self-assembled bismuth vanadate water treatment agent

The invention relates to a method for preparing a rectorite self-assembled bismuth vanadate water treatment agent, which comprises the following steps of: (1) adding bismuth salt and a stabilizer into phosphate buffer, and stirring for 15 to 60 minutes to form suspension; and dissolving metavanadate in the phosphate buffer, and adding into the suspension to form transparent solution; and (2) regulating the pH value of the transparent solution to be between 4.5 and 9 by using alkaline solution, adding rectorite in a mass ratio of the rectorite to the bismuth salt in the step (1) of 5:1-20:1 at the temperature of between 20 and 100 DEG C, performing reflux reaction for 6 to 24 hours with stirring, and filtering and baking a product. The method is low in cost and simple; and the prepared water treatment agent is suitable for the advanced treatment of multiple kinds of wastewater, is environment-friendly, avoids secondary pollution, can overcome the defects of the conventional bismuth-based water treatment agent, has a good water treatment effect and a good application prospect, and can be recycled.
Owner:DONGHUA UNIV

A preparation method of carbon nanotube composite bismuth molybdate green deep water treatment agent

The invention relates to a preparation method of a carbon nano tube composite bismuth molybdate environmentally friendly and deep water treatment agent. The preparation method comprises the following steps: (1), carboxylation and amination modification are performed on a carbon nano tube and 2,4,6-trifluoro-5-chloro-pyrimidine is modified to prepare a reaction type carbon nano tube; (2), bismuth salt, a stabilizer, a template agent and the reaction type carbon nano tube are added into a phosphate buffer solution, and stirring is performed for 30 to 60 min, so as to form turbid liquid; molybdate is dissolved into the phosphate buffer solution, and then the phosphate buffer solution is added into the turbid liquid, so as to form a transparent solution; (3), the product is obtained after filtering and drying. The preparation method provided by the invention has the advantages that the cost is low, the preparation method is simple, requirements for equipment are low, and the maneuverability is excellent; the water treatment agent can be used for removing high concentration organic pollutants in water, is suitable for deep treatment on various wastewater, environmental protection and zero secondary pollution are achieved, and the water treatment agent is antibacterial, deodorant and can absorb other heavy metal ions and the like.
Owner:DONGHUA UNIV +1

A kind of preparation method of carbon nanotube composite ferric vanadate green advanced water treatment agent

The invention relates to a preparation method for an environment-friendly advanced water treatment agent by combining a carbon nano tube and ferric vanadate. The preparation method includes the steps that firstly, carboxylation, aminated modification and 2, 4, 6-trifluoro-5-chloropyrimidine modification are sequentially conducted on the carbon nano tube to obtain a reaction type carbon nano tube; secondly, molysite, a stabilizer, a template agent and the reaction type carbon nano tube are added into phosphate buffered saline to be stirred for 30 min-60 min to form turbid liquid, metavanadate is dissolved in phosphate buffered saline to be added into the turbid liquid, and a transparent solution is formed; thirdly, the transparent solution is filtered and dried to obtain the environment-friendly advanced water treatment agent. The preparation method is low in cost, simple, low in equipment requirement and good in operability. The water treatment agent can be used for removing high-concentration organic pollutants in water, is suitable for advanced treatment of various kinds of wastewater, environmentally friendly and free of secondary pollution and has the advantages of being antibacterial, deodorant, capable of adsorbing other heavy metal ions and the like.
Owner:DONGHUA UNIV +1

Fiber/CNT(carbon nano tube)/MgFe2O4 three-dimensional recyclable efficient catalytic material, as well as preparation and application thereof

The invention relates to a fiber / CNT(carbon nano tube) / MgFe2O4 three-dimensional recyclable efficient catalytic material, as well as preparation and application thereof. A three-dimensional continuous structure is constructed on the surface of textile fiber by CNTs, and surfaces of the CNTs are loaded with nano MgFe2O4. Preparation comprises: soaking fiber in a dispersion liquid containing CNT compound MgFe2O4 and polyethylene glycol 2000, lasting reaction for 2-4 h at 60-80 DEG C, drying, washing with water, repeating processes of soaking, drying and washing with water for 3-5 times, and obtaining the material. The fiber / CNT / MgFe2O4 three-dimensional recyclable efficient catalytic material is low in cost, the preparation method is simple, requirements on equipment is are low, and the operability is good; a water treatment agent provided by the invention can remove high-concentration organic pollutants in water, is suitable for advanced treatment of various wastewater, protects the environment, avoids secondary pollution, and has the advantages of being antibacterial, removing odor, absorbing other heavy metal ions, and the like.
Owner:DONGHUA UNIV

Sewage treatment device and control method thereof

The invention discloses a sewage treatment device and a control method thereof, and belongs to the technical field of sewage treatment. The device comprises a grating flocculation tank (1) and a biological treatment tank (2) which are connected in sequence; an outlet of the biological treatment tank (2) is connected with the lower part of a photocatalysis tank (4) through a first pump (3), and the first pump (3) conveys sewage from the biological treatment tank (2) to the photocatalysis tank (4); the top of the photocatalytic tank (4) is communicated with a second pump (5), an inlet of the second pump (5) is positioned at the upper part of the photocatalytic pool (4), an outlet of the second pump (5) is connected with a first water quality detection device (11), and an outlet of the first water quality detection device (11) is connected with a first water outlet valve (16); and the device further comprises a third pump (6) which is used for conveying the sewage of the photocatalysis tank (4) to a membrane treatment tank (7).
Owner:常州嘉博染织有限公司

A kind of anti-clogging egr system and control method

The invention discloses an anti-blockage EGR (Exhaust Gas Recirculation) system and a control method. The anti-blockage EGR system comprises an EGR cooling unit, an exhaust waste heat exchange device, an NTP (Non-Thermal Plasma) injection system and a control module, wherein the exhaust waste heat exchange device is arranged at the tail end of an exhaust pipeline; a snake loop pipeline is arranged inside the exhaust waste heat exchange device; the inlet of the snake loop pipeline is connected with the NTP injection system; a nozzle is arranged at the tail end of an injection pipeline at the outlet of the snake loop pipeline; the nozzle extends to the inlet of the EGR cooling unit; both the EGR cooling unit and the NTP injection system are connected with the control module. Oxidation removal of carbon deposit can be realized under the situation that the temperature is lower than the engine exhaust particulate matter combustion temperature; through the exhaust waste heat exchange device for an engine, the reaction reaches a proper reaction temperature range; under the state of normal work of one EGR cooler branch, instant regeneration is performed on another EGR cooler branch, so that regeneration of an EGR cooler is realized efficiently in an energy-saving way, and the problem of blockage of the EGR system is solved.
Owner:JIANGSU UNIV

Fiber/CNT(carbon nano tube)/AgBiOX three-dimensional recyclable efficient catalytic material, as well as preparation and application thereof

The invention relates to a fiber / CNT(carbon nano tube) / AgBiOX three-dimensional recyclable efficient catalytic material, as well as preparation and application thereof. A three-dimensional continuous structure is constructed on the surface of textile fiber by CNTs, and surfaces of the CNTs are loaded with nano AgBiOX. Preparation comprises: soaking fiber in a dispersion liquid containing CNT compound AgBiOX and polyethylene glycol 2000, lasting reaction for 2-4 h at 60-80 DEG C, drying, washing with water, repeating processes of soaking, drying and washing with water for 3-5 times, and obtaining the material. The fiber / CNT / AgBiOX three-dimensional recyclable efficient catalytic material is low in cost, the preparation method is simple, requirements on equipment is are low, and the operability is good; a water treatment agent provided by the invention can remove high-concentration organic pollutants in water, is suitable for advanced treatment of various wastewater, protects the environment, avoids secondary pollution, and has the advantages of being antibacterial, removing odor, absorbing other heavy metal ions, and the like.
Owner:DONGHUA UNIV +1

A kind of carbon nanotube composite wo 3 Preparation method of green deep water treatment agent

The invention relates to a method for preparing a carbon nanotube composite WO3 green deep water treatment agent, which includes: (1) sequentially carboxylating the carbon nanotubes, amination modification, 2,4,6-trifluoro-5-chloropyrimidine Modify to prepare reactive carbon nanotubes; (2) Add nano-WO3, stabilizer, template agent and reactive carbon nanotubes to phosphate buffer, stir for 30 to 60 minutes to form a suspension; (3) Filter and dry Just get the product. The present invention has low cost, simple preparation method, low requirements for equipment and good operability; the water treatment agent of the present invention can remove high-concentration organic pollutants in water, is suitable for the advanced treatment of various wastewaters, and is environmentally friendly and has no secondary pollution. , and has the advantages of antibacterial, deodorizing, and can absorb other heavy metal ions.
Owner:DONGHUA UNIV +1

Fiber/CNT(carbon nano tube)/ZnPc three-dimensional recyclable efficient catalytic material, as well as preparation and application thereof

The invention relates to a fiber / CNT(carbon nano tube) / ZnPc three-dimensional recyclable efficient catalytic material, as well as preparation and application thereof. A three-dimensional continuous structure is constructed on the surface of textile fiber by CNTs, and surfaces of the CNTs are loaded with nano ZnPc. Preparation comprises: soaking fiber in a dispersion liquid containing CNT compound ZnPc and polyethylene glycol 2000, lasting reaction for 2-4 h at 60-80 DEG C, drying, washing with water, repeating processes of soaking, drying and washing with water for 3-5 times, and obtaining the material. The fiber / CNT / ZnPc three-dimensional recyclable efficient catalytic material is low in cost, the preparation method is simple, requirements on equipment is are low, and the operability is good; a water treatment agent provided by the invention can remove high-concentration organic pollutants in water, is suitable for advanced treatment of various wastewater, protects the environment, avoids secondary pollution, and has the advantages of being antibacterial, removing odor, absorbing other heavy metal ions, and the like.
Owner:DONGHUA UNIV

A kind of photoelectric catalytic anode material and treatment method for removing phthalates

The invention relates to a photoelectric catalytic anode material and a treatment method for removing phthalates. The photoelectric catalytic anode material is synthesized in three steps: first, the pseudo-template molecules are modified on the surface of silica microspheres or polystyrene microspheres , and then arrange the modified microspheres into a three-dimensional array of opal structure by self-assembly method, and finally fill the gap between the microspheres with the titanium dioxide sol-gel precursor, and remove the pseudo-template and microspheres by high-temperature annealing, and form titanium dioxide crystals at the same time . This pseudo-template imprinted titania photoelectrocatalytic anode material was used for the removal of phthalate pollutants. Compared with the prior art, the photoelectric catalysis anode material prepared by the invention has special affinity for phthalate pollutants, and can realize the preferential removal of phthalates. In a complex system, complete removal of phthalates can be achieved even under the interference of a thousand times the concentration of natural organic matter.
Owner:TONGJI UNIV

A kind of preparation method of carbon nanotube composite ag/biox green deep water treatment agent

The invention relates to a preparation method for an environment-friendly advanced water treatment agent by combining a carbon nano tube and Ag / BiOX. The preparation method includes the steps that firstly, carboxylation, aminated modification and 2, 4, 6-trifluoro-5-chloropyrimidine modification are sequentially conducted on the carbon nano tube to obtain a reaction type carbon nano tube; secondly, the Ag / BiOX (X=C1, Br and I), a stabilizer, a template agent and the reaction type carbon nano tube are added into phosphate buffered saline to be stirred for 30 min-60 min to form turbid liquid; thirdly, the turbid liquid is filtered and dried to obtain the environment-friendly advanced water treatment agent. The preparation method is low in cost, simple, low in equipment requirement and good in operability. The water treatment agent can be used for removing high-concentration organic pollutants in water, is suitable for advanced treatment of various kinds of wastewater, environmentally friendly and free of secondary pollution and has the advantages of being antibacterial, deodorant, capable of adsorbing other heavy metal ions and the like.
Owner:DONGHUA UNIV +1

Preparation method of layered aluminum matrix composite without residual pyrolytic carbon

The invention relates to a preparation method for a laminated aluminum matrix composite material without residual pyrolytic carbon. The preparation method for the laminated aluminum matrix composite material without residual pyrolytic carbon disclosed by the invention aims at solving the problems that in an existing laminated aluminum matrix composite material preparation process, a thickness control method is complex, thickness control is inaccurate, cost is high, interface combination performance of the laminated composition material is weak, a prefabricated body is prone to collapsing in acomposite material preparation process, and the prepared laminated aluminum matrix composite material has residual pyrolytic carbon. The preparation method comprises the steps: 1, weighing materials;2, preparing SiC slurry; 3, tape casting SiC nanowire raw sheets; 4, preparing the prefabricated body; 5, degreasing, preheating and removing residual pyrolytic carbon; 6, impregnating molten aluminum. According to the preparation method disclosed by the invention, oxidizing and removing the pyrolytic carbon is achieved, preheating time is shortened, the thickness control method is simple, the thickness is accurate, a technology is simple, aluminum foils can separate SiC nanowire layers and further can ensure integrity of a laminated structure of the composite material, and interface combination of the composite material is excellent.
Owner:HARBIN INST OF TECH

Photoelectrocatalysis anode material for removing phthalates and treatment method

The invention relates to a photoelectrocatalysis anode material for removing phthalates and a treatment method. The photoelectrocatalytic anode material is synthesized through three steps: firstly, modifying pseudo template molecules on the surface of silicon dioxide microspheres or polystyrene microspheres; arranging the modified microspheres into a three-dimensional array with an opal structurethrough a self-assembly method, finally filling gaps among the microspheres with a titanium dioxide sol-gel precursor, removing the pseudo template and the microspheres through high-temperature annealing and also forming titanium dioxide crystals. The titanium dioxide photoelectrocatalytic anode material imprinted by the pseudo template is used for removing phthalate pollutants. Compared with thematerials in the prior art, the photoelectrocatalytic anode material has special affinity for phthalate pollutants and can realize preferential removal of phthalate. In a complex system, the completeremoval of the phthalates can still be realized even under the interference of natural organic matters with the concentration of 1000 times.
Owner:TONGJI UNIV

A kind of carbon nanotube composite srfeo 3 Preparation method of green deep water treatment agent

The invention relates to a method for preparing a carbon nano tube composite SrFeO3 green deep water treatment agent. The method comprises the following steps: (1) sequentially performing carboxylated and aminated modification and 2,4,6-trifluoro-5-chloropyrimidine modification on carbon nano tubes, thereby obtaining reactive carbon nano tubes; (2) adding nanometer SrFeO3, a stabilizer, a template agent and the reactive carbon nano tubes into a phosphate buffer solution, stirring for 30-60 minutes, and forming a turbid liquid; and (3) filtering and drying, thereby obtaining the product. The method disclosed by the invention is low in cost, simple in preparation method, low in equipment requirements and high in operability. Moreover, the water treatment agent disclosed by the invention can remove high-concentration organic pollutants in water, is suitable for deep treatment of various kinds of wastewater, is environment-friendly, does not cause secondary pollution and has the advantages of bacteria resistance, deodorization, capacity of adsorbing other heavy metal ions and the like.
Owner:DONGHUA UNIV +1
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