The invention discloses a method for preparing a 13X
molecular sieve by adopting
coal slime. The method comprises the steps of 1,
grinding and sieving the
coal slime, and calcining the sieved matter to obtain
coal slime ash; 2, mixing a
hydrochloric acid solution with the coal slime ash, reacting while stirring, filtering to obtain filter residue, and
drying the filter residue for later use; 3, mixing NaOH with the dried filter residue, and performing alkali fusion to obtain
slag; 4, adding
sodium metaaluminate and water into the
slag, and stirring uniformly to obtain a mixture; 5,
ageing the mixture and then crystallizing to obtain a
solid-liquid mixture; and 6, filtering the
solid-liquid mixture in vacuum to obtain a
filter cake, washing the
filter cake with deionized water, and
drying to obtain the 13X
molecular sieve. By adopting the method, the coal slime can be sufficiently utilized, the
utilization rate and the additional value of the coal slime are greatly improved, the preparation cost of the 13X
molecular sieve is reduced,
land occupation and environmental
pollution caused by accumulating massive 13X molecular
sieve are avoided, and the prepared 13X molecular
sieve product has uniform
granularity distribution and stable quality.