The invention provides a preparation process of a connecting conductor material for a power source system of a new energy vehicle. The preparation process includes discharging, material strip detection, slitting, loading, polymer diffusion welding, surface treatment, punching, polishing, secondary blanking, secondary polishing, electroplating, third-time polishing, sleeving / plastic dipping, inspection, packaging, and the obtaining of the finished product. The polymer diffusion welding step includes first placing the well slit material in a jig for positioning; and a well-positioned to-be-welded material in a graphite welding area for welding. The material has the advantages of strong applicability, strong electrical conductivity, high current resistance, small resistance value and durability. The material is mainly used to connect each unit battery pack in the new energy vehicle power source system to finally form a power system of the electric vehicle.