The invention relates to an ultra low-volume liquid containing metaflumizone and an organophosphorus pesticide. The ultra low-volume liquid comprises a chemical component compounded of metaflumizone and an active ingredient II, and the balance at least one surfactant and at least one solvent, wherein the active ingredient II is any one of fenitrothion, trichlorfon, methyl parathion, isazofos, pyridafenthion, quinalphos, triazophos, fosthiazate, diazinon, phoxim, fenitrothion, pirimiphos-methyl, fenthion, cyanophos, profenofos, chlorpyrifos, chlorpyrifos-methyl, prothiofos, sulprofos, dimethoate, malathion, methidathion and isocarbophos. The ultra low-volume liquid is convenient for processing, has a long duration of efficacy and high efficacy, does not cause pesticide resistance of targets easily, produces low pollution on the environment, saves pesticides and water, improves a pesticide utilization rate, and realizes control of insect pests damaging paddy, wheat, corn, vegetables, tobacco, tea trees, fruit trees and sugarcane through ultra low-volume spraying, low-volume spraying or ultra low-volume electrostatic spraying.