This invention provides a sealing device and method for a high-speed
solid-state NMR rotor. The sealing device includes a first structure, a second structure, a precision
needle gauge, a first base, a second base, a sleeve, a sample, a sample loading tool guide rod, a rotor drive cap, and a manual precision
vise. The sealing method utilizes a sealing
gasket of appropriate thickness, pressed against the inner wall of the rotor by
centrifugal force at high speed, sealing the gap between the bottom cap / drive cap at both ends of the rotor and the inner wall of the rotor, thereby preventing external air from contacting the sample
powder. This invention significantly improves the stability of the sample during sampling and enables the acquisition of high-resolution
solid-state NMR spectra at high speeds. The developed sealing tool can be used in conjunction with the rotor's sample loading tool in the
inert atmosphere of a glove box, achieving the
processing and sealing of
solid-state NMR samples in one step. The method is simple to operate, highly practical, and suitable for various dehydrated samples and solid samples sensitive to water /
oxygen / air.