The invention discloses a preparation method for phosphor powder of lanthanum, cerium, and terbium oxide, and is characterized in that the invention includes the following steps: confecting oxalic acid solution and taking the solution of lanthanum, cerium, and terbium oxide according to the proportion that the ratio of the mass of oxalic acid crystal to the mass of lanthanum, cerium, and terbium oxide equals to 1.2 to 1; adding distilled water or the composite liquid of the distilled water and ethanol into a reaction bottle is heated up to the preset value of 40 to 80 DEG C, and adding a surface additive and then adding acid to the reaction bottle to be stirred in the bottle; using two constant-pressure droppers respectively to add the solution of lanthanum, cerium, and terbium oxide and the oxalic acid solution with the mass proportion at the same time, and the solution of lanthanum, cerium, and terbium oxide and the oxalic acid solution can be dropped at the same time, and then stirring and ageing are went on to carry out; the sediment is separated from the mother liquid, and sucking filtration, washing and drying are carried out after the sediment mother liquid is cleared and cooled to the room temperature; putting the drying matter onto a resistance furnace and the temperature quickly raises to 920 to 980 DEG C and cooling the drying matter after the temperature is kept for 3 to 4 hours. As the surface additive and the acid are added in the crystal reaction process, the lanthanum, cerium, and terbium oxide in polyhedron that is similar to the sphericity is finally obtained.