The invention discloses a preparation method for
phosphor powder of
lanthanum,
cerium, and
terbium oxide, and is characterized in that the invention includes the following steps: confecting
oxalic acid solution and taking the solution of
lanthanum,
cerium, and
terbium oxide according to the proportion that the ratio of the
mass of
oxalic acid crystal to the
mass of
lanthanum,
cerium, and
terbium oxide equals to 1.2 to 1; adding
distilled water or the composite liquid of the
distilled water and
ethanol into a reaction
bottle is heated up to the preset value of 40 to 80 DEG C, and adding a surface additive and then adding acid to the reaction
bottle to be stirred in the
bottle; using two constant-pressure droppers respectively to add the solution of lanthanum, cerium, and terbium oxide and the
oxalic acid solution with the
mass proportion at the same time, and the solution of lanthanum, cerium, and terbium oxide and the oxalic acid solution can be dropped at the same time, and then stirring and
ageing are went on to carry out; the
sediment is separated from the mother liquid, and sucking
filtration, washing and
drying are carried out after the
sediment mother liquid is cleared and cooled to the
room temperature; putting the
drying matter onto a resistance furnace and the temperature quickly raises to 920 to 980 DEG C and cooling the
drying matter after the temperature is kept for 3 to 4 hours. As the surface additive and the acid are added in the
crystal reaction process, the lanthanum, cerium, and terbium oxide in polyhedron that is similar to the
sphericity is finally obtained.