The invention discloses a high luminance gain metal curtain preparation method. The high luminance gain metal curtain preparation method comprises dosing, mixing, film manufacturing and baking processes sequentially. According to the dosing process, raw materials comprise, by weight, 100 parts of polyvinyl chloride (PVC) pastes, 3-10 parts of metal powder, 10-15 parts of anatase titanium dioxide, 70-85 parts of dioctyl phthalate or/and dioctyl adipate plasticizers, 3-8 parts of chlorination aliphatic ester surface treating agents, and 6-10 parts of epoxidized soybean oil heat stabilizers. The mixing process comprises the following steps: premixing all the raw materials in the dosing process S1, grinding sizing agents through a three-roll grinder, standing and dissolving, and dispersing through a dispersion machine. According to the film manufacturing process, a scraper coating machine coats the sizing agents obtained through the mixing process on a curtain blank in a scraping mode. According to the baking process, a subsection baking process with temperature increased successively is adopted for baking the curtain blank coated with the sizing agents in the scraping mode. Compared with the prior art, luminance gain of a metal curtain obtained through the method is high and can reach 3.0-3.5.