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42results about How to "Solve easy collapse" patented technology

Preparation method of super-hydrophobic polytetrafluoroethylene film

The invention provides a preparation method of a polytetrafluoroethylene film. The preparation method comprises the steps of preparing a spinning solution, preparing fibers and sintering and is characterized by adding polytetrafluoroethylene emulsion after preparing a solution with a fiber forming carrier and a solvent, wherein the fiber forming carrier is sodium alginate, and the solvent is water; adopting multistep continuous sintering through program temperature control, and in flowing atmospheres, insulating at 90-120 DEG C for 30-120 minutes, increasing the temperature from 90-120 DEG C to 260-300 DEG C at a rate of 3-10 DEG C/min and insulating at 260-300 DEG C for 30-120 minutes; increasing the temperature from 260-300 DEG C to 370-390 DEG C at a rate of 2-8 DEG C/min and insulating at 370-390 DEG C for 5-120 minutes. The preparation method has the beneficial effects that the problem that fibers are easy to collapse during sintering of a polytetrafluoroethylene precursor film is well solved; a reticular film with bead-like superfine fibers is obtained; the fibers adhere to each other instead of being stacked out of order; the fibers have uniform morphologies, intact surfaces and greatly improved strength and tenacity and can bear a certain vacuum pressure.
Owner:四川百途环保材料科技有限公司 +2

Preparation method of super-hydrophobic polytetrafluoroethylene film

The invention provides a preparation method of a polytetrafluoroethylene film. The preparation method comprises the steps of preparing fibers with a fiber forming carrier and sintering and is characterized by adopting multistep continuous sintering through program temperature control, and in flowing atmospheres, increasing the temperature from a room temperature to 120-200 DEG C at a rate of 3-10 DEG C/min and insulating at 120-200 DEG C for 30-120 minutes; increasing the temperature from 120-200 DEG C to 360-400 DEG C at a rate of 2-8 DEG C/min and insulating at 360-400 DEG C for 5-120 minutes; carrying out cooling treatment after sintering: in the flowing atmospheres, reducing the temperature from 360-400 DEG C to 150-200 DEG C at a rate of 3-15 DEG C/min, insulating at 150-200 DEG C for 30-120 minutes and then carrying out natural cooling. The preparation method has the beneficial effects that the polytetrafluoroethylene film with bead-like superfine fibers is prepared and a hydrophobic surface with a multistage coarse structure is formed together; the surface water contact angle is not less than 150 degrees and the porosity is higher than 80%; the problem that fibers are easy to collapse during sintering of a polytetrafluoroethylene precursor film is solved; the fibers have intact morphologies and surfaces and greatly improved strength and tenacity and can bear a certain vacuum pressure.
Owner:成都百途医药科技有限公司

Preparation method of polytetrafluoroethylene super-hydrophobic membrane

The invention provides a preparation method of a polytetrafluoroethylene membrane. The preparation method comprises spinning solution preparation, fiber formation and sintering. The preparation methodis characterized in that a fiber formation carrier and a solvent are processed into a solution, the solution is added into a polytetrafluoroethylene emulsion, the fiber formation carrier is polyacrylic acid, the solvent is water, the sintering process utilizes programmed temperature-controlled segmented continuous sintering and comprises that in a flowing atmosphere, the materials are heated fromthe room temperature to 120-200 DEG C at a heating rate of 3-10 DEG C / min, then are subjected to heat preservation at 120-200 DEG C for 30-120min, then are heated from the 120-200 DEG C to 360-400 DEG C at a heating rate of 2-8 DEG C / min and then are subjected to heat preservation at 360-400 DEG C for 5-120min, the sintering product is cooled from 360-400 DEG C to 150-200 DEG C at a rate of 3-15DEG C / min in a flowing atmosphere, is subjected to heat preservation at 150-200 DEG C for 30-120min and then is naturally cooled, and the polytetrafluoroethylene membrane has thickness of 174-222 microns. The beaded ultra-fine fiber polytetrafluoroethylene membrane is formed through the preparation method, forms a hydrophobic surface with a multi-level rough structure, has a surface water contactangle of greater than or equal to 150 degrees and porosity of 80% or more, solves the problem that in the polytetrafluoroethylene precursor membrane sintering, fibers easily collapse, has good fiber morphology and surface integrity and higher strength and toughness and can bear a certain vacuum pressure.
Owner:CHENGDU BAITU PHARM TECH CO LTD +2

Preparation method for easy-suturing high-simulation tissue engineering neural repair scaffold

InactiveCN108714247ASolve problemsSolve the problem of nerve stump suturingTissue regenerationProsthesisFreeze-dryingAcetic acid solution
The invention relates to a preparation method for an easy-suturing high-simulation tissue engineering neural repair scaffold. The preparation method comprises a step of preparing suspension, a step ofpreparing an array micro-pipe inner core, a step of preparing collagen outer skin and a step of cutting and assembling. The step of preparing the suspension comprises the following steps: weighing collagen and chitosan, after uniformly mixing, and dissolving in acetic acid solution. The step of preparing the array micro-pipe inner core comprises the following steps: enabling the suspension to beinjected in a mould, inserting a temperature conducting rod, immerging in liquid nitrogen and performing gradient cooling, freeze-drying, crosslinking, washing, freeze-storing and freeze-drying again.The step of preparing the collagen outer skin comprises the following steps: enabling the suspension to be injected in the mould, washing, drying, crosslinking, washing again, freeze-storing and drying again. The step of cutting and assembling comprises the following steps: cutting and assembling. The provided rational preparation method is capable of solving problems of an existing scaffold product that an internal three-dimensional structure is lacked and the collapse is easy, and solving a problem that the parallel and level tail end of the porous scaffold is not easily sutured.
Owner:沈阳尚贤再生医学科技股份有限公司

A kind of preparation method of polytetrafluoroethylene superhydrophobic film

The invention provides a preparation method of a polytetrafluoroethylene film. The preparation method comprises the steps of preparing fibers with a fiber forming carrier and sintering and is characterized by adopting multistep continuous sintering through program temperature control, and in flowing atmospheres, increasing the temperature from a room temperature to 120-200 DEG C at a rate of 3-10 DEG C / min and insulating at 120-200 DEG C for 30-120 minutes; increasing the temperature from 120-200 DEG C to 360-400 DEG C at a rate of 2-8 DEG C / min and insulating at 360-400 DEG C for 5-120 minutes; carrying out cooling treatment after sintering: in the flowing atmospheres, reducing the temperature from 360-400 DEG C to 150-200 DEG C at a rate of 3-15 DEG C / min, insulating at 150-200 DEG C for 30-120 minutes and then carrying out natural cooling. The preparation method has the beneficial effects that the polytetrafluoroethylene film with bead-like superfine fibers is prepared and a hydrophobic surface with a multistage coarse structure is formed together; the surface water contact angle is not less than 150 degrees and the porosity is higher than 80%; the problem that fibers are easy to collapse during sintering of a polytetrafluoroethylene precursor film is solved; the fibers have intact morphologies and surfaces and greatly improved strength and tenacity and can bear a certain vacuum pressure.
Owner:成都百途医药科技有限公司

A kind of preparation method of superhydrophobic polytetrafluoroethylene film

The invention provides a preparation method of a polytetrafluoroethylene film. The preparation method comprises the steps of preparing a spinning solution, preparing fibers and sintering and is characterized by adding polytetrafluoroethylene emulsion after preparing a solution with a fiber forming carrier and a solvent, wherein the fiber forming carrier is sodium alginate, and the solvent is water; adopting multistep continuous sintering through program temperature control, and in flowing atmospheres, insulating at 90-120 DEG C for 30-120 minutes, increasing the temperature from 90-120 DEG C to 260-300 DEG C at a rate of 3-10 DEG C / min and insulating at 260-300 DEG C for 30-120 minutes; increasing the temperature from 260-300 DEG C to 370-390 DEG C at a rate of 2-8 DEG C / min and insulating at 370-390 DEG C for 5-120 minutes. The preparation method has the beneficial effects that the problem that fibers are easy to collapse during sintering of a polytetrafluoroethylene precursor film is well solved; a reticular film with bead-like superfine fibers is obtained; the fibers adhere to each other instead of being stacked out of order; the fibers have uniform morphologies, intact surfaces and greatly improved strength and tenacity and can bear a certain vacuum pressure.
Owner:四川百途环保材料科技有限公司 +2

A kind of preparation method of superhydrophobic polytetrafluoroethylene film

The invention provides a production method of a super-hydrophobic polytetrafluoroethylene membrane. The method comprises the steps of preparing a spinning solution, producing fibers, and sintering, wherein a fiber forming carrier and a solvent are adopted to prepare a solution, a polytetrafluoroethylene emulsion is added, the fiber forming carrier is polyacrylic acid, and the solvent is water; and the sintering step adopts temperature programmed control sectional continuous sintering, and is characterized by carrying out heat insulation in flowing atmosphere at 90-120DEG C for 30-120min, heating to 260-300DEG C from 90-120DEG C at a rate of 3-10DEG C / min, carrying out heat insulation at 260-300DEG C for 30-120min, heating to 370-390DEG C from 260-300DEG C at a rate of 2-8DEG C / min, and carrying out heat insulation at 370-390DEG C for 5-120min. The method well solves the problem of easy collapsing of fibers in the sintering process of a polytetrafluoroethylene precursor membrane, and allows the beaded ultrafine fiber netted membrane, disordered stacking between fibers becomes mutual adhesion, and the fibers have the characteristics of uniform form, complete surface, and greatly improved strength and toughness, and can bear a certain vacuum pressure.
Owner:成都百途医药科技有限公司

Preparation method of super-hydrophobic polytetrafluoroethylene film

The invention provides a preparation method of a polytetrafluoroethylene film. The preparation method of the polytetrafluoroethylene film comprises the steps of preparing a spinning solution, making afiber and sintering. The preparation method is characterized in that a fiber forming carrier and a solvent are prepared into a solution, the solution is added into a polytetrafluoroethylene emulsion,the fiber forming carrier is gelatin, and the solvent is water; sectional continuous sintering is adopted through programmed temperature control, the heat is preserved at the temperature of 90-120 DEG C for 30-120 minutes under the flowing atmosphere, the temperature is raised from 90-120 DEG C to 260-300 DEG C at the speed of 3-10 DEG C per minute, and the heat is preserved at the temperature of260-300 DEG C for 30-120 minutes; the temperature is raised from 260-300 DEG C to 370-390 DEG C at the speed of 2-8 DEG C per minute, and the heat is preserved at the temperature of 370-390 DEG C for5-120 minutes; and the thickness of the polytetrafluoroethylene film is 170-212 [mu]m. The preparation method excellently solves the problem that a fiber collapses easily in the sintering of a polytetrafluoroethylene precursor film, a beaded superfine fiber network film is obtained, the state of the fibers is changed from disordered stacking to mutual adhesion, the fiber morphology is uniform, the surface is complete, the strength and the tenacity are also greatly improved, and the film can bear certain vacuum pressure.
Owner:成都百途医药科技有限公司 +2

A kind of preparation method of polytetrafluoroethylene superhydrophobic film

The invention provides a preparation method of a polytetrafluoroethylene film. The preparation method comprises the steps of preparing a spinning solution, preparing fibers and sintering and is characterized by adding polytetrafluoroethylene emulsion after preparing a solution with a fiber forming carrier and a solvent, wherein the fiber forming carrier is gelatin, and the solvent is water; adopting multistep continuous sintering through program temperature control, and in flowing atmospheres, increasing the temperature from a room temperature to 120-200 DEG C at a rate of 3-10 DEG C / min and insulating at 120-200 DEG C for 30-120 minutes; increasing the temperature from 120-200 DEG C to 360-400 DEG C at a rate of 2-8 DEG C / min and insulating at 360-400 DEG C for 5-120 minutes; carrying out cooling treatment after sintering: in the flowing atmospheres, reducing the temperature from 360-400 DEG C to 150-200 DEG C at a rate of 3-15 DEG C / min, insulating at 150-200 DEG C for 30-120 minutes and then carrying out natural cooling. The preparation method has the beneficial effects that the polytetrafluoroethylene film with bead-like superfine fibers is prepared and a hydrophobic surface with a multistage coarse structure is formed together; the surface water contact angle is not less than 150 degrees and the porosity is higher than 80%; the problem that fibers are easy to collapse during sintering of a polytetrafluoroethylene precursor film is solved; the fibers have intact morphologies and surfaces and greatly improved strength and tenacity and can bear a certain vacuum pressure.
Owner:四川百途环保材料科技有限公司 +2

A kind of preparation method of polytetrafluoroethylene superhydrophobic film

The invention provides a preparation method of polytetrafluoroethylene film, which includes dosing of spinning solution, fiber making and sintering, and is characterized in that polytetrafluoroethylene emulsion is added after the fiber-forming carrier and solvent are prepared into a solution, and the fiber-forming carrier It is sodium alginate, the solvent is water; the sintering adopts the program temperature control segmental continuous sintering, under the flow atmosphere, the temperature is raised from room temperature to 120 ℃ ~ 200 ℃ at a rate of 3 ~ 10 ℃ / min, and the temperature is kept at 120 ℃ ~ 200 ℃ 30-120min; heat up from 120-200°C to 360-400°C at a rate of 2-8°C / min, keep warm at 360°C-400°C for 5-120min; cool after sintering, the cooling is in a flowing atmosphere Cool down from 360-400°C to 150-200°C at a rate of 3-15°C / min, keep warm at 150-200°C for 30-120min, and then cool naturally. The present invention has produced the polytetrafluoroethylene film with beaded superfine fibers, forming a hydrophobic surface with a multi-level rough structure together; the surface water contact angle is more than or equal to 150°, and the porosity is as high as more than 80%; and solves the problem of polytetrafluoroethylene In the sintering of the precursor film, the fiber is easy to collapse, the shape and surface of the fiber are intact, the strength and toughness are also greatly improved, and it can withstand a certain vacuum pressure.
Owner:成都百途医药科技有限公司
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