16 results about "Mass separation" patented technology

The mass spectrometer according to the present disclosure is a mass spectrometer that generates a group of product ions from a precursor ion derived from a sample component having a hydrocarbon chain and performs mass spectrometry thereon, and includes a reaction chamber, an electrode, an introduction unit, a mass separation unit, a detection unit, a power supply unit, and a controller. The controller performs mass spectrometry on the sample component while alternating between a first analysis mode in which ions are detected in a first polarity mode and in a multimode, and a second analysis mode in which ions are detected in a second polarity mode and in a single mode.

A method for producing a positive electrode active material, includes the steps of (1) bringing an electrode mixture containing a positive electrode active material, a binder, and an electrolyte into contact with an electrolyte cleaning solvent to obtain a slurry containing a solid component and a liquid component, and then separating the slurry into the solid component and the liquid component, wherein an amount of P in the liquid component after separation is 0.0020 to 2.0 mass %, an amount of F in the liquid component after separation is 0.01 to 7.0 mass %, and an amount of P remaining in the solid component after separation is 0.7 mass % or less; (2) mixing an activation treatment agent with the separated solid component; and (3) heating a mixture obtained to activate the positive electrode active material contained in the mixture.

An analysis method includes: preparing a sample containing peptide to be analyzed and an antioxidizing agent for preventing oxidation of methionine, the antioxidizing agent containing a protein, ionizing the peptide by laser desorption / ionization; and mass-separating and detecting the peptide that has been ionized.

The present specification relates to the technical field of two-phase flow measurement, and particularly relates to a gas-liquid two-phase flow measurement method and device, computer equipment and a storage medium. The method comprises obtaining a measured volume flow, a measured mass flow and a measured density corresponding to a gas-liquid two-phase flow to be measured by a measurement device; collecting and calculating a first accurate density corresponding to a target liquid, and calculating a second accurate density corresponding to a target gas based on a gas pressure, a gas temperature and the target gas; substituting the measured volume flow, the measured mass flow, the measured density, the first accurate density and the second accurate density into a fitting formula to obtain fitting data; and processing the first accurate density, the second accurate density, the measured volume flow, the fitting data and the measured mass flow by using a mass separation formula to obtain a target gas mass flow and a target liquid mass flow corresponding to the target gas and the target liquid respectively, so that the mass flow of each phase can be determined conveniently and accurately.

The embodiment of the invention provides a hole-reducing efficient rock-breaking blasting time sequence method and system. The method is applied to the technical field of blasting and comprises the steps that a high-energy hole is charged and detonated, a stress field is initialized, and a free face is formed; detonating the main wedge-shaped slotting hole to form a directional crack, and expanding the formed initial free face to form a primary expanded free face; second-stage wedge-shaped slotting holes and caving holes are formed, millisecond detonation is carried out, a second-stage expansion free face is formed, and a caved rock mass is formed; the third-stage slotting holes are charged with explosives, auxiliary hole distribution design is cooperatively carried out, a third-stage expansion free face is formed, and rock mass separation is achieved; and charging the peripheral holes and the floor holes and carrying out collaborative detonation. In this way, the combined blasting mode of the wedge-shaped slotting holes and the high-energy holes is adopted, the positions, where the slotting holes are distributed, of the tunnel face are optimized into the seed cooling holes of the wedge-shaped slotting holes and the high-energy holes, the blasting time sequence of the blast holes is optimized, and the blasting efficiency and energy utilization are improved.

The present mass spectrometer has one or more intermediate vacuum chambers between an ion source to generate ions derived from a sample component in an atmospheric pressure atmosphere and a vacuum chamber where a mass separator is arranged, including an ion transport unit to have an ion outlet in a first intermediate vacuum chamber at a subsequent stage of the ion source and send ions to the first chamber, an exhaust opening portion to evacuate the first chamber, which is provided in front of ion flow discharged from the ion outlet into the first chamber, an ion delivery opening portion to send ions to a next stage, which is provided on a line intersecting a straight line connecting the ion outlet and the exhaust opening portion, and an ion guide to guide ions to the ion delivery opening portion by an action of a radio-frequency electric field.

The preparation method of the high-permeability high-efficiency sulfuric acid catalyst comprises the following steps: adding vanadium pentoxide powder into a potassium sulfate supersaturated solution, dispersing, and adding potassium hydroxide and sodium sulfite until potassium hydroxide and sodium sulfite are dissolved; the preparation method comprises the following steps: slowly adding dilute sulphuric acid at the constant temperature of 60-80 DEG C, adjusting the acid-base property to be neutral, adding polyethylene glycol (6000), sodium benzenesulfonate, soluble starch and organic silicon, stirring at the constant temperature for 15-30 minutes, adding macroporous silicon dioxide powder, stirring for 10 minutes, adding dilute sulphuric acid, and stirring at the constant temperature for 20-30 minutes to obtain a colloidal catalytic activity intermediate; performing equal-mass separation and reunion dispersion on disc-shaped diatomite and straight-chain diatomite to obtain a mixed carrier; and mechanically stirring and mixing the colloidal catalytic activity intermediate, the mixed carrier and the organic matter additive until the catalytic activity substance is fully dispersed in a diatomite skeleton and pore channels, molding to obtain a catalyst wet blank, drying and roasting to obtain the product. The catalyst is good in air permeability, high in catalytic activity and high in thermal stability.

A mass spectrometer including: a reaction chamber into which a precursor ion derived from a sample molecule is introduced; a collision gas supply part configured to supply collision gas to the reaction chamber; a radical supply part configured to supply hydrogen radicals, oxygen radicals, nitrogen radicals, or hydroxyl radicals to the reaction chamber; a dissociation operation control part configured to control operations of the collision gas supply part and the radical supply part to generate the product ions by collision-induced dissociation and radical attachment dissociation of the precursor ion inside the reaction chamber, an ion detection part configured to mass-separate and detect ions ejected from the reaction chamber, and a spectrum data generation part configured to generate spectrum data based on a detection result by the ion detection part.

The invention provides a glow discharge mass spectrometry system for high-purity solid material analysis, and in the system, a glow discharge ion source atomizes a solid sample and ionizes the solid sample into charged ions; the gas source assembly provides a gas environment for ionization and collision reaction; the interface extraction structure and the ion transmission structure cooperate to realize air pressure conversion, ion extraction, transmission and focusing; the collision reaction tank eliminates mass spectrum interference; the quadrupole rod mass analyzer is used for carrying out mass separation on the ions; the detector converts the ion signal into an electric signal; and the vacuum pump system provides a required vacuum environment for each component. The method has the advantages of low matrix effect, high analysis speed, high detection sensitivity, controllable instrument cost and high stability, can directly analyze a solid sample, does not need complex pretreatment, effectively eliminates mass spectrum interference, and realizes rapid and accurate detection of trace components in a high-purity solid material.

In the initial processing phase of a LIB separation system raw lithium-ion batteries are de-energized, and the discharged batteries' circuit boards and exterior metals are removed for recycling. The remaining deconstructed batteries are shredded in the presence of an aqueous solution to form a semi- solid black mass. In a black mass separation phase the black mass is fed into an elutriator that scrubs and separates the material into high specific gravity components and low specific gravity components for subsequent recycling of their respective components. The elutriator may have a rectangular or cylindrical orientation, and is integral to a substantially closed system wherein the volume of aqueous solution is circulated through various subprocesses, and is itself mined for solubilized components.

The utility model relates to the technical field of fuel cells, and discloses a fuel cell bipolar plate and a fuel cell stack, the fuel cell bipolar plate comprises a plate body; a plurality of hydrogen runners are arranged on one side surface of the plate body, and a plurality of oxygen runners are arranged on the other side surface of the plate body; hydrogen main flow holes are formed in the plate body, the hydrogen main flow holes are communicated with the hydrogen flow channels, and hydrogen substances are distributed to the multiple hydrogen flow channels through the hydrogen main flow holes; the oxygen substance is directly communicated with air through a plurality of oxygen flow channels; a cooling cavity is formed in the plate body; a cooling liquid inlet and a cooling liquid outlet are formed in the two opposite corners of the plate body respectively, located at the two ends of the cooling cavity respectively and communicated with the cooling cavity. According to the utility model, the transmission of hydrogen-oxygen reaction gas and the circulating heat dissipation of cooling liquid can be realized at the same time; and a heat flow path and an oxyhydrogen substance flow path can be completely decoupled in a three-dimensional space through heat-mass separation topological setting, so that better heat dissipation and temperature uniformity can be realized.

This invention belongs to the field of lithium-ion battery safety technology and relates to a method for mass decoupling of multiphase ejections during battery thermal runaway. The method obtains the mass of non-condensable reactive gases through a gas analysis measuring tank, obtains the mass of the electrolyte droplets and solid particle mixture ejected during the safety valve opening phase by interrupting heating, and obtains the total mass of electrolyte vapor and non-condensable reactive gases discharged during the thermal runaway phase by continuous heating. Combining this with the total battery mass loss before and after thermal runaway, the method achieves staged mass separation of the multiphase ejections according to mass conservation, and further constructs the hydrodynamic simulation boundary conditions for the discrete phase model. This method can improve the accuracy of mass quantification of multiphase ejections during battery thermal runaway.

Provided is an apparatus capable of performing both mass analysis and electron beam diffraction measurement for identifying isomers by a single measurement. Further, provided is a technique capable of performing electron beam diffraction measurement more efficiently than ever before in such an apparatus. A mass analysis apparatus (1) includes: an ionization section (201) that generates ions from a sample; a mass separation section (231, 235) that mass separates the ions generated by the ionization section; an ion detector (237) that detects the ions mass separated by the mass separation section; an ion trapping section (31) that traps the ions mass separated by the mass separation section; and an electron beam detection section (32) that detects an electron beam diffracted by the ions trapped by the ion trapping section.

A method of mass spectrometry is disclosed comprising: performing a plurality of cycles of operation during a single experimental run, wherein each cycle comprises: mass selectively transmitting precursor ions of a single mass, or range of masses, through or out of a mass separator or mass filter at any given time, wherein the mass separator or mass filter is operated such that the single mass or range of masses transmitted therefrom is varied with time; and mass analysing ions.

A method for producing a positive electrode active material, includes the steps of (1) bringing an electrode mixture containing a positive electrode active material, a binder, and an electrolyte into contact with an electrolyte cleaning solvent to obtain a slurry containing a solid component and a liquid component, and then separating the slurry into the solid component and the liquid component, wherein an amount of P in the liquid component after separation is 0.0020 to 2.0 mass %, an amount of F in the liquid component after separation is 0.01 to 7.0 mass %, and an amount of P remaining in the solid component after separation is 0.7 mass % or less; (2) mixing an activation treatment agent with the separated solid component; and (3) heating a mixture obtained to activate the positive electrode active material contained in the mixture.

The present invention discloses a gas-feeding reaction and separation coupling device and method for enhanced countercurrent mass transfer. The present invention achieves more efficient utilization of the effective components and molecular motion dynamics in the gas feed through the organic combination of gas-feeding mass separation, regionalized feeding, solid-phase drag separation, rational utilization of fluid dynamics, optimized control of reaction kinetics, and enhanced mass transfer. Micronized bubbles are used for countercurrent contact with wastewater, increasing the frequency of gas-liquid contact, enhancing the efficiency of mass transfer and reaction, and improving the mineralization level of wastewater treatment. The reaction zone and separation zone are integrated and coupled to achieve in-situ separation of sludge by properties. This model of invention is suitable for the design of advanced oxidation and advanced biological treatment reactors for wastewater using ozone catalytic oxidation with catalyst addition and biologically activated sludge (anaerobic, aerobic, and hydrolysis).