The invention discloses a method and equipment for preparing high-purity electronic-grade
hydrogen chloride from
hydrogen-rich
hydrogen chloride feed gas. The bid invitation comprises the following steps: (1) removing water through a two-stage deep freezer; (2) further removing water through adsorption of an adsorption
tower; (3) rectifying: directly discharging gas-phase materials at the top of the
tower, namely hydrogen,
carbon dioxide and other non-condensable steam, into an alkali washing section; (4) introducing the material into a light component removal
tower for further rectification, directly discharging a gas-phase material at the top of the tower, namely
hydrogen chloride gas containing C1 and C2, into an alkali washing section, and circulating a material at the bottom of the tower back to the light component removal tower through a
dehydrogenation tower; and (5) introducing the material into a heavy component removal tower for further rectification, directly discharging
hydrogen chloride liquid containing
chlorine and other high-boiling-point impurities in a tower kettle into an alkali washing section, and extracting a
vapor phase at the top of the tower to obtain high-purity electronic-grade
hydrogen chloride. According to the method, the load of the adsorption tower is reduced, and the treatment capacity per unit time is increased; the method has the advantages of simple process, low
energy consumption, high
recovery rate, easiness in stable preparation of high-purity electronic-grade hydrogen
chloride, and facilitation of improvement of production scale and yield.