The invention discloses a
tin-
zinc-
copper powder ultrafine
powder batch preparation process, and relates to the technical field of
metal powder preparation, and the
tin-
zinc-
copper powder ultrafine powder batch preparation process comprises the following steps: dissolving
tin salt,
zinc salt and
copper salt in deionized water, adding a complexing agent, and uniformly mixing to obtain a
mixed metal salt
aqueous solution; dissolving a
rosin-based
polyamine hyperbranched dispersant in an
organic solvent to serve as an
oil phase; slowly adding a
mixed metal salt
aqueous solution into the
oil phase, and uniformly dispersing to obtain a water-in-oil
microemulsion system; dropwise adding a
reducing agent solution, and continuously carrying out heat preservation reaction for 0.5-3 hours after dropwise adding is finished, so as to obtain
slurry containing
alloy particles; and carrying out demulsification treatment,
centrifugal separation, repeated washing and
drying to obtain the surface-modified tin-zinc-copper superfine powder. Superfining of particles is achieved through confinement growth, synchronous co-deposition of multi-component elements is guaranteed, a homogeneous
alloy phase is formed, component segregation is avoided, and a protective layer formed on the surface of the powder in situ endows the material with excellent
oxidation resistance and good weld-aid wettability.